United States Patent 54] PLASTICIZER WITH FULL DIAMETER ROTOR 7 Claims, 4 Drawing Figs.
[52] US. Cl 259/9; 18/30 [5 l Int. Cl. B01! 7/08 [50] Field ofS earch 259/9, 10,
109, i 10, 2s, 26, 45,465, 6, 21,4o ,41, 10s; l8/3l, 12 (ss 12 SW 3,191,234 6/1965 Hendry 153/12 Primary Examiner-Robert W. Jenkins Attorney-Woodhams, Blanchard and Flynn ABSTRACT: A plasticizing apparatus comprising a feed barrel having a constant diameter opening therethrough, the feed barrel having a rotatable feed screw mounted at one end thereof and a rotatably driven plasticizing element mounted in the other end thereof. The feed screw and the rotor both have a diameter substantially equal to the interior diameter of the feed barrel opening and are coaxially positioned within the opening so as to define a compression and plasticizing zone. The end of the rotor adjacent the feed screw is provided with a steep conical face thereon for coacting with the plastic material for plasticizing same. The screw feeds particulate plastic material into the compression zone whereby the powder is highly compacted and compressed within this zone, the compressed powder thus being forced against the face of the rotor [56] References Cited so as to plasticize the material. Passageways are provided for UNITED STATES PATENTS withdrawing the volatiles from the plasticizing region, the 2,499,398 3/1950 Lyon 18/12 volatiles being withdrawn through the compacted and com- 3,183,55 3 5/ 1965 Slater 259/9 pressed material within the compression zone.
1 24 l" 54 5 I I I I 1l 4/ 42 N 1M 29 1 47 4 43 5s 3/ z/ a 1 1 1 1 v v PLASTICIZER wmi ruu. DIAMETER ROTOR Y FIELD OF Tl-lElNVENTlON The present invention relates to a plasticizing apparatus BACKGROUND OF THE INVENTION The devolatilization of plastic materials has long been a major problem in the plastication and fabrication of plastics. Manyplastic materials are hygroscopic and'thus have a tendency to absorb a considerable amount of moisture. Further, the amount of moisture absorbed by the materials is dependent upon the environmental conditions, such as humidity and temperature, which conditionsundergo considerable varia' tions so that the amount of moisture absorbed by the material is highly variable. Also, in the manufacture of some plastic materials, other volatiles are inherently present and these volatiles are released during the plasticizing operation and must be removed from the material. The problem of removing volatiles from the plasticized material has never been satisfactorily solved and the retention of volatiles within plastic material has often caused products fabricated from the material to have bubbles therein, which products thus are of an inferior quality. a
To assist in the drying of plastic materials, the plastic industry at present often utilizes dryers in the form of hoppers or trays, which dryers contain the granular or particulate plastic material therein, whereupon-the dryers are heated at a fairly low temperature so as to assistin drying and removing the moisture and other volatiles from the plastic material. However, use of these dryers is undesirable and inefficient since the material often must be maintained within the dryer for a considerable length of time in order to remove any appreciable amount of moisture from the material. Further, the use of such dryers still does not solve the-devolatilization problem since the dryers are often ineffective to completely remove all of the moisture and since additional volatiles are released during the plasticizing operation, which volatiles tend to become trapped in the material and cause the material to be of an inferior quality. j; I
The prior art is most closely represented by the plasticizing device illustrated in US. Pat. No. 3,358,334, The plasticizing apparatus of the above patent comprises feed barrel having a first opening in one end thereof rotatably and snugly receiving therein a rotatable conical plasticizing element. The other end of the feed barrel is supplied with a second opening coaxially aligned with and connected tothe first opening, a feeding device, such as a ram or a screw, being operably received within the second opening. Thesecond opening is of substantially smaller diameter than the first opening and is interconnected thereto by means of a tapered portion located in the region of AND closely surrounding the conical nose of the plasticizing element. The tapered portion of the feed barrel generally has an inclination substantially equal to, that is, within at least a few degrees of, the inclination formed on the nose of the rotor element. The tapered portion thus effectively forms a seat surrounding the nose of the plasticizing element. Further, the end of the feed screw is'positioned closely adjacent to the nose of the plasticizing-rotor. Plastic particles such as amorphous or regular powder, granules or the like, hereinafter referred to generally as granular plastic material, is thus fed and compressed by the feeding device into a small region closely adjacent the nose of the plasticizing rotor whereby the material is at least partially plasticized and moved radially outwardly along the conical face of the rotor, thereby being completely plasticized, with the material then being moved to a dispensing port.
