技术领域Technical field
本发明涉及一种材料，特别是涉及应用于化学领域的一种OMSA高分子聚合物材料。The present invention relates to a material, in particular to an OMSA high molecular polymer material used in the chemical field.
背景技术Background technique
OMSA高分子聚合物是一种聚酰胺类高分子材料，由单体在催化剂的作用下进行缩聚反应制备而成的，采用不同的单体，可以制备出不同性能的OMSA高分子聚合物，只有选择合适的单体，才能制备出理想性能的OMSA高分子聚合物。OMSA polymer is a polyamide polymer material, which is prepared by the polycondensation reaction of monomers under the action of a catalyst. Using different monomers, OMSA polymers with different properties can be prepared. Only Only by selecting appropriate monomers can OMSA polymers with ideal properties be prepared.
OMSA高分子聚合物是一种新兴的材料，其性能和应用领域还在不断拓展和完善中，选择什么样的单体，才能制备出适用于设备损坏处的修补、重塑与再造的OMSA高分子聚合物，是我们亟需解决的问题。因此，我们提出一种OMSA高分子聚合物材料。OMSA polymer is an emerging material, and its performance and application fields are still being expanded and improved. What kind of monomer should be selected to prepare OMSA polymer suitable for repairing, reshaping and rebuilding of damaged equipment? Molecular polymers are a problem that we urgently need to solve. Therefore, we propose an OMSA polymer material.
发明内容Contents of the invention
针对上述现有技术，本发明要解决的技术问题是：如何制备出适用于设备损坏处的修补、重塑与再造的OMSA高分子聚合物。In view of the above-mentioned existing technologies, the technical problem to be solved by the present invention is: how to prepare OMSA polymer suitable for repairing, reshaping and rebuilding damaged parts of equipment.
为解决上述问题，本发明提供了一种OMSA高分子聚合物材料，OMSA高分子聚合物材料由单体和催化剂通过熔融缩聚反应制备而成，单体为尼龙66盐，催化剂为三氟化硼；In order to solve the above problems, the present invention provides an OMSA polymer material. The OMSA polymer material is prepared from a monomer and a catalyst through a melt polycondensation reaction. The monomer is nylon 66 salt and the catalyst is boron trifluoride. ;
OMSA高分子聚合物材料的制备方法包括以下步骤：The preparation method of OMSA polymer material includes the following steps:
S1、将适量单体添加至反应釜中，对单体进行加热熔化；S1. Add an appropriate amount of monomer to the reaction kettle, and heat and melt the monomer;
S2、将适量催化剂添加至反应釜中，使催化剂和熔融状态的单体进行混合；S2. Add an appropriate amount of catalyst into the reaction kettle to mix the catalyst and the molten monomer;
S3、将温度升高至375℃，使单体在催化剂的作用下进行缩聚反应；S3. Raise the temperature to 375°C to allow the monomer to undergo polycondensation reaction under the action of the catalyst;
S3、反应完成后，即可制得液态的OMSA高分子聚合物。S3. After the reaction is completed, the liquid OMSA polymer can be obtained.
上述OMSA高分子聚合物材料，是以尼龙66盐为单体、三氟化硼为催化剂，经熔融缩聚反应制备而成的，其具有良好的力学性能、耐磨性、耐腐蚀性和耐高温性，特别适用于设备损坏处的修补、重塑与再造。The above-mentioned OMSA polymer material is prepared through melt polycondensation reaction using nylon 66 salt as the monomer and boron trifluoride as the catalyst. It has good mechanical properties, wear resistance, corrosion resistance and high temperature resistance. It is particularly suitable for repairing, reshaping and rebuilding damaged equipment.
作为本申请的进一步改进，反应釜的釜体上设置有活气提效机构，活气提效机构包括推拉气缸、活气筒，活气筒内设置有与之滑动密封连接的活塞板，活塞板的左端固定连接有连接杆，连接杆贯穿活气筒左端的外壁并与之滑动连接，连接杆的左端固定连接有保温隔热杆，推拉气缸的输出端上固定连接有联动板，联动板的底端与保温隔热杆固定连接，活气筒右端的外壁上贯穿嵌设有进气管，进气管的左端设置有与之相匹配的阻排塞，阻排塞和进气管上下两侧的内壁之间均固定连接有弹性拉绳，活气筒的底端外壁上贯穿嵌设有排气管，排气管的底端处设置有与之滑动密封连接的阻进塞，阻进塞的顶端固定连接有竖杆，竖杆和排气管左右两侧的内壁之间均固定连接有弹性吊绳。As a further improvement of this application, the body of the reaction kettle is provided with a mechanism for improving the efficiency of activated gas. The mechanism for improving efficiency of activated gas includes a push-pull cylinder and an activated gas cylinder. A piston plate is provided in the activated gas cylinder and is connected with it in a sliding and sealing manner. The left end of the piston plate is fixed. There is a connecting rod connected, which penetrates through the outer wall of the left end of the active cylinder and is slidingly connected with it. The left end of the connecting rod is fixedly connected with a thermal insulation rod. The output end of the push-pull cylinder is fixedly connected with a linkage plate. The bottom end of the linkage plate is connected to the thermal insulation rod. The heat insulation rod is fixedly connected. The outer wall of the right end of the air cylinder is embedded with an air inlet pipe. The left end of the air inlet pipe is provided with a matching blocking plug. The blocking plug is fixedly connected to the inner walls of the upper and lower sides of the air inlet pipe. There is an elastic drawstring, and an exhaust pipe is embedded in the outer wall of the bottom end of the air cylinder. The bottom end of the exhaust pipe is provided with a blocking plug that is slidingly and sealingly connected to it. The top of the blocking plug is fixedly connected with a vertical rod. Elastic hanging ropes are fixedly connected between the vertical rod and the inner walls on the left and right sides of the exhaust pipe.
