Synthesis and characterization of hierarchical ZSM-5 zeolite containing Ni nanoparticles for one-pot reductive amination of aldehydes with nitroarenes

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1. Department of Chemical Engineering, The University of Melbourne, Parkville, Victoria, 3010 Australia

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In this paper, we wish to report the synthesis and characterization of nickel nanoparticles supported on acidic
form of ZSM-5 zeolite (Ni/H-mZSM-5) with microporous/mesoporous hierarchical structure. This catalyst was
effectively employed as novel acid-metal bi-functional heterogeneous catalyst for direct one-pot reductive
amination of aldehydes with nitroarenes in the presence of NaBH4 as a mild reducing agent. Excellent yields at
room temperature and short reaction time in aqueous media conditions were obtained.

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10.5281/zenodo.6616124

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License: Creative Commons Attribution 4.0 International
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Created: June 6, 2022
Modified: July 16, 2024

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