The plasticizing apparatus disclosed in Pat. No. 3,358,334 has proven to he highly successful and results in a satisfactory plasticizing operation for most applications. However, the above device is limited in the amount of volatiles which can be withdrawn from the plasticizing region. The conical seat and the small diameter feeding device necessarily define a feeding region closely adjacent the nose of the conical rotor having a relatively small cross-sectional area. Thus, the volatiles produced by the plasticizing operation cannot always be completely withdrawn from this small region and the resulting plasticized product sometimes contains small amounts of volatiles trapped therein. Such a small amount of volatiles may be a of little consequence in some plastics products. However, where it is desired to produce a high grade product which is essentially free of bubbles, this small feeding region often inhibits and prevents removal of a sufficient amount of the volatiles to produce a resultant product of a desired quality.
Accordingly, it is an object of this invention to provide:
1. A plasticizing apparatus capable of removing substantially all volatiles from the plasticized material.
2. A plasticizing apparatus, as aforesaid, wherein the e devolatilization of the plasticized material is carried out at a substantially high temperature.
3. A plasticizing apparatus, as aforesaid, wherein the devolatilization is carried out under a vacuum.
4. A plasticizing apparatus, as aforesaid, wherein the plasticizing apparatus is of the frictional type and has a feed screw of substantially equal diameter as the plasticizing rotor so as to define a relatively large compression and plasticizing zone.
5 A plasticizing apparatus, as aforesaid, wherein a plasticizing rotor and a feed screw of substantially equal diameter are coaxially aligned within a feed barrel having a constant diameter opening therethrough.
6. A plasticizing apparatus, as aforesaid, wherein the compression zone has a large and unobstructed cross-sectional area to permit substantially all volatiles to be removed from the plasticizing zone,
7. A plasticizing apparatus, as aforesaid, which is more economical to manufacture and more efficient to maintain.
Other objects and advantages of the present invention will be apparent to persons acquainted with devices of this type upon reading the accompanying description and inspecting the accompanying drawings.
'BRIEF'DESCRIPTION OF THE DRAWINGS FIG. 1 is an elevational view, partially in cross section, illustrating the plasticizing apparatus of the present invention.
FIG. 2 is an enlargement of a portion of FIG. 1 illustrating the plasticizing zone.
FIG. 3 is a partial sectional view similar to FIG. 2 illustrating the plasticizing zone of the apparatus disclosed in Pat. No. 3,358,334.
FIG. 4 is an elevational view, partially in cross section, of an alternate embodiment of the present invention.
SUMMARY OF THE INVENTION The present invention relates .to a plasticizing apparatus which represents an improvement of the device illustrated in Pat. No. 3,358,334 by permitting more complete removal of the volatiles released by the plasticizing operation.