作为本申请的进一步改进，推拉气缸通过支撑板固定安装在釜体的顶端，活气筒位于釜体内，且活气筒与釜体的顶端内壁固定连接，保温隔热杆贯穿釜体的左侧外壁并与之滑动密封连接，且保温隔热杆采用隔热保温材料制成，阻排塞设置为左粗右细的圆台状，可大大提高催化剂与单体的接触面积，从而能显著提高缩聚反应的反应效率。As a further improvement of this application, the push-pull cylinder is fixedly installed on the top of the kettle body through the support plate, the activating air cylinder is located in the kettle body, and the activating air cylinder is fixedly connected to the top inner wall of the kettle body, and the thermal insulation rod runs through the left outer wall of the kettle body and It is connected with a sliding seal, and the heat insulation rod is made of heat insulation material. The blocking plug is set in a truncated cone shape with a thick left and a thin right, which can greatly increase the contact area between the catalyst and the monomer, thereby significantly improving the efficiency of the polycondensation reaction. reaction efficiency.
作为本申请的进一步改进，竖杆的顶端固定连接有与排气管相匹配的防偏网，防偏网与排气管滑动连接，防止阻进塞偏离排气管，阻进塞的顶端设置为球面状，防止单体进入到排气管内，排气管左右两侧的内壁上均固定安装有阻升块，阻升块位于阻进塞的上方，使得推拉气缸向左拉动活塞板时，阻进塞不会向上移动。As a further improvement of this application, the top end of the vertical rod is fixedly connected with an anti-deviation net that matches the exhaust pipe. The anti-deviation net is slidingly connected to the exhaust pipe to prevent the obstruction plug from deviating from the exhaust pipe. The top end of the obstruction plug is provided It is spherical in shape to prevent the monomer from entering the exhaust pipe. Anti-lift blocks are fixedly installed on the inner walls of the left and right sides of the exhaust pipe. The anti-lift blocks are located above the blocking plug, so that when the push-pull cylinder pulls the piston plate to the left, The choke will not move upward.
作为本申请的进一步改进，进气管上下两侧的内壁上均固定安装有防偏块，防偏块的一端与阻排塞相抵，且防偏块与阻排塞相抵的一端设置为与阻排塞相匹配的形状，防止阻排塞偏离进气管。As a further improvement of this application, anti-deviation blocks are fixedly installed on the inner walls of the upper and lower sides of the intake pipe. One end of the anti-deviation block offsets the discharge plug, and the end of the anti-deviation block and the discharge plug is set to be in contact with the discharge plug. The matching shape of the plug prevents the obstruction plug from deviating from the intake pipe.
作为本申请的又一种改进，活气提效机构还包括固定安装在釜体顶端的活气智控器，活气智控器中设置有触控面板、自动活气模块、周期设置模块、安全检密模块，触控面板与自动活气模块电连接，自动活气模块与推拉气缸电连接，周期设置模块与自动活气模块电连接，可提高活气提效机构的自动化、智能化程度。As another improvement of the present application, the vitality improvement mechanism also includes an intelligent vitality controller fixedly installed on the top of the kettle body. The intelligent vitality controller is provided with a touch panel, an automatic vitality module, a cycle setting module, and a safety inspection module. , the touch panel is electrically connected to the automatic live gas module, the automatic live gas module is electrically connected to the push-pull cylinder, and the period setting module is electrically connected to the automatic live gas module, which can improve the automation and intelligence of the live gas efficiency improvement mechanism.
作为本申请的又一种改进的补充，活气提效机构还包括安全检密组件，安全检密组件包括套设在保温隔热杆上的安检密封盒，安检密封盒的顶端外壁上贯穿嵌设有密封筒，密封筒的顶端内壁上固定安装有电动伸缩杆，电动伸缩杆的输出端上固定连接有与密封筒相匹配的推气板，安检密封盒的内壁上固定安装有气压传感器。As another improved supplement of this application, the live gas efficiency improvement mechanism also includes a safety inspection component. The safety inspection component includes a security inspection sealing box set on the thermal insulation rod. The top outer wall of the security inspection sealing box is embedded through There is a sealing cylinder. An electric telescopic rod is fixedly installed on the top inner wall of the sealing cylinder. An air push plate matching the sealing cylinder is fixedly connected to the output end of the electric telescopic rod. An air pressure sensor is fixedly installed on the inner wall of the security sealing box.
