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JP2001207265A - Film forming equipment - Google Patents

Film forming equipment

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Publication number
JP2001207265A
JP2001207265AJP2000018887AJP2000018887AJP2001207265AJP 2001207265 AJP2001207265 AJP 2001207265AJP 2000018887 AJP2000018887 AJP 2000018887AJP 2000018887 AJP2000018887 AJP 2000018887AJP 2001207265 AJP2001207265 AJP 2001207265A
Authority
JP
Japan
Prior art keywords
gas
pressure
film
plasma
film formation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
JP2000018887A
Other languages
Japanese (ja)
Inventor
Takahiro Mizoguchi
高宏 溝口
Koji Yokota
浩二 横田
Yoshito Hayakawa
義人 早川
Makoto Maeda
誠 前田
Hironori Hara
裕紀 原
Masami Kubota
昌実 久保田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kubota Corp
Original Assignee
Kubota Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kubota CorpfiledCriticalKubota Corp
Priority to JP2000018887ApriorityCriticalpatent/JP2001207265A/en
Publication of JP2001207265ApublicationCriticalpatent/JP2001207265A/en
Withdrawnlegal-statusCriticalCurrent

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Abstract

Translated fromJapanese

(57)【要約】【構成】 はじめに放電限界下限ガス圧よりも十分に高
い第1圧力の非成膜ガス(Ar)をガス導入手段により
成膜チャンバにスパイク導入し、プラズマ生成手段によ
りプラズマを発生させる。その後、第1圧力より低く放
電限界下限ガス圧よりもやや高い第2圧力すなわちプラ
ズマ放電を持続可能な程度の圧力で非成膜ガスを供給
し、プラズマ放電を安定させて持続させる。そして、成
膜時には、非成膜ガスに替えて成膜ガス(C22)を成
膜チャンバに導入する。成膜後には、再び第2圧力の非
成膜ガスに切り替えて、次の成膜までプラズマ放電を持
続させる。【効果】 非成膜ガスをスパイク導入して、プラズマ放
電を効率よく発生させるようにしたので、より早くプラ
ズマ放電の安定状態を得ることができる。
(57) [Summary] [Configuration] First, a non-deposition gas (Ar) having a first pressure sufficiently higher than a discharge limit lower limit gas pressure is spike-introduced into a deposition chamber by a gas introduction unit, and plasma is generated by a plasma generation unit. generate. Thereafter, the non-deposition gas is supplied at a second pressure lower than the first pressure and slightly higher than the lower limit gas pressure at the discharge limit, that is, a pressure at which the plasma discharge can be sustained, and the plasma discharge is stabilized and maintained. Then, at the time of film formation, a film formation gas (C2 H2 ) is introduced into the film formation chamber instead of the non-film formation gas. After the film formation, the gas is switched again to the non-film formation gas at the second pressure, and the plasma discharge is continued until the next film formation. [Effect] Since a non-deposition gas is spike-introduced to efficiently generate plasma discharge, a stable state of plasma discharge can be obtained more quickly.

Description

Translated fromJapanese
【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】この発明は成膜装置に関し、特に
たとえばハードディスク,半導体装置,LCD,機械部
品または刃物等の被処理体に対してCVD法により成膜
する、成膜装置に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a film forming apparatus, and more particularly to a film forming apparatus for forming a film on an object to be processed such as a hard disk, a semiconductor device, an LCD, a mechanical part or a blade by a CVD method.

【0002】[0002]

【従来の技術】この種の従来の成膜装置では、成膜チャ
ンバ内に成膜ガスを所定圧力で導入し、これをプラズマ
生成装置でプラズマ化して被処理体の表面に堆積させる
ようにしていた。そして、放電の初期段階には、プラズ
マを効率よく発生させるために、成膜チャンバ内のガス
圧を高めに設定していた。
2. Description of the Related Art In a conventional film forming apparatus of this type, a film forming gas is introduced into a film forming chamber at a predetermined pressure, and the gas is converted into plasma by a plasma generating apparatus and deposited on the surface of an object to be processed. Was. In the initial stage of the discharge, the gas pressure in the film forming chamber was set to be high in order to generate plasma efficiently.