In particular, the objects and purposes of the present invention are achieved by providing a plasticizing apparatus wherein a feed barrel has a coaxially aligned feed screw and plasticizing element rotatably mounted in respective opposite ends thereof. The feed barrel is provided with a constant diameter feed opening therethrough whereby the feed screw and the rotor are of substantially equal diameters. The adjacent ends of the feed screw and the rotor define a working zone adjacent and between the ends thereof. Granular plastic material is fed from a hopper into the feed screw which in turn feeds the material into the working zone adjacent the end face of the rotating plasticizing element. Continual feeding of material by the feed screw causes the granular material in the working zone to be tightly compacted and pressed against the end face of the rotor. The rotor, which is preferably provided with a tapered conical face thereon, is rotatably driven at a high speed whereby the plastic material compressed against the conical face is rapidly frictionally heated and plasticized. The plasticized material then moved radially outward over the conical face into a small passage between the rotor and the feed barrel and from which it is then transferred to a feed outlet. The feed barrel or the hopper is further interconnected to a suction source whereby the volatiles released during the plasticizing operation are withdrawn through the unplasticized granular material from the plasticizing region The working zone, having a large and unobstructed cross-sectional area, pennits withdrawal of substantially all of the hot volatiles from the plasticizing region, thereby resulting in a high quality product. Also, the large working zone permits a greater amount of material to be plasticized by the device and thus results in a greater delivery rate by the machine.
DETAILED DESCRIPTION A preferred embodiment of my invention is illustrated in FIGS. 1 and 2 wherein there is shown a plasticizing apparatus 11 having a feed barrel orhousing 12 which comprises a generallytubular section 13 having acylindrical opening 16 therein, the ends of thetubular section 13 being closed by means ofend plates 17 and 18 connected thereto by any suitable means such as by welding or by bolts. Ahopper 19 is mounted directly above the feed barrel adjacent one end thereof, the hopper being interconnected to the feed barrel by means of ahopper feed opening 21 whereby the interior of the hopper is in communication with theopening 16 of the feed barrel. The hopper is preferably sealed by means of acover plate 22 having alock feeder 23 positioned therein so as to permit granular or powdered plastic material to be fed into and stored within thehopper 19.
The raw granular plastic material contained within thehopper 19 can be fed into the feed barrel by means of gravity if so desired. However, it is preferably to mount a conveyor screw member 26 within the hopper whereby rotation of this screw will forcibly transfer material from the hopper to thefeed barrel 12. The screw 26 has one end thereof terminating in thehopper feed opening 21 while the other end thereof passes through thecover plate 22 and is connected as convenient to adrive motor 27 which is supported on thecover plate 22 for rotatably driving the screw. The use of a screw within the hopper prevents the material within the hopper from becoming solidified, in which condition the material would be prevented from dropping by gravity into thefeed barrel 12. The hopper is also preferably provided with a pair ofpassageways 28 and 29 leading therefrom, which passageways are connected to a suitable external suction means (not shown) whereby thevapor sand volatiles contained within the hopper and the feed barrel can be removed from the system.
A fedscrew 31 is rotatably positioned within one end of thefeed barrel 12, the feed screw having an outside diameter substantially equal to, but slightly smaller than, the diameter of thefeed opening 16. he feedscrew 31 preferably has a large root diameter so as to subject the particulate plastic material within thehousing 12 to a large compressive force for a purpose to be explained hereinafter. The feed screw is positioned such that a portion thereof is positioned directly beneath thehopper feed opening 21. The feed screw is provided with ashaft portion 32 which extends through and is rotatably supported in an opening 33 provided in theend plate 18. A thrust bearing 34 is positioned between thefeed screw 31 and theend plate 18 for transmitting axial thrusts imposed on the feed screw to thehousing 12. AN O-ring 36 is also preferably mounted between theend plate 18 and theshaft portion 32 of the feed screw so as to effectivelyseal the interior of the feed barrel from the atmosphere. The extendingshaft portion 32 is preferably connected to agear speed reducer 37 which in turn is connected to thedrive shaft 38 of amotor 39. While FIG. 1 illustrates thefeed screw 31 as being driven by thedrive motor 39, it is of course obvious that the fee screw could be driven in any conventional manner.
Other end of thefeed barrel 12 has aplasticizing element 41 rotatably mounted therein, which element is axially aligned with and axially spaced from thefeed screw 31. The plasticizing element comprises first and second coaxialcylindrical portions 42 and 43 respectively, which portions are interconnected by a reduced section orshoulder 46. The plasticizing element is formed with a bearing shaft portion 47 on one end thereof, which portion extends through an opening 48 contained within theend plate 17 and is rotatably supported therein by means ofrotary thrust bearing 49. Ableed seal 51 is preferably formed in on theportion 42 adjacent theend plate 17 so as to effectively seal the interior of thefeed barrel 12 from the atmosphere, thebleed seal 51 being more completely illustrated and described in Pat. No. 3,358,334.