作为本申请的又一种改进的补充，保温隔热杆贯穿安检密封盒并与之固定连接，安检密封盒设置为与釜体相匹配的扇形状，安检密封盒的一端与釜体的外壁紧密贴合并设置为开口状，推气板与密封筒滑动密封连接，密封筒的底端设置为开口状。As another improved supplement of this application, the thermal insulation rod penetrates the security seal box and is fixedly connected to it. The security seal box is set in a fan shape matching the kettle body. One end of the security seal box is closely connected to the outer wall of the kettle body. Fitted and set in an open shape, the air pushing plate is slidingly and sealingly connected with the sealing cylinder, and the bottom end of the sealing cylinder is set in an open shape.
作为本申请的又一种改进的补充，安全检密组件还包括固定安装在活气智控器顶端的反馈灯，活气智控器中还设置有安全检密模块，触控面板与安全检密模块电连接，安全检密模块与电动伸缩杆电连接，气压传感器与安全检密模块电连接，安全检密模块与反馈灯电连接，反馈灯可发出红色和绿色两种颜色的灯光，可大大提高活气提效机构的可靠性和安全性。As another improved supplement of this application, the safety inspection component also includes a feedback light fixedly installed on the top of the vitality intelligent controller. The vitality intelligent controller is also provided with a safety inspection module, a touch panel and a safety inspection module. Electrical connection, the safety inspection module is electrically connected to the electric telescopic pole, the air pressure sensor is electrically connected to the safety inspection module, the safety inspection module is electrically connected to the feedback light, the feedback light can emit red and green lights, which can greatly improve The reliability and safety of the live gas efficiency improvement mechanism.
作为本申请的又一种改进的补充，密封筒的外壁上开设有通气孔，通气孔位于推气板的上方，有利于推气板的上、下移动。As another improved supplement of the present application, a ventilation hole is provided on the outer wall of the sealing cylinder, and the ventilation hole is located above the air pushing plate, which is beneficial to the upward and downward movement of the air pushing plate.
综上所述，本申请中的OMSA高分子聚合物材料以尼龙66盐为单体、三氟化硼为催化剂，经熔融缩聚反应制备而成，其具有良好的力学性能、耐磨性、耐腐蚀性和耐高温性，特别适用于设备损坏处的修补、重塑与再造，弥补了OMSA高分子聚合物在这一应用领域的空白；通过活气提效机构的设置，使得活气提效机构可将处在单体上方、难以与单体充分接触的混合气体，导向熔化的单体，致使混合气体中的催化剂能与单体充分接触，结合反应釜的搅拌功能，可大大提高催化剂与单体的接触面积，能显著提高缩聚反应的反应效率，进而可有效提高生产效率；通过活气智控器的设置，使得工作人员无需手动去控制推拉气缸，从而可提高活气提效机构的自动化、智能化程度；通过安全检密组件的设置，使得开始制备之前，安全检密组件可对保温隔热杆和釜体外壁连接处进行密封性检测，防止因保温隔热杆和釜体外壁连接处的密封性存在缺陷而产生安全事故，进而可大大提高活气提效机构的可靠性和安全性。To sum up, the OMSA polymer material in this application is prepared through melt polycondensation reaction using nylon 66 salt as the monomer and boron trifluoride as the catalyst. It has good mechanical properties, wear resistance, and Corrosive and high temperature resistance, it is especially suitable for repairing, reshaping and rebuilding damaged equipment, filling the gap of OMSA polymer in this application field; through the setting of the active gas efficiency improvement mechanism, the active gas efficiency improvement mechanism can The mixed gas that is above the monomer and is difficult to fully contact with the monomer is directed to the molten monomer, so that the catalyst in the mixed gas can fully contact the monomer. Combined with the stirring function of the reactor, it can greatly improve the relationship between the catalyst and the monomer. The contact area can significantly improve the reaction efficiency of the polycondensation reaction, which can effectively improve production efficiency; through the setting of the live gas intelligent controller, the staff does not need to manually control the push-pull cylinder, thereby improving the automation and intelligence of the live gas efficiency improvement mechanism. degree; through the setting of the safety inspection component, before starting the preparation, the safety inspection component can conduct a sealing test on the connection between the insulation rod and the outer wall of the kettle to prevent the sealing of the connection between the insulation rod and the outer wall of the kettle. Safety accidents may occur due to defects in performance, which can greatly improve the reliability and safety of the active gas efficiency improvement mechanism.
