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.2020 Jan 17;10(1):562.
doi: 10.1038/s41598-019-57262-5.

In situ Rb-Sr dating of slickenfibres in deep crystalline basement faults

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In situ Rb-Sr dating of slickenfibres in deep crystalline basement faults

Mikael Tillberg et al. Sci Rep..

Abstract

Establishing temporal constraints of faulting is of importance for tectonic and seismicity reconstructions and predictions. Conventional fault dating techniques commonly use bulk samples of syn-kinematic illite and other K-bearing minerals in fault gouges, which results in mixed ages of repeatedly reactivated faults as well as grain-size dependent age variations. Here we present a new approach to resolve fault reactivation histories by applying high-spatial resolution Rb-Sr dating to fine-grained mineral slickenfibres in faults occurring in Paleoproterozoic crystalline rocks. Slickenfibre illite and/or K-feldspar together with co-genetic calcite and/or albite were targeted with 50 µm laser ablation triple quadrupole inductively coupled plasma mass spectrometry analyses (LA-ICP-MS/MS). The ages obtained disclose slickenfibre growth at several occasions spanning over 1 billion years, from at least 1527 Ma to 349 ± 9 Ma. The timing of these growth phases and the associated structural orientation information of the kinematic indicators on the fracture surfaces are linked to far-field tectonic events, including the Caledonian orogeny. Our approach links faulting to individual regional deformation events by minimizing age mixing through micro-scale analysis of individual grains and narrow crystal zones in common fault mineral assemblages.

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Conflict of interest statement

The authors declare no competing interests.

Figures

Figure 1
Figure 1
Maps of geological features. (a) Regional Forsmark area with ductile strain character, surrounding major shear zones and Forsmark tectonic lens indicated. (b) Surface map of local Forsmark area (rectangle in “a”) with color coding simply to distinguish the different fracture domains (see Olofssonet al. for details), deformation zones and sampled boreholes (with sub-surface projection). (c) Profile view of transect A’-A” in (b) showing the sub-surface orientation of the deformation zones and the location of the mineral samples at the borehole intercept of the zones. The samples in KFM08A and KFM06C intersect possible deformation zones that are not modeled stochastically and thus not existing in the 3D database. Modified from Stephenset al., and based on data extracted from the site database (Sicada).
Figure 2
Figure 2
Fracture surfaces (a,d, photographs) and micro-textures (b,c,e–g back-scattered SEM-images showing representative detailed examples of common features throughout the fracture surfaces). (a–c) Samples that yielded Proterozoic ages, and (d–g) samples that yielded Paleozoic ages. (a) Photograph of the slickensided open fracture surface of sample DZ4:-549. (b) Illite at the outermost tips of a stepped slickensided fracture surface, sample DZ4:-549. (c) Adularia grown at the outermost tips of steps of a slickensided fault surface in sample ZFM1203:-112. (d) Sample DZ1:-122, with sinistral movement indicated by calcite steps and lineation on illite (light green), chlorite (dark green) and hematite-stained adularia (red). (e) BSE-SEM image of the fracture surface in (d) showing slickensided fabric and stepped appearance of fault surface with adularia and calcite grown at the outermost tips. (f) Slickensided fabric and stepped surfaces with adularia and calcite grown at the outermost tips, sample ZFMA2:-171. (g) Slickensided fabric and stepped surfaces with illite, adularia and calcite grown at the outermost tips, sample ZFMA2:-44. Movement of the missing blocks over the fracture surfaces is indicated, as interpreted in this study based on the stepped appearance of the fracture surface morphology (slickenfibres) and the orientation of the slickenlines. The relative motion of the fracture surface is hence in the opposite direction of the arrow.
Figure 3
Figure 3
Rb-Sr isochrons and corresponding examples of Proterozoic mineral assemblages used for LA-ICP-MS spot analysis. (a) Sample DZ4:-549, yielding 1527 ± 23 Ma, (b) slickenfibre mineral assemblage, consisting of albite and illite. (c) Sample ZFM1203:-112, yielding two isochrons at 1438 ± 33 Ma and a more uncertain at 1074 ± 74 Ma where the initial87Sr/86Sr value is derived from Sandström and Tullborg, (d) fine-grained adularia (with small amounts of albite = dark) overgrowths of two generations on primary perthitic wall rock feldspar on the slickensided surfaces on the open fracture. Errors represented by the ellipses are relative standard errors based on 1σ standard deviations.
Figure 4
Figure 4
Rb-Sr isochrons and corresponding examples of Devonian mineral assemblages used for LA-ICP-MS spot analysis (a) Sample ZFMA2:-44, yielding 398.6 ± 5.1 Ma, (b) slickenfibre mineral assemblage consisting of calcite, chlorite and adularia (illite existing in other aliquots). (c) Sample ZFMA2:-171m, yielding 392 ± 18 Ma, (d) slickenfibre mineral assemblage consisting of fine-grained intergrown calcite and adularia. Errors represented by the ellipses are relative standard errors based on 1σ standard deviations.
Figure 5
Figure 5
Rb-Sr isochrons and corresponding examples of Carboniferous mineral assemblages used for LA-ICP-MS spot analysis (a) Sample DZ1:-122, yielding 348.9 ± 8.6 Ma, (b) slickenfibre mineral assemblage consisting of fine-grained intergrown calcite and adularia. Errors represented by the ellipses are relative standard errors based on 1σ standard deviations.
Figure 6
Figure 6
Stereoplots of fault slip data derived from Saintotet al. with fault planes as lines and striae as arrows according to indicated movement and sense.
Figure 7
Figure 7
Timeline in millions of years before present showing the distribution of previous fracture mineral geochronological data (*=,) compared with the data in this study.
See this image and copyright information in PMC

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