The extending bearing shaft 47 is provided with agear 52 fixedly keyed thereto, which gear is drivingly interconnected to a power source ormotor 54 so as to rotatably drive the plasticizing element within the feed barrel. It will, of course, be obvious that therotating plasticizing element 41 could be driven in any desired manner. For instance, theplasticizing element 41 could be coaxially aligned with and directly connected to themotor 54 or it could be connected to themotor 54 by means of an external drive train consisting of gear, belts or the like. When theplasticizing element 41 is driven by a separate drive motor, it is of course desirably to interconnect the drive motors of the plasticizing element and the feed screw by suitable control means well known in the art so as to permit simultaneous control of the rotation of both thefeed screw 31 and theplasticizing rotor 41. On the other hand, if desired, the plasticizingrotor 41 could be interconnected to thedrive motor 39 of the feed screw by any suitable well known drive means whereby only a single motor is thus utilized for controlling both the rotor and the feed screw. However, use of separate drive motors is preferred.
As is clearly illustrated in FIG. 2, the firstcylindrical portion 42 of the rotor is of a diameter substantially equal to, but slightly less than the diameter of theopening 16 contained in thefeed barrel 12 whereby the cylindrical portion is thus snugly but rotatably received therein. The secondcylindrical portion 43 is of a smaller diameter than the firstcylindrical portion 43 whereby a cylindrical annulus orpassageway 53 is defined between the periphery of the secondcylindrical portion 43 and the interior wall of thefeed barrel 12. The radial clearance comprising theannular passageway 53 will of course vary in magnitude, being dependent upon such factors as the type of plastic, the size of granules, the temperature and the vapor content. The criticalness of the clearance is more thoroughly discussed in Pat. No. 3,358,334. Thefeed barrel 12 is further provided with anoutlet port 56 communicating with thecylindrical passageway 53 in the region adjacent the reduced section orshoulder 46 for a purpose to be explained hereinafter. The front or plasticizingface 57 of therotor 41 is preferably formed with a conical configuration thereon.
The adjacent ends of therotor 41 and thefeed screw 31 are coaxially spaced adjacent one another and, in conjunction with the interior wall of thefeed barrel 13, define a workingzone 60, in which zone the particulate or granular material is subjected to extremely high compressive forces since the material is forced into contact with the taperedplasticizing face 57 by means of therotating feed screw 31. The material within the workingzone 60 closely adjacent the taperedplasticizing face 57 is rapidly frictionally heated by the rotation of therotor 41 and accordingly is plasticized thereby, the position of the working zone which is closely adjacent theplasticizing face 57 thus comprising aplasticizing zone 58. While the material contained within the plasticizing zone, is, for the most part, either partially or completely plasticized,
the remainder of the material in the workingzone 60 is still substantially granular. The high compressive forces on such granular material act against the material in theplasticizing zone 58 for holding same in engagement with theplasticizing face 57. The granular material in the workingzone 60 thus functions substantially in the manner of a stationary seat.
On the other hand, while functioning as a seat, the granular material within the workingzone 60 also functions in a manner similar to a porous plug and the volatiles released in or near theplasticizing zone 58 can pass through such granular material so as to permit such volatiles to be withdrawn through the feed barrel and out of the system. Use of a plug of porous granular material subjected to a high compressive force as a seat for holding material within the plasticizing zone tightly adjacent the plasticizing face is thus highly advantageous since it performs not only the holding function but it also provides a large cross-sectional area of porous material through which the volatiles can be withdrawn, thereby greatly increasing the percentage of the volatiles withdrawn from the plasticized material.
FIG. 3 illustrates the plasticizing region of the prior art device disclosed in Pat. No. 3,358,334 when the screw-fed form thereof is used, The same reference numerals are used to represent the corresponding parts and elements of FIGS. 2 and 3, with the numerals of FIG. 3 having the suffix A" added thereto.