附图说明Description of drawings
图1为本申请第一种实施方式中OMSA高分子聚合物材料的性能测试结果；Figure 1 shows the performance test results of the OMSA polymer material in the first embodiment of the present application;
图2为本申请第一种实施方式中活气提效机构的立体结构示意图；Figure 2 is a schematic three-dimensional structural diagram of the vitality improvement mechanism in the first embodiment of the present application;
图3为本申请第一种实施方式中活气提效机构安装至反应釜釜体上后的结构示意图；Figure 3 is a schematic structural diagram of the active gas efficiency improving mechanism installed on the reactor body in the first embodiment of the present application;
图4为本申请第一种实施方式中活气筒处的剖视结构示意图；Figure 4 is a schematic cross-sectional structural view of the active air cylinder in the first embodiment of the present application;
图5为本申请第一种实施方式中进气管处的剖视结构示意图；Figure 5 is a schematic cross-sectional structural view of the air inlet pipe in the first embodiment of the present application;
图6为本申请第一种实施方式中排气管处的剖视结构示意图；Figure 6 is a schematic cross-sectional structural view of the exhaust pipe in the first embodiment of the present application;
图7为本申请第二种实施方式中活气提效机构的立体结构示意图；Figure 7 is a schematic three-dimensional structural diagram of the vitality improvement mechanism in the second embodiment of the present application;
图8为本申请第二种实施方式中安检密封盒处的侧视剖面结构示意图；Figure 8 is a schematic side sectional structural view of the security inspection sealing box in the second embodiment of the present application;
图9为本申请第二种实施方式中活气智控器的系统结构框图。Figure 9 is a system structural block diagram of the vitality intelligent controller in the second embodiment of the present application.
图中标号说明：Description of numbers in the figure:
101、推拉气缸；102、活气筒；103、活塞板；104、连接杆；105、保温隔热杆；106、联动板；107、进气管；108、阻排塞；109、弹性拉绳；110、排气管；111、阻进塞；112、竖杆；113、弹性吊绳；114、防偏网；115、防偏块；116、阻升块；117、支撑板；002、活气智控器；301、安检密封盒；302、密封筒；303、电动伸缩杆；304、推气板；305、气压传感器；306、反馈灯；307、通气孔。101. Push-pull cylinder; 102. Active air cylinder; 103. Piston plate; 104. Connecting rod; 105. Insulation rod; 106. Linkage plate; 107. Intake pipe; 108. Blocking plug; 109. Elastic pull cord; 110 , exhaust pipe; 111. blocking plug; 112. vertical rod; 113. elastic sling; 114. anti-deviation net; 115. anti-deviation block; 116. resistance block; 117. support plate; 002. vitality intelligent control 301. Security sealing box; 302. Sealing cylinder; 303. Electric telescopic rod; 304. Air push plate; 305. Air pressure sensor; 306. Feedback light; 307. Ventilation hole.
具体实施方式Detailed ways
下面结合附图对本申请的两种实施方式作详细说明。Two embodiments of the present application will be described in detail below with reference to the accompanying drawings.
第一种实施方式：First implementation:
图1-6示出一种OMSA高分子聚合物材料，所述OMSA高分子聚合物材料由单体和催化剂通过熔融缩聚反应制备而成，所述单体为尼龙66盐，所述催化剂为三氟化硼；Figures 1-6 show an OMSA polymer material. The OMSA polymer material is prepared from a monomer and a catalyst through a melt polycondensation reaction. The monomer is nylon 66 salt, and the catalyst is nylon 66 salt. boron fluoride;
所述OMSA高分子聚合物材料的制备方法包括以下步骤：The preparation method of the OMSA polymer material includes the following steps:
S1、将适量单体添加至反应釜中，对单体进行加热熔化；S1. Add an appropriate amount of monomer to the reaction kettle, and heat and melt the monomer;
S2、将适量催化剂添加至反应釜中，使催化剂和熔融状态的单体进行混合；S2. Add an appropriate amount of catalyst into the reaction kettle to mix the catalyst and the molten monomer;
S3、将温度升高至375℃，使单体在催化剂的作用下进行缩聚反应；S3. Raise the temperature to 375°C to allow the monomer to undergo polycondensation reaction under the action of the catalyst;
S3、反应完成后，即可制得液态的OMSA高分子聚合物。S3. After the reaction is completed, the liquid OMSA polymer can be obtained.
请参阅图1，本申请中的OMSA高分子聚合物材料以尼龙66盐为单体、三氟化硼为催化剂，经熔融缩聚反应制备而成，其具有良好的力学性能、耐磨性、耐腐蚀性和耐高温性，特别适用于设备损坏处的修补、重塑与再造，弥补了OMSA高分子聚合物在这一应用领域的空白。Please refer to Figure 1. The OMSA polymer material in this application is prepared through melt polycondensation reaction using nylon 66 salt as the monomer and boron trifluoride as the catalyst. It has good mechanical properties, wear resistance, and Corrosion and high temperature resistance, it is especially suitable for repairing, reshaping and rebuilding damaged equipment, filling the gap of OMSA polymer in this application field.
