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.2013;61(4):460-3.
doi: 10.1248/cpb.c12-00826.

Niobium(V) chloride catalyzed oxidation of dithioacetals with 30% hydrogen peroxide: a concise preparation of bissulfonylmethylene compounds

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Niobium(V) chloride catalyzed oxidation of dithioacetals with 30% hydrogen peroxide: a concise preparation of bissulfonylmethylene compounds

Masayuki Kirihara et al. Chem Pharm Bull (Tokyo).2013.
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Abstract

The oxidation of dithioacetals with 16 eq of 30% hydrogen peroxide in the presence of 10 mol% niobium(V) chloride at room temperature provides bissulfonylmethylenes in high yields.

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