Vegetable capsule of starch composition and preparation methodTechnical field
The invention belongs to medical and health, healthcare products, makeup and functional food field, particularly a kind of vegetable capsule of starch composition and preparation method.
Background technology
Capsule has very in medicine, healthcare products and functional food industry to be used widely.Conventional capsules to be utilized by the skin of animal, gelatin that the bone hydrolysis makes as capsule casing material.Yet, along with spreading of European mad cow disease and foot and mouth disease, and the transformation of consumption idea, people begin to query the security of animals products.Therefore, plant capsule is gone with the tide of historical development becomes the market of medicine, healthcare products, makeup and functional food new lover.At present the plant capsule demand of world market and is the trend that grows steadily at 15,000,000,000 according to estimates.The cellulose capsule Vcaps of U.S. exploitation has been used for the packing of some drugs, healthcare products, makeup, has just used the Vcaps plant capsule as the product of Sunrider (Sunrider) company.Domestic Harbin Hong Tai company utilizes the carrageenin that extract from marine alga to develop plant capsule for main raw material.But the said products still can not contend with traditional gelatine capsule on production cost or price.
Summary of the invention
In order to solve deficiency of the prior art, the invention provides a kind of vegetable capsule of starch composition prescription and preparation method.
The vegetable capsule of starch composition prescription is as follows:
A kind of vegetable capsule of starch composition prescription, component and content are as follows:
10 parts of starch,
1 ~ 6 part in polyalcohols, polyose or long-chain fat acids softening agent,
0.15 ~ 2 part of vegetable jelly and inorganic salts gel,
0 ~ 0.3 part of the esters surface active agent of negatively charged ion or non-ionic type,
0 ~ 2 part of natural or synthetic oxide compound or calcium salt opalizer,
0 ~ 0.3 part of food dye,
0 ~ 0.3 part in oxidation inhibitor of edible natural,
0 ~ 0.2 part of sanitas of food,
0 ~ 0.2 part of derivatived cellulose and water-soluble polymers toughener.
Described starch is common starch or modified starch: starch comprises wheat starch, W-Gum, arrowroot starch, Starch rice, yam starch and tapioca (flour); Modified starch mainly comprises starch acetate, starch-phosphate, Sumstar 190, pregelatinized Starch, hydroxypropylated starch, carboxymethyl starch, hydroxyethylamyle, hydrolyzed starch or dextrin; Above-mentioned starch is to select for use one or more to mix to use.
Described polyalcohols, polyose or long-chain fat acids softening agent are that one or more mixing of glycerine, polyoxyethylene glycol, sorbyl alcohol, N.F,USP MANNITOL, Xylitol, stearic acid, Palmiticacid, fructose, sucrose, maltose, Oligomeric maltose or triethyl citrate are used; For the hard film preparation, plasticizer dosage is 1 ~ 3 part; For the flexible film preparation, plasticizer dosage is 2 ~ 6 parts.
Described vegetable jelly and inorganic salts gel are Viscogum BE, and one or more of carrageenin, sodium alginate, carrageenin, tara gum, xanthan gum, ghatti gum, tragacanth gum, konjak mannan, gum gellan, araban, pectin, kuteera gum, Sudan Gum-arabic, salt of wormwood, yellow soda ash, Repone K, sodium bicarbonate, sodium-acetate or Potassium ethanoate mix use.
The esters surface active agent of described negatively charged ion or non-ionic type is sodium lauryl sulphate, dimethyl polysiloxane, Sodium dodecylbenzene sulfonate, glyceryl monooleate, sorbitan ester class, Yelkin TTS, Vinlub, dioctyl alkyl succinic acid sodium or sucrose fatty acid ester.
Described natural or synthetic oxide compound or calcium salt opalizer are that titanium dioxide, silicon-dioxide, ferric oxide, lime carbonate, natural algae soil are as diatomite or potter's clay.