请参阅图2-6，反应釜的釜体上设置有活气提效机构，活气提效机构包括推拉气缸101、活气筒102，活气筒102内设置有与之滑动密封连接的活塞板103，活塞板103的左端固定连接有连接杆104，连接杆104贯穿活气筒102左端的外壁并与之滑动连接，连接杆104的左端固定连接有保温隔热杆105，推拉气缸101的输出端上固定连接有联动板106，联动板106的底端与保温隔热杆105固定连接，活气筒102右端的外壁上贯穿嵌设有进气管107，进气管107的左端设置有与之相匹配的阻排塞108，阻排塞108和进气管107上下两侧的内壁之间均固定连接有弹性拉绳109，活气筒102的底端外壁上贯穿嵌设有排气管110，排气管110的底端处设置有与之滑动密封连接的阻进塞111，阻进塞111的顶端固定连接有竖杆112，竖杆112和排气管110左右两侧的内壁之间均固定连接有弹性吊绳113，推拉气缸101通过支撑板117固定安装在釜体的顶端，活气筒102位于釜体内，且活气筒102与釜体的顶端内壁固定连接，保温隔热杆105贯穿釜体的左侧外壁并与之滑动密封连接，且保温隔热杆105采用隔热保温材料制成，阻排塞108设置为左粗右细的圆台状，在本申请中，制备OMSA高分子聚合物材料时，所使用到的催化剂三氟化硼是一种气体，反应过程中，催化剂会和反应釜中的空气混合形成混合气体，单体被加热熔化后，步骤S3中，熔融状态的单体，在高温和催化剂的条件下进行缩聚反应的过程中，启动推拉气缸101，使推拉气缸101通过联动板106、保温隔热杆105、连接杆104向左拉动活塞板103，可产生一个吸力，在该吸力的作用下，阻排塞108会向左移动，致使进气管107导通，从而可将一定量的由空气和催化剂组成的混合气体，经进气管107抽吸至活气筒102中，活塞板103移动一定的距离后停止拉动，阻排塞108会在弹性拉绳109的作用下自动复位，然后控制推拉气缸101，使推拉气缸101向右推动活塞板103，直至活塞板103复位，在此过程中，阻进塞111会在气压的作用下向下移动，致使排气管110导通，然后活气筒102内的混合气体会经排气管110注入熔化的单体中，然后混合气体会以气泡的形式再从单体中逸出，混合气体中的催化剂可与单体充分接触，另外，活塞板103复位后，阻进塞111会在弹性吊绳113的作用下快速复位，重新将排气管110堵塞密封，多次重复上述操作，可大大提高催化剂与单体的接触面积，因此，通过活气提效机构的设置，使得活气提效机构可将处在单体上方、难以与单体充分接触的混合气体，导向熔化的单体，致使混合气体中的催化剂能与单体充分接触，结合反应釜的搅拌功能，可大大提高催化剂与单体的接触面积，能显著提高缩聚反应的反应效率，进而可有效提高生产效率。Please refer to Figure 2-6. The body of the reaction kettle is provided with a live gas efficiency improving mechanism. The live gas efficiency improving mechanism includes a push-pull cylinder 101 and a live gas cylinder 102. The live gas cylinder 102 is provided with a piston plate 103 connected with it in a sliding seal. The piston The left end of the plate 103 is fixedly connected with a connecting rod 104. The connecting rod 104 penetrates the outer wall of the left end of the activating cylinder 102 and is slidingly connected with it. The left end of the connecting rod 104 is fixedly connected with a thermal insulation rod 105, and the output end of the push-pull cylinder 101 is fixedly connected. There is a linkage plate 106, and the bottom end of the linkage plate 106 is fixedly connected to the thermal insulation rod 105. The outer wall of the right end of the active air cylinder 102 is embedded with an air inlet pipe 107, and the left end of the air inlet pipe 107 is provided with a matching blocking plug. 108. An elastic drawstring 109 is fixedly connected between the drain plug 108 and the inner walls of the upper and lower sides of the air inlet pipe 107. An exhaust pipe 110 is embedded in the outer wall of the bottom end of the air cylinder 102. The bottom end of the exhaust pipe 110 A blocking plug 111 is provided with a sliding and sealing connection therewith. A vertical rod 112 is fixedly connected to the top of the blocking plug 111. An elastic sling 113 is fixedly connected between the vertical rod 112 and the inner walls of the left and right sides of the exhaust pipe 110. , the push-pull cylinder 101 is fixedly installed on the top of the kettle body through the support plate 117, the activating air cylinder 102 is located in the kettle body, and the activating air cylinder 102 is fixedly connected to the top inner wall of the kettle body, and the thermal insulation rod 105 penetrates the left outer wall of the kettle body and is connected with the kettle body. The thermal insulation rod 105 is made of thermal insulation material, and the drainage plug 108 is set in a truncated cone shape with a thick left and a thin right. In this application, when preparing the OMSA polymer material, the The catalyst boron trifluoride is a gas. During the reaction, the catalyst will mix with the air in the reactor to form a mixed gas. After the monomer is heated and melted, in step S3, the molten monomer mixes with the catalyst at high temperature. During the polycondensation reaction under the conditions, the push-pull cylinder 101 is started to pull the piston plate 103 to the left through the linkage plate 106, the thermal insulation rod 105, and the connecting rod 104, which can generate a suction force. Under the action of the suction force, , the obstruction plug 108 will move to the left, causing the air inlet pipe 107 to open, so that a certain amount of mixed gas composed of air and catalyst can be sucked into the active air cylinder 102 through the air inlet pipe 107, and the piston plate 103 moves a certain amount Stop pulling after the distance, the blockage plug 108 will automatically reset under the action of the elastic pull cord 109, and then control the push-pull cylinder 101 to push the piston plate 103 to the right until the piston plate 103 is reset. In this process, the blockage The plug 111 will move downward under the action of air pressure, causing the exhaust pipe 110 to conduct, and then the mixed gas in