The plasticizing apparatus illustrated in FIG. 3, and shown here for reference purposes to emphasize the exact nature of the present invention, comprises a plasticizing element 41A and a feed screw 31A both of which are rotatably mounted an coaxially aligned within a feedbarrel 12A. The plasticizing element 41A is provided with first andfsecondcylindrical portions 42A and 43A, respectively, which are identical to the first and secondcylindrical portions 42 and 43 as illustrated in FIG. 2. The plasticizing element 41A is provided with aplasticizing face 57A on one end thereof, which face has a generally conical configuration having a gentle taper thereon converging to form a rounded nose 61 at the end thereof as is clearly shown in FIG. 3. Atapered seat portion 59 is formed within the feed barrel 12A, which seat portion surrounds and closely conforms to the periphery of the taperedplasticizing face 57A so as to compress and compact the granular plastic material into the region surrounding the nose 61 of the rotor whereby sufficient pressure is developed to plasticize the material in response to the rotation of the plasticizing element 41A.
In consequence of the taperedplasticizing face 57A and the seat 59surrounding the same, the feed screw 31A is necessarily of a much smaller diameterthan the rotor member as is clearly illustrated in FIG. 3. The cylindrical opening 16A in which is positioned the feed screw 31A is thus of a relatively small cross-sectional area, and thus withdrawal of volatiles from theplasticizing zone 58A is somewhat restricted. l
OPERATION Although the plasticizing operation of the present invention is believed obvious from the description given above, a brief description of the operation will be given below so as to assure a complete and clear understanding thereof.
Referring to FIGS. I and 2, powdered or granular plastic material will be deposited into thefeed hopper 19 through the lockedfeeder 23. Assuming that the hopper screw 26, thefeed screw 31, and theplasticizing element 41 are rotating, the material will be carried from thehopper 19 into theopening 16 contained within thefeed barrel 12. The material deposited into the feed barrel will then be transferred axially therealong by means of afeed screw 31 untilthe material reaches the workingzone 60 andplasticizing zone 58.
After sufficient material has plasticizing deposited into thezones 58 and 60 so as to fill the same, thefeed screw 31 will continue to transfer more material into thezone 60 so as to compact and compress the granular material therein whereupon the material within theplasticizing zone 58 will be forced under high pressure against the taperedplasticizing face 57 of therotating plasticizing element 41. Thefeed screw 31 thus functions as a pressure means for compacting and compressing the material contained within thezones 58 and 60. Due to the high rotational speed of therotor 41, the material within thezone 58 directly adjacent to and compressed against theface 57 by thefeed screw 31 will be rapidly heated and plasticized, the plasticizing action taking place at a relatively high temperature, which temperature may be within the range of 300 F. to 450 F depending upon the material utilized, the speed of rotation of the plasticizing rotor and the pressure imposed by the feed screw. The material will move radially outwardly over theface 57 until it reaches theannular passageway 53, the plasticized material then traveling down the passageway and passing out through theoutlet port 56 into a conventional injection mold or appropriate extruding apparatus. Thus, the plasticizing operation is accomplished solely due to the high rotational speed of therotor 41 and the high compressive pressure applied to the material within thezone 58 by thefeed screw 31..
While the plasticizing operation is being carried out, a suction or partial vacuum is maintained within the plasticizing apparatus by means of an external suction source interconnected thereto through thepassageways 28 and 29. Since thehopper 19 is in communication with the feed barrel opening 16 by means of thehopper feed opening 21 therebetween, the plastic material within the feed barrel will be subjectedto a suction so as to remove the volatiles therefrom. Similarly, the volatiles released adjacent theplasticizing face 57 and within theplasticizing zone 58 during the plastification of the material will be withdrawn axially through the compressed but porous plug of granular material within the workingzone 60, the volatiles then being withdrawn axially along thefeed screw 31 into thehopper 19 from which they are withdrawn by means of thepassageways 28 and 29. Since thezone 60 has a real relatively large and unrestricted cross-sectional area, a partial vacuum developed within the feed barrel is effective in removing a high percentage of the volatiles released during the plasticizing operation and thus the plasticized material delivered by the apparatus is of, a high quality, being essentially free of entrapped volatiles and gas vapors.