【0003】この従来技術では、プラズマ放電開始時か
ら成膜ガスを導入していたので、プラズマ放電が不安定
な成膜初期段階に、性能および品質で劣る膜が多量に形
成されるという問題があった。つまり、成膜初期段階に
は、良好な性能および品質が得られるエネルギレベルよ
りも小さいエネルギのプラズマによって膜の堆積が生じ
るため膜の密着性が悪くなり、膜が剥離し易くなってい
た。また、成膜チャンバの内壁等にもこの質の悪い膜が
堆積されるため、パーティクルの発生原因になってい
た。
In this prior art, since a film forming gas is introduced from the start of plasma discharge, there is a problem that a large number of films having poor performance and quality are formed at the initial stage of film formation in which plasma discharge is unstable. there were. That is, in the initial stage of the film formation, the film is deposited by the plasma having the energy lower than the energy level at which good performance and quality can be obtained, so that the adhesion of the film is deteriorated and the film is easily peeled. In addition, since this poor quality film is deposited on the inner wall of the film forming chamber or the like, it has been a cause of generation of particles.

【0004】そこで、成膜初期段階から安定した膜を形
成するための技術として、たとえば特開平8−4585
7号公報のものが提案されている。この技術は、プラズ
マ放電の開始時に、不活性ガス,窒素ガス,酸素ガス,
水素ガスまたはハロゲンガス等の非成膜ガスのみを一定
圧力で成膜チャンバ内に導入し、この非成膜ガスでプラ
ズマ放電を安定させて持続させ、その後、成膜ガスを成
膜チャンバへ導入するようにしたものである。
Therefore, as a technique for forming a stable film from the initial stage of film formation, for example, Japanese Patent Application Laid-Open No. H8-4585.
No. 7 has been proposed. This technique uses an inert gas, nitrogen gas, oxygen gas,
Only a non-deposition gas such as a hydrogen gas or a halogen gas is introduced into the deposition chamber at a constant pressure, and the plasma discharge is stabilized and maintained by the non-deposition gas, and then the deposition gas is introduced into the deposition chamber. It is something to do.

【0005】[0005]

【発明が解決しようとする課題】上述の従来技術(特開
平8−45857号)では、成膜初期段階に質の悪い膜
が堆積されるのを防止できるものの、非成膜ガスのガス
圧が一定値に設定されていたのでプラズマ放電が安定す
るまでに時間がかかり、生産性が低いという問題があっ
た。
In the above-mentioned prior art (Japanese Patent Laid-Open No. 45857/1996), deposition of a poor quality film at the initial stage of film formation can be prevented, but the gas pressure of the non-film formation gas is reduced. Since it is set to a constant value, it takes time for the plasma discharge to stabilize, and there is a problem that productivity is low.

【0006】それゆえに、この発明の主たる目的は、プ
ラズマ放電の安定状態をより早く得ることができるとと
もに、膜質の劣化を防止できる、成膜装置を提供するこ
とである。
[0006] Therefore, a main object of the present invention is to provide a film forming apparatus capable of obtaining a stable state of plasma discharge more quickly and preventing deterioration of film quality.

【0007】[0007]

【課題を解決するための手段】この発明は、被処理体を
収容する成膜チャンバ、非成膜ガスおよび成膜ガスを切
り替えながら成膜チャンバへ連続的に導入するガス導入
手段、非成膜ガスおよび成膜ガスをプラズマ化するプラ
ズマ生成手段、および非成膜ガスおよび成膜ガスの圧力
を制御する圧力制御手段を備え、非成膜ガスを第1圧力
でスパイク導入してプラズマを発生させ、非成膜ガスを
第1圧力より低い第2圧力で導入してプラズマを持続さ
せ、非成膜ガスに替えて成膜ガスを導入して成膜する、
成膜装置である。
SUMMARY OF THE INVENTION The present invention provides a film forming chamber for accommodating an object to be processed, a gas introducing means for continuously introducing a non-film forming gas and a film forming gas into the film forming chamber while switching the same, and a non-film forming method. A plasma generating means for converting the gas and the film forming gas into a plasma, and a pressure control means for controlling the pressure of the non-film forming gas and the film forming gas, wherein the non-film forming gas is spiked at a first pressure to generate plasma Introducing a non-deposition gas at a second pressure lower than the first pressure to sustain plasma, and introducing a deposition gas in place of the non-deposition gas to form a film;
It is a film forming apparatus.