the active gas cylinder 102 will be injected into the molten monomer through the exhaust pipe 110, and then the mixed gas will be in the form of bubbles Then escape from the monomer, the catalyst in the mixed gas can fully contact with the monomer. In addition, after the piston plate 103 is reset, the blocking plug 111 will be quickly reset under the action of the elastic sling 113, and the exhaust pipe 110 will be re-opened. Blocking and sealing, and repeating the above operation many times can greatly increase the contact area between the catalyst and the monomer. Therefore, through the setting of the active gas improvement mechanism, the active gas efficiency improvement mechanism can remove the areas above the monomer that are difficult to fully contact with the monomer. The mixed gas is directed to the molten monomer, so that the catalyst in the mixed gas can fully contact the monomer. Combined with the stirring function of the reactor, the contact area between the catalyst and the monomer can be greatly increased, and the reaction efficiency of the polycondensation reaction can be significantly improved. It can effectively improve production efficiency.
请参阅图5-6，竖杆112的顶端固定连接有与排气管110相匹配的防偏网114，防偏网114与排气管110滑动连接，防止阻进塞111偏离排气管110，阻进塞111的顶端设置为球面状，防止单体进入到排气管110内，排气管110左右两侧的内壁上均固定安装有阻升块116，阻升块116位于阻进塞111的上方，使得推拉气缸101向左拉动活塞板103时，阻进塞111不会向上移动，进气管107上下两侧的内壁上均固定安装有防偏块115，防偏块115的一端与阻排塞108相抵，且防偏块115与阻排塞108相抵的一端设置为与阻排塞108相匹配的形状，防止偏离进气管107，活气筒102、活塞板103、连接杆104、进气管107、阻排塞108等均采用耐高温材料制成。Please refer to Figure 5-6. The top of the vertical rod 112 is fixedly connected with an anti-deviation net 114 that matches the exhaust pipe 110. The anti-deviation net 114 is slidingly connected to the exhaust pipe 110 to prevent the blocking plug 111 from deviating from the exhaust pipe 110. , the top of the blocking plug 111 is set in a spherical shape to prevent the monomer from entering the exhaust pipe 110. The lifting blocking blocks 116 are fixedly installed on the inner walls of the left and right sides of the exhaust pipe 110, and the lifting blocking blocks 116 are located on the blocking plug. 111, so that when the push-pull cylinder 101 pulls the piston plate 103 to the left, the blocking plug 111 will not move upward. Anti-deviation blocks 115 are fixedly installed on the inner walls of the upper and lower sides of the intake pipe 107. One end of the anti-deviation block 115 is connected to The blocking plug 108 is offset, and the end of the anti-deviation block 115 that is against the blocking plug 108 is set in a shape that matches the blocking plug 108 to prevent deviation from the intake pipe 107, the air cylinder 102, the piston plate 103, the connecting rod 104, the inlet The trachea 107, the obstruction plug 108, etc. are all made of high temperature resistant materials.
第二种实施方式：Second implementation:
图7-9示出一种OMSA高分子聚合物材料，与第一种实施方式不同的是，活气提效机构还包括固定安装在釜体顶端的活气智控器002，活气智控器002中设置有触控面板、自动活气模块、周期设置模块、安全检密模块，触控面板与自动活气模块电连接，自动活气模块与推拉气缸101电连接，周期设置模块与自动活气模块电连接，缩聚反应开始后，相关工作人员可通过触控面板向自动活气模块下达指令，收到指令后，自动活气模块先是会控制推拉气缸101，使推拉气缸101向左拉动活塞板103，然后自动活气模块会控制推拉气缸101，使推拉气缸101向右推动活塞板103，且工作人员还可通过周期设置模块设置一个周期，致使自动活气模块每间隔一个周期的时间，便会执行一次上述操作，如此，使得工作人员无需手动去控制推拉气缸101，从而可提高活气提效机构的自动化、智能化程度。Figures 7-9 show an OMSA polymer material. Different from the first embodiment, the live gas efficiency improving mechanism also includes a live gas intelligent controller 002 fixedly installed on the top of the kettle body. The live gas intelligent controller 002 It is provided with a touch panel, an automatic vitality module, a period setting module, and a safety inspection module. The touch panel is electrically connected to the automatic vitality module, the automatic vitality module is electrically connected to the push-pull cylinder 101, and the period setting module is electrically connected to the automatic vitality module. After the reaction starts, the relevant staff can issue instructions to the automatic vitality module through the touch panel. After receiving the instruction, the automatic vitality module will first control the push-pull cylinder 101 to make the push-pull cylinder 101 pull the piston plate 103 to the left, and then the automatic vitality module will Control the push-pull cylinder 101 so that the push-pull cylinder 101 pushes the piston plate 103 to the right, and the staff can also set a cycle through the cycle setting module, so that the automatic live air module will perform the above operation once every interval, so that Workers do not need to manually control the push-pull cylinder 101, thereby improving the automation and intelligence of the live gas efficiency improvement mechanism.