Described food dye is that riboflavin, anthocyanidin, carotene, turmeric, cochineal extract, ponceau 4R, acid bright green BS, patent blue V, red iron oxide, iron oxide yellow, iron oxide black, carbon black, D+C are red 33, D+C is red 22, D+C is red 26, D+C is red 28, D+C Huang 10, yellow 2G, red 2G, FD+C are green 3, FD+C blue 1 or FD+C indigo plant 2.
Described edible natural oxidation inhibitor be gallic acid ester, Rosmarinus officinalis, carotene, phytic acid, xitix, tea-polyphenol, monascorubin, cacao color or phosphatide.
Described food sanitas is Sodium Benzoate, P-hydroxybenzoic acid sodium, potassium sorbate or propylparaben.
Described derivatived cellulose and water-soluble polymers toughener are polyvinyl alcohol, hydroxypropylcellulose, Walocel MT 20.000PV or Polyvinylpyrolidone (PVP).
The preparation method of vegetable capsule of starch composition prescription of the present invention, starch or starch composites are mixed, be dispersed in the distilled water of 10-200 part, heated 15-60 minute down at 60-95 ℃, make the abundant lakeization of starch, add softening agent, gel, tensio-active agent, opalizer, food dye, sanitas, oxidation inhibitor and toughener by proportioning then, thorough mixing is the back vacuum defoaming evenly, and the glue that obtains can rotate punch die encystation method or dropping method makes starch composites plant soft capsule with routine; Or making the starch composites plant hollow hard capsule with mode dunking method, the encystation temperature is at 40-95 ℃, preferred 50-85 ℃.
The invention has the advantages that: with the starch composites is main raw material, be that pure natural is pollution-free, and raw material sources is extensive, and production cost is low.
Embodiment
Example 1:
Get 10 parts of starch, wherein tapioca (flour) and pregelatinized Starch are each 5 parts, add in 140 parts the deionized water, stir 4min, 85 ℃ of following gelatinizations, treat that gelatinization adds 2 parts of glycerine, 0.3 part polyvinyl alcohol, 0.2 part sodium alginate in the back fully, stir and make its thorough mixing, utilize conventional capsular production unit and production technique to produce starch plant soft capsule and empty hard capsule after mixing.
Softening agent glycerine can change sorbyl alcohol, Xylitol, polyoxyethylene glycol, stearic acid, Palmiticacid, sucrose, triethyl citrate etc. in the body series.
The gel sodium alginate can change carrageenin, tara gum, xanthan gum, ghatti gum, tragacanth gum, konjak mannan, gum gellan, araban, pectin, kuteera gum, Sudan Gum-arabic etc. into.
Example 2:
Get 10 parts starch, wherein yam starch is 3 parts, 2 parts of 5 parts of tapioca (flour)s and hydrolyzed starches, the deionized water that adds 190 parts, stir 4min, 75 ℃ of following gelatinizations, treat that the complete back of gelatinization adds 3 parts softening agent, wherein glycerine is 2 parts, 1 part of polyoxyethylene glycol, 0.3 the sodium lauryl sulphate of part, 0.4 the gel of part, wherein carrageenin is 0.2 part, 0.1 part of xanthan gum, 0.1 part in salt of wormwood, 0.1 the titanium dioxide of part, 0.1 the acid bright green BS of part stirs and makes its thorough mixing, utilizes conventional capsular production unit and production technique to produce starch plant soft capsule and empty hard capsule after mixing.
In the body series gelling system salt of wormwood can yellow soda ash, Repone K, sodium bicarbonate, sodium-acetate, Potassium ethanoate etc.
Tensio-active agent sodium lauryl sulphate (SLS) can change dimethyl polysiloxane, Sodium dodecylbenzene sulfonate, glyceryl monooleate, sorbitan ester class, Yelkin TTS, dioctyl alkyl succinic acid sodium, sucrose fatty acid ester, Vinlub into.Opalizer titanium dioxide can change silicon-dioxide, ferric oxide, lime carbonate, natural algae soil into as diatomite, potter's clay etc.