【0008】[0008]

【作用】たとえば、はじめに放電限界下限ガス圧よりも
十分に高い第1圧力の非成膜ガスをガス導入手段により
成膜チャンバにスパイク導入し、プラズマ生成手段によ
りプラズマを発生させる。その後、第1圧力より低く放
電限界下限ガス圧よりもやや高い第2圧力すなわちプラ
ズマ放電を持続可能な程度の圧力で非成膜ガスを供給
し、プラズマ放電を安定させて持続させる。そして、成
膜時には、非成膜ガスに替えて成膜ガスを成膜チャンバ
に導入する。プラズマ放電は非成膜ガスによって安定し
て持続されるため、非成膜ガスを成膜ガスに切り替えて
もプラズマ放電の安定状態は維持される。成膜後には、
再び第2圧力の非成膜ガスに切り替えて、次の成膜まで
プラズマ放電を持続させる。
For example, first, a non-deposition gas having a first pressure sufficiently higher than the lower limit gas pressure of the discharge limit is spike-introduced into the deposition chamber by the gas introduction means, and plasma is generated by the plasma generation means. Thereafter, the non-deposition gas is supplied at a second pressure lower than the first pressure and slightly higher than the lower limit gas pressure at the discharge limit, that is, a pressure at which the plasma discharge can be sustained, and the plasma discharge is stabilized and maintained. Then, at the time of film formation, a film formation gas is introduced into the film formation chamber instead of the non-film formation gas. Since the plasma discharge is stably maintained by the non-deposition gas, the stable state of the plasma discharge is maintained even if the non-deposition gas is switched to the deposition gas. After film formation,
Switching to the non-deposition gas at the second pressure is again performed, and the plasma discharge is continued until the next deposition.

【0009】[0009]

【発明の効果】この発明によれば、成膜初期段階にたと
えば放電限界下限ガス圧よりも十分に高い第1圧力の非
成膜ガスをスパイク導入して、プラズマ放電を効率よく
発生させるようにしたので、より早くプラズマ放電の安
定状態を得ることができる。
According to the present invention, a non-deposition gas having a first pressure sufficiently higher than, for example, a discharge lower limit gas pressure is spike-introduced at the initial stage of film formation so that plasma discharge can be efficiently generated. Therefore, a stable state of plasma discharge can be obtained more quickly.

【0010】また、第1圧力より低い第2圧力でプラズ
マ放電を安定させて持続させるようにしたので、高エネ
ルギのプラズマによって装置内部が叩かれるのを防止で
き、装置の耐久性を向上できる。
Further, since the plasma discharge is stably maintained at the second pressure lower than the first pressure, it is possible to prevent the inside of the apparatus from being hit by the high-energy plasma, thereby improving the durability of the apparatus.

【0011】この発明の上述の目的,その他の目的,特
徴および利点は、図面を参照して行う以下の実施例の詳
細な説明から一層明らかとなろう。
The above and other objects, features and advantages of the present invention will become more apparent from the following detailed description of embodiments with reference to the drawings.

【0012】[0012]

【実施例】図1を参照して、この実施例の成膜装置10
は、たとえばハードディスクの製造工程において、搬送
機12によって順次搬送される被処理体としての基板1
4にダイアモンドライクカーボン(DLC)膜等のよう
な保護膜を成膜するものである。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Referring to FIG.
For example, in a hard disk manufacturing process, a substrate 1 as an object to be processed which is sequentially transported by the transporter 12 is
In No. 4, a protective film such as a diamond-like carbon (DLC) film is formed.

【0013】ここで、搬送機12は、開口16aを有す
るケーシング16を含み、ケーシング16の内部には、
基板14を搬送する搬送部18が設けられる。搬送部1
8は、上下方向へ変位可能な保持部20を含み、保持部
20の基部には鍔22が形成され、鍔22の上面にはO
リング等のような環状のシール材24が装着される。
Here, the transporter 12 includes a casing 16 having an opening 16a.
A transport unit 18 that transports the substrate 14 is provided. Transport unit 1
8 includes a holding portion 20 that can be displaced in the vertical direction, a flange 22 is formed at the base of the holding portion 20, and an O
An annular sealing material 24 such as a ring is mounted.