MODIFICATION FIG. 4 illustrates a modification of the present invention wherein the plasticizing apparatus is symmetrically positioned about a vertical axis so as to facilitate the transfer of plastic material therethrough. Since the individual components and elements of the invention are basically similar to the embodiment illustrated in FIG. 1, the corresponding parts have been designated by the same reference numerals with the suffix B added thereto.
As shown in FIG. 4, the plasticizing apparatus comprises ahopper 198 which is interconnected to the upper end of thefeed barrel 128, the hopper being provided with an opening in the bottom therein communicating with acylindrical opening 168 formed within thefeed barrel. The hopper is preferably closed and sealed by means of a cover plate 228 connected thereto. The interior of the hopper and the feed barrel is evacuated so as to maintain a partial vacuum therein by means of a suction source (not shown) interconnected thereto by means of thepassages 28!! and 298. A conveyor screw 26B is coaxially positioned within the hopper and extends substantially down into theopening 168 within thefeed barrel 128. the upper end of thescrew 268 being connected to amotor 278 which is fixedly mounted to the cover plate 228. The lower end of the conveyor screw 26B is fixedly interconnected to the feed screw 31B positioned within the opening 16B. The lower end of thefeed barrel 128 has a plasticizing rotor 41B mounted therein for rotation about the vertical axis of the feed barrel. The rotor has a gear 528 externally connected thereto whereby the rotor is driven by means of an external power source 548. The upper end of the rotor is provided with aplasticizing face 578 having a conical surface thereon. The lower end of the feed screw 31B and theplasticizing face 578 of the rotor are axially spaced closely adjacent one another with the region adjacent theplasticizing face 578 constituting a plasticizing zone 588. The granular plastic material is plasticized by therotating face 578 from which the material then passes downwardly through thecylindrical passageway 53B and out through theoutlet port 568.
The operation of the plasticizing apparatus illustrated in H6. 4 is substantially identical to the operation of the device illustrated in H6. 2 as explained above and thus further explanation thereof is not necessary.
The present invention thus relates to a plasticizing machine which possesses a larger feed screw in proportion to the size of the plasticizing rotor and thus results in a larger cross-sectional area being provided between the plasticized and the unplasticized material so that a more complete withdrawal of the volatiles will be obtained. Further, the present invention eliminates the need for a fixed seat closely surrounding the plasticizing rotor so as to define a narrow space therebetween through which the plastic materialmust move, thus permitting the apparatus of the present invention to be able to deliver a larger quantity of plasticized material than in prior known devices.
The plasticizing apparatus according to the present invention thus permits devolatilization of plastic materials to be carried out at much higher temperatures and under vacuum or partial vacuum conditions. This combination of a high temperature and a vacuum environment thus permits substantially complete removal of all volatiles from the plasticized material. Further, this should result in the plasticized material having less heat history and consequently resulting in a plastic material of improved quality. It is also conceivable that some kinds of volatile materials, such as those with very high boiling hydrocarbon constituents, cannot be removed from plastic materials except under vacuum conditions and at extremely high temperatures. The present device is able to withdraw these volatiles from the plasticized material and thus the present invention results in an advantageous operation which was not possible with the prior known plasticizing devices.
In order to permit the volatiles to become completely withdrawn from the system, it will of course be necessary to maintain the volatiles at a sufficient temperature so as to prevent their condensation before being completely withdrawn from the plasticizing device. Accordingly, the rearward end of thefeed barrel 13 adjacent thefeed opening 21 may have to be surrounded with heating chambers or similar devices containing warm air or water therein so as to prevent the volatiles from cooling to a temperature below the condensation temperature. Similarly, it may be desirable to provide a cooling jacket in surrounding relationship to the forward end of thefeed barrel 13 adjacent theplasticizing rotor 41 so as to prevent premature plasticizing of the material before the material reaches the interface area adjacent theplasticizing face 57 whereupon most of the volatiles are released.