请参阅图7-9，活气提效机构还包括安全检密组件，安全检密组件包括套设在保温隔热杆105上的安检密封盒301，安检密封盒301的顶端外壁上贯穿嵌设有密封筒302，密封筒302的顶端内壁上固定安装有电动伸缩杆303，电动伸缩杆303的输出端上固定连接有与密封筒302相匹配的推气板304，安检密封盒301的内壁上固定安装有气压传感器305，保温隔热杆105贯穿安检密封盒301并与之固定连接，安检密封盒301设置为与釜体相匹配的扇形状，安检密封盒301的一端与釜体的外壁紧密贴合并设置为开口状，推气板304与密封筒302滑动密封连接，密封筒302的底端设置为开口状，安全检密组件还包括固定安装在活气智控器002顶端的反馈灯306，活气智控器002中还设置有安全检密模块，触控面板与安全检密模块电连接，安全检密模块与电动伸缩杆303电连接，气压传感器305与安全检密模块电连接，安全检密模块与反馈灯306电连接，反馈灯306可发出红色和绿色两种颜色的灯光，由于保温隔热杆105会经常与釜体的外壁发生摩擦，时间一长，保温隔热杆105和釜体外壁连接处的密封性容易出现问题，需要及时发现并进行维护，在开始制备之前，工作人员可通过触控面板给安全检密模块下达检测指令，收到指令后，安全检密模块会启动电动伸缩杆303，使电动伸缩杆303带动推气板304向下移动一定的距离，推气板304下降至指定高度后，会在该位置停留一定的时间，一定时间后，安全检密模块会控制电动伸缩杆303，使电动伸缩杆303带动推气板304向上移动复位，推气板304向下移动时，会使安检密封盒301内的气压增大，气压传感器305可对安检密封盒301内部的气压进行检测，且检测数据会反馈给安全检密模块，在推气板304开始向下移动至推气板304向上移动复位之前的这段时间内，若保温隔热杆105与釜体外壁连接处的密封性良好，安检密封盒301内的空气将不会泄漏，安检密封盒301内的气压先是会持续增大，然后保持不变，反之，若保温隔热杆105与釜体外壁连接处的密封性存在问题，那么空气将会从缺陷处泄漏至反应釜内，安检密封盒301内的气压会先持续增大，然后会逐渐减小（如果密封性缺陷较大，安检密封盒301内的气压也有可能几乎不变），使得安全检密模块可通过分析气压传感器305所检测到的气压数据，判断出保温隔热杆105与釜体外壁连接处的密封性是否存在问题，若结果表明保温隔热杆105与釜体外壁连接处的密封性良好，安全检密模块会使反馈灯306发出绿色的灯光，若结果表明保温隔热杆105与釜体外壁连接处的密封性存在问题，安全检密模块则会使反馈灯306发出红色的灯光，如果工作人员观察到反馈灯306发出绿色的灯光，可直接关闭反馈灯306，然后开始制备OMSA高分子聚合物材料，如果工作人员观察到反馈灯306发出红色的灯光，则需要对保温隔热杆105与釜体外壁的连接处进行相应的维护，然后才能开始制备，因此，通过安全检密组件的设置，使得开始制备之前，安全检密组件可对保温隔热杆105和釜体外壁连接处进行密封性检测，防止因保温隔热杆105和釜体外壁连接处的密封性存在缺陷而产生安全事故，进而可大大提高活气提效机构的可靠性和安全性。Please refer to Figure 7-9. The live gas efficiency improvement mechanism also includes a safety inspection component. The safety inspection component includes a security seal box 301 set on the thermal insulation rod 105. The top outer wall of the security seal box 301 is embedded with a The sealing cylinder 302 has an electric telescopic rod 303 fixedly installed on the top inner wall of the sealing cylinder 302. The output end of the electric telescopic rod 303 is fixedly connected with a push plate 304 that matches the sealing cylinder 302. The inner wall of the security inspection sealing box 301 is fixed. An air pressure sensor 305 is installed, and the thermal insulation rod 105 penetrates the security sealing box 301 and is fixedly connected to it. The security sealing box 301 is set in a fan shape matching the kettle body, and one end of the security sealing box 301 is closely attached to the outer wall of the kettle body. The combination is set in an open shape. The air pushing plate 304 is connected with the sealing cylinder 302 in a sliding and sealing manner. The bottom end of the sealing cylinder 302 is set in an open shape. The safety inspection component also includes a feedback light 306 fixedly installed on the top of the living gas intelligent controller 002. The living gas The smart controller 002 is also provided with a safety inspection module. The touch panel is electrically connected to the safety inspection module. The safety inspection module is electrically connected to the electric telescopic rod 303. The air pressure sensor 305 is electrically connected to the safety inspection module. The safety inspection module is electrically connected. The module is electrically connected to the feedback light 306. The feedback light 306 can emit red and green lights. Since the thermal insulation rod 105 will often rub against the outer wall of the kettle body, over time, the thermal insulation rod 105 and the kettle body will be damaged. The sealing of the outer wall connection is prone to problems, which need to be discovered and maintained in time. Before starting preparation, the staff can give detection instructions to the safety inspection module through the touch panel. After receiving the instruction, the safety inspection module will start the electric motor. The telescopic rod 303 causes the electric telescopic rod 303 to drive the air pushing plate 304 to move downward a certain distance. After the air pushing plate 304 drops to a specified height, it will stay at this position for a certain period of time. After a certain period of time, the safety inspection module will control The electric telescopic rod 303 drives the air pushing plate 304 to move upward and reset. When the air pushing plate 304 moves downward, the air pressure in the security inspection sealed box 301 will increase. The air pressure sensor 305 can monitor the inside of the security