【0014】成膜装置10は、基板14の表面に成膜す
るプラズマCVD装置(以下、単に「CVD装置」とい
う。)26を含む。CVD装置26は、基板14を収容
する成膜チャンバ28を含み、成膜チャンバ28の互い
に対向する2つの側面には開口28aが形成され、上面
には排気口28bが形成され、下面には開口28cが形
成される。そして、各開口28aにはプラズマ生成装置
30が取り付けられ、排気口28bには真空ポンプ等の
ような図示しない圧力制御手段(排気手段)が接続され
る。
The film forming apparatus 10 includes a plasma CVD apparatus (hereinafter, simply referred to as “CVD apparatus”) 26 for forming a film on the surface of the substrate 14. The CVD apparatus 26 includes a film forming chamber 28 for accommodating the substrate 14, an opening 28a is formed on two opposite sides of the film forming chamber 28, an exhaust port 28b is formed on the upper surface, and an opening 28b is formed on the lower surface. 28c are formed. A plasma generator 30 is attached to each of the openings 28a, and a pressure control unit (exhaust unit) (not shown) such as a vacuum pump is connected to the exhaust port 28b.

【0015】プラズマ生成装置30は、たとえば米国特
許第5,858,477号公報において開示されたよう
な周知のものであり、図2からよくわかるように、ガス
導入部32およびプラズマ生成部34を含む。ガス導入
部32は導入管36を含み、導入管36の先端にはプラ
ズマ生成部34を構成するRF電極38が形成される。
また、RF電極38の先方にはプラズマ生成領域を囲む
ようにして磁石40が配置され、さらにその先方にはグ
リッド42が配置される。
The plasma generating apparatus 30 is a well-known type as disclosed in, for example, US Pat. No. 5,858,477. As can be clearly understood from FIG. 2, the gas introducing section 32 and the plasma generating section 34 are connected to each other. Including. The gas introduction unit 32 includes an introduction tube 36, and an RF electrode 38 constituting the plasma generation unit 34 is formed at a tip of the introduction tube 36.
Further, a magnet 40 is arranged in front of the RF electrode 38 so as to surround the plasma generation region, and a grid 42 is further arranged in front of the magnet 40.

【0016】また、ガス導入部32の導入管36には、
図1に示すように、図示しないガス供給源からの成膜ガ
スを導く1つの管路44aと非成膜ガスを導く2つの管
路44bおよび44cとが接続され、管路44aおよび
44cには、各ガスの流量を制御するためのマスフロー
コントローラ(MFC)46が設けられ、管路44bに
は、非成膜ガスをスパイク導入すなわち短時間に高圧で
導入するためのピエゾバルブ48が設けられる。さら
に、各管路44a,44bおよび44cにおけるマスフ
ローコントローラ(MFC)46またはピエゾバルブ4
8の下流側には、導入ガスを切り替えるための切替バル
ブ50が設けられる。なお、ピエゾバルブ48は、トグ
ル式の手動バルブ等のような瞬間的に開閉できる他のバ
ルブに置き換えられてもよい。
The introduction pipe 36 of the gas introduction section 32 has
As shown in FIG. 1, one conduit 44a for guiding a film forming gas from a gas supply source (not shown) is connected to two conduits 44b and 44c for leading a non-film forming gas, and the conduits 44a and 44c are connected to the conduits 44a and 44c. A mass flow controller (MFC) 46 for controlling the flow rate of each gas is provided, and a piezo valve 48 for introducing a non-film-forming gas by spikes, that is, a high pressure in a short time, is provided in the pipeline 44b. Further, a mass flow controller (MFC) 46 or a piezo valve 4 in each of the pipes 44a, 44b and 44c is provided.
On the downstream side of 8, a switching valve 50 for switching the introduced gas is provided. Note that the piezo valve 48 may be replaced with another valve that can be opened and closed instantaneously, such as a toggle-type manual valve.

【0017】そして、ガス導入部32には、成膜ガスお
よび非成膜ガスのいずれかが、切替バルブ50によって
選択的に供給され、RF電極38にはRF電源52から
電力が印加される。したがって、ガス導入部32からプ
ラズマ生成部34にガス(成膜ガスまたは非成膜ガス)
が導入されると、そのガスがプラズマ化され、磁石40
によって作られる双曲線形磁場54およびグリッド42
を通して成膜チャンバ28内へ導入される。
Then, one of a film forming gas and a non-film forming gas is selectively supplied to the gas introducing section 32 by a switching valve 50, and power is applied to the RF electrode 38 from an RF power supply 52. Therefore, the gas (film-forming gas or non-film-forming gas) is supplied from the gas introduction unit 32 to the plasma generation unit 34.
Is introduced, the gas is turned into plasma and the magnet 40
Magnetic field 54 and grid 42 produced by
Through the film formation chamber 28.