The present invention could under same circumstances, as where withdrawal of volatiles is of minor importance, and batch operation is acceptable, be modified by replacing the feed screw with a reciprocable ram member, the ram having a diameter substantially equal to the rotor diameter. Such a ram member would effectively feed and compress the granular material into the compression and plasticizing zone.
Although a particular preferred embodiment of apparatus appropriate for carrying out the method and apparatus embodying the invention has been disclosed in detail hereinabove for illustrative purposes, it will be understood that variations and modifications of such disclosure which lie within the scope of the appended claims are fully contemplated.
lclaim:
1. An apparatus for plasticizing particulate plastic material comprising:
a housing having a cylindrical opening therethrough;
a plasticizing means rotatably mounted w|thm said opening and having a cross section substantially equal to the cross section of said opening, said plasticizing means comprising a rotor rotatably mounted within said opening;
pressure creating means rotatably mounted within said opening and having a cross section substantially equal to the cross section of said opening, the cross section of said pressure creating means being substantially equal to the cross section of said rotor;
said rotor and said pressure creating means being axially spaced along said cylindrical opening and cooperating with said housing to define a working zone for receiving particulate plastic material therein; and
said pressure creating means also feeding particulate plastic material to said working zone whereby said pressure creating means compacts said material and forces a portion thereof into bearing contact with said plasticizing means for plastification thereof.
2. An apparatus according to claim 1, wherein said rotor has a plasticizing face formed on one end thereof defining one wall of said working zone, the plasticizing face having a conical configuration.
3. An apparatus according to claim 2, further including suction means interconnected to said cylindrical opening at a location axially removed from said rotor so as to create a partial vacuum within said opening whereby to withdraw volatiles from the working zone adjacent the rotor, the volatiles being withdrawn through the particulate material contained within the zone.
4. An apparatus according to claim 1, wherein said rotor has a cylindrical portion having a diameter slightly less than the diameter of the cylindrical opening so as to define a narrow passageway therebetween, the rotor also having a tapered conical end face confronting the end of the pressure creating means.
5. An apparatus according to claim 1, further including means for withdrawing volatiles from the plastification region adjacent the rotor through the particulate material contained within said working zone.
6. An apparatus according to claim 1, wherein said pressure creating means comprises a feed screw coaxially positioned within said cylindrical opening, one end of said screw terminating adjacent said rotor.
7. An apparatus according to clam 6, further including an enclosed hopper mounted above one end of the housing, the interior of the hopper being interconnected with the cylindrical opening in the region of the feed screw; and suction means connected to the interior of said hopper so as to create a partial vacuum therein thereby to withdraw the volatiles from the plasticizing region adjacent the rotor, the volatiles being withdrawn through the particulate material contained within the working zone and then through the particulate material contained in the feed screw and the hopper.
UNITED STATES PATENT OFFICE CERTIFICATE OF CORRECTION Patent No. 3 563 514 Dated February 16, 1971 Invent0 Robert Shattuck It is certified that error appears in the above-identified patent and that said Letters Patent are hereby corrected as shown below:
Column 1, line 5; "feed" should read feeds;
line 50; "334," should read --334.---;
line 51; "feed" should read -a feed--;
Column 3,line 56; "vapor sand" should read -vapors and--- line 62; "he" should read -the--.
Column 4, line 30; "gear" should read --gears--;
line 32; "desirably" should read --desirable--.
Column 5, line 72; "plasticizing" should read -been--.
Column 6,line 39; "real relatively" should read --relative Column 7,line 58; "same" should read some.
Signed and seal-ed this 13th day or July 1971.
(SEAL) Attest:
EDJARD M.FLETCHER,JR. WILLIAM E. SCHUYLER, J. Attestlng Officer Commissioner of Patent