inspection sealed box 301. The air pressure is detected, and the detection data will be fed back to the safety inspection module. During the period before the air pushing plate 304 starts to move downward and before the air pushing plate 304 moves upward to reset, if the thermal insulation rod 105 is in contact with the outer wall of the kettle The sealing of the connection is good, and the air in the security sealing box 301 will not leak. The air pressure in the security sealing box 301 will continue to increase first, and then remain unchanged. On the contrary, if the thermal insulation rod 105 is connected to the outer wall of the kettle If there is a problem with the sealing at the defect, air will leak into the reactor from the defect. The air pressure in the security seal box 301 will continue to increase first, and then gradually decrease (if the sealing defect is large, the air pressure in the security seal box 301 will The air pressure inside may also be almost unchanged), so that the safety inspection module can determine whether there is a problem with the sealing of the connection between the heat insulation rod 105 and the outer wall of the kettle by analyzing the air pressure data detected by the air pressure sensor 305. If the result It shows that the sealing between the thermal insulation rod 105 and the outer wall of the kettle is good. The safety inspection module will make the feedback light 306 emit green light. If the result shows that there is a problem with the sealing between the thermal insulation rod 105 and the outer wall of the kettle. , the security inspection module will cause the feedback light 306 to emit red light. If the staff observes that the feedback light 306 emits green light, the feedback light 306 can be directly turned off, and then the preparation of OMSA polymer material can be started. When the feedback light 306 emits red light, it is necessary to perform corresponding maintenance on the connection between the thermal insulation rod 105 and the outer wall of the kettle before preparation can be started. Therefore, through the setting of the safety inspection component, safety is ensured before starting preparation. The sealing component can detect the sealing of the connection between the thermal insulation rod 105 and the outer wall of the kettle to prevent safety accidents caused by defects in the sealing between the thermal insulation rod 105 and the outer wall of the kettle, thereby greatly improving the live gas lift. the reliability and safety of effective institutions.
请参阅图8，密封筒302的外壁上开设有通气孔307，通气孔307位于推气板304的上方，有利于推气板304的上、下移动。Please refer to Figure 8. A vent hole 307 is provided on the outer wall of the sealing cylinder 302. The vent hole 307 is located above the air pushing plate 304, which facilitates the upward and downward movement of the air pushing plate 304.
结合当前实际需求，本申请采用的上述实施方式，保护范围并不局限于此，在本领域技术人员所具备的知识范围内，不脱离本申请构思作出的各种变化，仍落在本发明的保护范围。In combination with the current actual needs, the protection scope of the above-mentioned embodiments adopted in this application is not limited thereto. Within the scope of knowledge possessed by those skilled in the art, various changes can be made without departing from the concept of this application, and still fall within the scope of the present invention. protected range.
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311629361.8ACN117603446A (en) | 2023-12-01 | 2023-12-01 | OMSA high-molecular polymer material |
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311629361.8ACN117603446A (en) | 2023-12-01 | 2023-12-01 | OMSA high-molecular polymer material |
| Publication Number | Publication Date |
|---|---|
| CN117603446Atrue CN117603446A (en) | 2024-02-27 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202311629361.8APendingCN117603446A (en) | 2023-12-01 | 2023-12-01 | OMSA high-molecular polymer material |
| Country | Link |
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| CN (1) | CN117603446A (en) |
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| Date | Code | Title | Description |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | Application publication date:20240227 | |
| RJ01 | Rejection of invention patent application after publication |