The acid bright green BS of food dye can change riboflavin, anthocyanidin, carotene, turmeric, cochineal extract, ponceau 4R, patent blue V, red iron oxide, iron oxide yellow, iron oxide black etc. into.
Example 3:
Get 10 parts starch, wherein 3 parts of Sumstar 190s, 3 parts of hydroxypropylated starchs and konjak starch are 4 parts, add 150 parts deionized water, stir 5min, 90 ℃ of gelatinizations, after treating gelatinization fully, add 2 parts softening agent, wherein the hydroxypropylcellulose of 1.5 parts of glycerine, 0.5 part, 0.5 part of stearic acid, 0.4 the gelling system of part, wherein 0.2 part of carrageenin, 0.1 part of tragacanth gum, 0.1 part of Potassium ethanoate, 0.1 part titanium dioxide, 0.1 part acid bright green BS stir and make its thorough mixing.Like this starch solution homogeneous 4min under high-speed stirring of preparation, carry out the vacuum froth breaking again after, can utilize conventional capsular production unit and production technique to produce starch plant soft capsule and empty hard capsule then.
Opalizer titanium dioxide can change silicon-dioxide, ferric oxide, lime carbonate, natural algae soil into as diatomite, potter's clay etc. in the body series.
The toughener hydroxypropylcellulose can change polyvinyl alcohol, Walocel MT 20.000PV, Polyvinylpyrolidone (PVP) into.
Example 4:
Get 10 parts starch, wherein 6 parts of Sumstar 190s, 2 parts of W-Gums and wheat starch are 2 parts, the distilled water that adds 120 parts stirs 5min, at 90 ℃ of gelatinization 45min, treat that gelatinization fully adds 3 parts glycerine and 1 portion of maltose, 1 part sodium alginate, 0.1 part polyvinyl alcohol, 0.2 part dioctyl sodium sulphosuccinate, 0.1 part tea-polyphenol, 0.2 part acid bright green BS in the back, stirring mixes it.Like this preparation starch mixture solution homogeneous 4min under high-speed stirring, carry out the vacuum froth breaking again after, can utilize conventional capsular production unit and production technique to produce starch plant soft capsule and empty hard capsule then.
Example 5:
Get 10 parts starch, wherein 5 parts of yam starchs, 3 parts of starch acetates and 2 parts in dextrin,, the distilled water that adds 90 parts stirs 4min, at 95 ℃ of gelatinization 40min, treat that the complete back of gelatinization adds 3 parts softening agent, wherein 1.5 parts of stearic acid, 1.5 parts of Palmiticacid, 1 part gelling system, wherein 0.5 part of carrageenin, 0.2 part of sodium bicarbonate and konjak mannan are 0.3 part, and 0.1 part potassium sorbate, 0.3 part acid bright green BS fully stir it is mixed.So preparation starch mixture solution homogeneous 4min under high-speed stirring after carrying out the vacuum froth breaking, can utilize conventional capsular production unit and production technique to produce starch plant soft capsule and empty hard capsule then.
Example 6:
Get 10 parts starch, wherein 4 parts of arrowroot starchs, 4 parts of hydrolyzed starches and carboxymethyl starch are 2 parts, the distilled water that adds 140 parts stirs 4min, at 90 ℃ of gelatinization 45min, treat that the complete back of gelatinization adds 2 parts softening agent, wherein 1.5 parts of glycerine and polyoxyethylene glycol are 0.5 part, 1 part gelling system, wherein 0.7 part of carrageenin and Repone K are 0.3 part, 1 part diatomite, 0.3 part acid bright green BS, 0.1 part tea-polyphenol, and fully stirring mixes it.So preparation starch mixture solution homogeneous 4min under high-speed stirring after carrying out the vacuum froth breaking, can utilize conventional capsular production unit and production technique to produce starch plant soft capsule and empty hard capsule then.
The present invention is not limited to the technology described in the embodiment; its description is illustrative; and it is nonrestrictive; authority of the present invention is limited by claim; based on present technique field personnel according to the present invention can change, technology related to the present invention that method such as reorganization obtains, all within protection scope of the present invention.