【0018】なお、基板14にDLC膜を成膜するため
には、アセチレン,メタン,エタン,エチレン,ベンゼ
ンまたはトルエン等のような炭化水素系のガスが成膜ガ
スとして用いられ、プラズマ放電の安定持続のために
は、アルゴン,ヘリウムまたはネオン等の不活性ガス等
が非成膜ガスとして用いられる。
In order to form a DLC film on the substrate 14, a hydrocarbon-based gas such as acetylene, methane, ethane, ethylene, benzene or toluene is used as a film-forming gas to stabilize plasma discharge. For sustaining, an inert gas such as argon, helium, or neon is used as a non-film-forming gas.

【0019】成膜装置10は、成膜チャンバ28の開口
28cが搬送機12の開口16aに位置的に対応するよ
うにして、搬送機12に固定される。これにより、搬送
機12と成膜チャンバ28とが連通され、CVD装置2
6内へ基板14を搬送するための搬送路56が得られ
る。
The film forming apparatus 10 is fixed to the carrier 12 such that the opening 28 c of the film forming chamber 28 corresponds to the opening 16 a of the carrier 12. As a result, the transfer device 12 and the film forming chamber 28 communicate with each other, and the CVD device 2
A transfer path 56 for transferring the substrate 14 into the inside 6 is obtained.

【0020】以下には、図3に従って、成膜装置10を
用いて基板14にDLC膜を成膜する方法を説明する。
なお、この実施例では、成膜ガスとしてアセチレン(C
22)を、非成膜ガスとしてアルゴン(Ar)を用いる
ものとする。
A method for forming a DLC film on the substrate 14 using the film forming apparatus 10 will be described below with reference to FIG.
In this embodiment, acetylene (C
2 H2 ) using argon (Ar) as a non-film-forming gas.

【0021】はじめに管路44aの切替バルブ50を閉
鎖するとともに管路44bおよび44cの各切替バルブ
50を開放し、管路44cから一定流量のアルゴンガス
を導入するとともに、ピエゾバルブ48によって管路4
4bから所定量のアルゴンガスを瞬間的に導入する。つ
まり、アルゴンガスをプラズマ放電下限ガス圧(約0.
1〜0.4mTorr)よりも十分に高い第1ガス圧
(約1.5〜5mTorr)でスパイク導入する。そし
て、このスパイク導入のタイミングに合わせてRF電極
38に電力(約300W)を印加し、プラズマを発生さ
せる。
First, the switching valve 50 of the pipe 44a is closed, and the switching valves 50 of the pipes 44b and 44c are opened. A constant flow rate of argon gas is introduced from the pipe 44c.
A predetermined amount of argon gas is instantaneously introduced from 4b. That is, the argon gas is supplied to the plasma discharge lower limit gas pressure (about 0.
The spike is introduced at a first gas pressure (approximately 1.5-5 mTorr) well above 1-0.4 mTorr. Then, power (approximately 300 W) is applied to the RF electrode 38 in synchronization with the timing of the spike introduction to generate plasma.

【0022】プラズマが発生した後は、ピエゾバルブ4
8およびその下流の切替バルブ50を閉じることによっ
て、第1圧力より低くかつ放電限界下限ガス圧よりもや
や高い第2圧力(約0.5mTorr)のアルゴンガス
を管路44cから所定時間導入し、プラズマ放電を安定
させる。つまり、比較的低いガス圧でプラズマ放電を安
定させて持続させる。
After the plasma is generated, the piezo valve 4
8 and the downstream switching valve 50, an argon gas having a second pressure (about 0.5 mTorr) lower than the first pressure and slightly higher than the discharge lower limit gas pressure is introduced from the pipe 44c for a predetermined time, Stabilizes plasma discharge. That is, the plasma discharge is stabilized and maintained at a relatively low gas pressure.

【0023】プラズマ放電が安定すると、アルゴンガス
(非成膜ガス)に替えて、第1圧力よりも低くかつ第2
圧力より高い第3圧力(約1.5mTorr)のアセチ
レンガス(成膜ガス)を成膜チャンバ28に導入し、R
F電極38に印加する電力を大きくする(約300
W)。そして、搬送機12の保持部20を上昇させて、
保持部20に固定された基板14を成膜チャンバ28内
に搬入し、基板14に対して成膜する。なお、保持部2
0を上昇させると、鍔22に装着されたシール材24が
搬送機12のケーシング16に圧接されて搬送路54が
封鎖されるので、成膜時におけるアセチレンガスの漏洩
は生じない。
When the plasma discharge is stabilized, the pressure is lower than the first pressure and the second pressure is changed to the second gas instead of the argon gas (non-deposition gas).
An acetylene gas (deposition gas) at a third pressure (about 1.5 mTorr) higher than the pressure is introduced into the deposition chamber 28, and R
The power applied to the F electrode 38 is increased (about 300
W). Then, the holding unit 20 of the transporter 12 is raised,
The substrate 14 fixed to the holding unit 20 is carried into the film forming chamber 28 and a film is formed on the substrate 14. The holding unit 2
When 0 is raised, the sealing material 24 attached to the flange 22 is pressed against the casing 16 of the transfer device 12 and the transfer path 54 is closed, so that acetylene gas does not leak during film formation.

【0024】成膜が終わると、基板14を成膜チャンバ
28から搬出し、導入ガスを第3圧力のアセチレンガス
から第2圧力のアルゴンガスに切り替えるとともに、R
F電極38に印加する電力を小さくする(約200
W)。それにより、プラズマ放電の安定状態を持続させ
て、次の成膜が開始されるまで待機する。
When the film formation is completed, the substrate 14 is unloaded from the film formation chamber 28, and the introduced gas is switched from acetylene gas at the third pressure to argon gas at the second pressure.
The power applied to the F electrode 38 is reduced (about 200
W). Thus, a stable state of the plasma discharge is maintained, and the process waits until the next film formation is started.

【0025】そして、次に処理する基板14が搬送機1
2により搬送されてくると、導入ガスを第2圧力のアル
ゴンガスから第3圧力のアセチレンガスに切り替えると
ともに、RF電極38に印加する電力を大きくし(約3
00W)、成膜チャンバ28内に基板14を搬入して成
膜する。このようにして、成膜およびプラズマ放電の安
定持続を交互に繰り返す。
Then, the substrate 14 to be processed next is
2, the gas to be introduced is switched from argon gas at the second pressure to acetylene gas at the third pressure, and the power applied to the RF electrode 38 is increased (about 3
00W), the substrate 14 is loaded into the film forming chamber 28 to form a film. In this way, the film formation and the stable maintenance of the plasma discharge are alternately repeated.

【0026】この実施例によれば、はじめに非成膜ガス
のスパイク導入によってプラズマを効率よく発生させる
ようにしたので、より早くプラズマの安定放電を得るこ
とができ、生産性を向上できる。
According to this embodiment, first, plasma is efficiently generated by introducing a spike of a non-deposition gas, so that a stable plasma discharge can be obtained more quickly and productivity can be improved.

【0027】また、成膜の必要がないときでも、成膜チ
ャンバ28に非成膜ガスを導入してプラズマ放電を安定
状態で持続させるようにしたので、繰り返し成膜を行う
場合には、2回め以降の成膜工程において成膜ガスのス
パイク導入を省略できる。
Even when film formation is not necessary, a non-film formation gas is introduced into the film formation chamber 28 to maintain plasma discharge in a stable state. The spike introduction of the deposition gas can be omitted in the subsequent deposition steps.

【0028】さらに、プラズマ放電を安定持続させる際
には、非成膜ガスの圧力を第1圧力よりも低い第2圧力
に設定しているので、成膜装置10の内部が高エネルギ
のプラズマで叩かれるのを防止できる。
Further, when the plasma discharge is stably maintained, the pressure of the non-film-forming gas is set to the second pressure lower than the first pressure, so that the inside of the film-forming apparatus 10 is made of high-energy plasma. It can be prevented from being hit.

【0029】なお、上述の実施例では、この発明をハー
ドディスク基板14に対する成膜に適用した場合を示し
たが、この発明は、半導体装置,LCD,機械部品また
は刃物等のような他の被処理体に対する成膜にも同様に
適用できる。
In the above-described embodiment, the case where the present invention is applied to film formation on the hard disk substrate 14 has been described. However, the present invention is not limited to the case where the present invention is applied to other processing such as a semiconductor device, an LCD, a mechanical part or a blade. The same can be applied to film formation on a body.

【図面の簡単な説明】[Brief description of the drawings]

【図1】この発明の一実施例を示す図解図である。FIG. 1 is an illustrative view showing one embodiment of the present invention;

【図2】図1実施例で用いられるプラズマ生成装置を示
す図解図である。
FIG. 2 is an illustrative view showing a plasma generating apparatus used in the embodiment in FIG. 1;

【図3】ガス圧の経時変化を示すタイミングチャートで
ある。
FIG. 3 is a timing chart showing a change over time in gas pressure.

【符号の説明】[Explanation of symbols]

10 …成膜装置 12 …搬送機 14 …基板 26 …プラズマCVD装置 28 …成膜チャンバ 30 …プラズマ生成装置 46 …マスフローコントローラ 48 …ピエゾバルブ 50 …切替バルブ DESCRIPTION OF SYMBOLS 10 ... Film-forming apparatus 12 ... Carrier 14 ... Substrate 26 ... Plasma CVD apparatus 28 ... Film-forming chamber 30 ... Plasma generation apparatus 46 ... Mass flow controller 48 ... Piezo valve 50 ... Switching valve

───────────────────────────────────────────────────── フロントページの続き (72)発明者 早川 義人 兵庫県伊丹市奥畑5丁目10番地 株式会社 クボタ内 (72)発明者 前田 誠 兵庫県伊丹市奥畑5丁目10番地 株式会社 クボタ内 (72)発明者 原 裕紀 兵庫県伊丹市奥畑5丁目10番地 株式会社 クボタ内 (72)発明者 久保田 昌実 兵庫県伊丹市奥畑5丁目10番地 株式会社 クボタ内 Fターム(参考) 4K030 AA09 AA16 BA28 BB12 CA12 EA03 FA02 HA04 JA09 KA30 LA19 5F045 AA08 AB07 AC01 BB08 EE02 EE14 EE19 EH19 EN04 ──────────────────────────────────────────────────続 き Continuing on the front page (72) Inventor Yoshito Hayakawa 5-10-10 Okuhata, Itami-shi, Hyogo Pref. (72) Inventor Makoto Maeda 5-10-10 Okuhata, Itami-shi, Hyogo Pref. (72) Inventor Hiroki Hara 5-10 Okuhata, Itami City, Hyogo Prefecture Inside Kubota Corporation (72) Inventor Masami Kubota 5-10-10 Okuhata, Itami City, Hyogo Prefecture F-term in Kubota Corporation (reference) 4K030 AA09 AA16 BA28 BB12 CA12 EA03 FA02 HA04 JA09 KA30 LA19 5F045 AA08 AB07 AC01 BB08 EE02 EE14 EE19 EH19 EN04

Claims (3)

Translated fromJapanese
【特許請求の範囲】[Claims]【請求項1】被処理体を収容する成膜チャンバ、 非成膜ガスおよび成膜ガスを切り替えながら前記成膜チ
ャンバへ連続的に導入するガス導入手段、 前記非成膜ガスおよび前記成膜ガスをプラズマ化するプ
ラズマ生成手段、および前記非成膜ガスおよび前記成膜
ガスの圧力を制御する圧力制御手段を備え、 前記非成膜ガスを第1圧力でスパイク導入してプラズマ
を発生させ、前記非成膜ガスを前記第1圧力より低い第
2圧力で導入して前記プラズマを持続させ、前記非成膜
ガスに替えて前記成膜ガスを導入して成膜する、成膜装
置。
A film forming chamber for accommodating an object to be processed; gas introducing means for continuously introducing a non-film forming gas and a film forming gas into the film forming chamber while switching the film forming gas; the non-film forming gas and the film forming gas Plasma generating means for converting the non-film-forming gas and the pressure of the film-forming gas into a plasma, and spike-introducing the non-film-forming gas at a first pressure to generate plasma; A film forming apparatus for introducing a non-film-forming gas at a second pressure lower than the first pressure to maintain the plasma, and introducing the film-forming gas instead of the non-film-forming gas to form a film.
【請求項2】前記成膜ガスを前記第1圧力より低くかつ
前記第2圧力より高い第3圧力で導入する、請求項1記
載の成膜装置。
2. The film forming apparatus according to claim 1, wherein said film forming gas is introduced at a third pressure lower than said first pressure and higher than said second pressure.
【請求項3】成膜後、前記成膜ガスに替えて前記非成膜
ガスを前記第2圧力で連続的に導入する、請求項1また
は2記載の成膜装置。
3. The film forming apparatus according to claim 1, wherein, after forming the film, the non-film forming gas is continuously introduced at the second pressure in place of the film forming gas.
JP2000018887A2000-01-272000-01-27 Film forming equipmentWithdrawnJP2001207265A (en)

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