A kind of jelly film and preparation method thereofTechnical field
The invention belongs to daily use chemicals technical fields, and in particular to a kind of jelly film and preparation method thereof.
Background technique
The skin care item that jelly film, i.e. appearance are in g., jelly-like, it has also become a kind of novel skin skin care products increasingly risen has poleThe big market demand, there are still some the problem of can not avoiding for the jelly film product on existing market: on the one hand, although there is benefitThe product category declared in terms of water is various, but generally tends to effect in terms of instant moisturizing, and long-acting moisturizing effects are simultaneously unknownIt is aobvious, thus generally can only as facial mask within a certain period of time using and play a role, and be not suitable as the substitute of face cream.SeparatelyOn the one hand, existing jelly film use feeling is generally more greasy, also becomes urgent problem to be solved.
CN201610041060.7 discloses a kind of Wuji bamboo charcoal black frost film, specifically discloses including following component: water, sweetOil, propylene glycol, polyethylene glycol-400, polyvinyl alcohol, carbomer, elastin laminin, Cer EOS, polysorbate -20, bamboo charcoal,Triethanolamine, dipotassium glycyrrhizinate, polyvinylpyrrolidone, methyl hydroxybenzoate, Nipasol, Bis(hydroxymethyl)imidazolidinyl urea, perfume (or spice)Essence.The product adsorption capacity is strong, can siphon away blackhead, hoary hair and residual color make-up completely.But in moisturizing, whitening and desalination microgroovePerformance does not protrude in terms of these more urgent public demands.
CN201711230582.2 discloses a kind of jelly film surface film containing growth factor, specifically discloses including following componentAnd its parts by weight: 0.5~4 part of fibroin peptide, 1~6 part of hydrolysed rice albumen, 0.5~4 part of carnosine, macromolecular moisturizer 2~12 parts, 0.00005~0.001 part of recombinant human horny cell growth factor-2, recombinant human epidermal growth factor 0.00005~0.001 part, 0.01~1 part of diguanosine tetraphosphate, 0.1~1 part of allantoin, 30~50 parts of film forming agent, panthenyl triacetate 1~8Part, 1~2 part of Sensiva SC50 and 30~50 parts of water.The product have preferably moist moisturizing, anti-ageing wrinkle resistant, whitening spot-removing,Anti-anaphylaxis repairs effect, and property is mild, safely and effectively, to improvement skin quality significant effect.But the main still body of its moisturizing effectImmediately the effect in terms of moisturizing now, the effect in terms of long-acting moisturizing shows slightly insufficient, further, since addition is a large amount of in formulaFilm forming agent has been difficult to avoid that rubs mud phenomenon with the hands in use though use feeling can be made salubrious.
Summary of the invention
The purpose of the present invention is to provide a kind of jelly film, the jelly film collection is made with long-acting moisturizing effects, desalination microgroove immediatelyWith and whitening function in one and use salubrious non-greasy.
Another object of the present invention is to provide a kind of preparation method for freezing film, what the preparation method was preparedIt is high to freeze membrane stability, active constituent is retained.
The technical solution of the present invention is as follows:
A kind of jelly film, raw material components include:
Water 50-85 parts by weight, polyalcohol 14-21 parts by weight, active peptide 1.45-7.6 parts by weight, hyaluronic acid 0.05-0.3Parts by weight, niacinamide 1-4 parts by weight, collagen 0.3-1 parts by weight, aloe barbadensis Miller leaf juice 0.1-1.2 parts by weight, Radix Malvae sylvestrisFlower extract 0.1-1.2 parts by weight, peony extract 0.1-1.2 parts by weight, honeysuckle flower extract 0.1-1.2 parts by weight, german chamomileFlower extract 0.1-1.2 parts by weight, Europe dandelion extract 0.1-1.2 parts by weight, Herba Violae extract 0.1-1.2 weightPart, grape seed oil 0.1-1.2 parts by weight, sturgeon roe sauce extract 0.1-0.5 parts by weight, superoxide dismutase 0.05-0.2 weightMeasure part, carbomer 0.1-0.3 parts by weight, pH adjusting agent 0.1-0.2 parts by weight, decoyl hydroximic acid 0.2-0.6 parts by weight, ethyl hexylBase glycerol 0.1-0.5 parts by weight.
Further, the raw material components for freezing film include:
Water 60-70 parts by weight, polyalcohol 16-19 parts by weight, active peptide 3.2-5.6 parts by weight, hyaluronic acid 0.1-0.2 weightMeasure part, niacinamide 2-3 parts by weight, collagen 0.5-0.8 parts by weight, aloe barbadensis Miller leaf juice 0.5-1 parts by weight, Radix Malvae sylvestris flowerExtract 0.5-1 parts by weight, peony extract 0.5-1 parts by weight, honeysuckle flower extract 0.5-1 parts by weight, german chamomile flower extract0.5-1 parts by weight, Europe dandelion extract 0.5-1 parts by weight, Herba Violae extract 0.5-1 parts by weight, grape seed oil 0.5-1Parts by weight, sturgeon roe sauce extract 0.2-0.4 parts by weight, superoxide dismutase 0.1-0.18 parts by weight, carbomer 0.12-0.2 parts by weight, pH adjusting agent 0.12-0.18 parts by weight, decoyl hydroximic acid 0.3-0.5 parts by weight, Sensiva SC50 0.2-0.4Parts by weight.
Further, the raw material components for freezing film include:
70 parts by weight of water, 17.5 parts by weight of polyalcohol, 4.35 parts by weight of active peptide, 0.15 parts by weight of hyaluronic acid, nicotinoyl2.5 parts by weight of amine, 0.65 parts by weight of collagen, 0.8 parts by weight of aloe barbadensis Miller leaf juice, 0.8 weight of Radix Malvae sylvestris flower extractPart, 0.8 parts by weight of peony extract, 0.8 parts by weight of honeysuckle flower extract, 0.8 parts by weight of german chamomile flower extract, Europe dandelion mentionTake 0.8 parts by weight of object, 0.8 parts by weight of Herba Violae extract, 0.8 parts by weight of grape seed oil, 0.35 weight of sturgeon roe sauce extractMeasure part, 0.15 parts by weight of superoxide dismutase, 0.15 parts by weight of carbomer, 0.15 parts by weight of pH adjusting agent, decoyl hydroximic acid0.4 parts by weight, 0.3 parts by weight of Sensiva SC50.
Further, the active peptide is by glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, oligopeptides -2, oligopeptides -5, -1 copper of tripeptides composition.
Further, the glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, oligopeptides -2, oligopeptides -5,Weight ratio between -1 copper of tripeptides is 1-4:0.1-0.5:0.1-0.4:0.05-0.5:0.05-0.5:0.05-0.5:0.1-1.2.
Further, the collagen is Isin glue collagen and/or deer-bone collagenous albumen.
Further, the collagen is Isin glue collagen and deer-bone collagenous albumen by weight 0.1-0.5:0.2-The mixture of 0.5 composition.
Further, the polyalcohol is propylene glycol, glycerol, 1,2- hexylene glycol by weight 7-9:5-7:0.2-0.4 groupAt mixture.
Further, the mixing that the polyalcohol is propylene glycol, glycerol, 1,2- hexylene glycol are formed by weight 8:6:0.3Object.
The preparation method for freezing film, includes the following steps:
(1) carbomer is added into water, is heated to 80-85 DEG C while stirring with the mixing speed of 2000-3000r/min,10-20min is kept the temperature, A phase is obtained；
(2) polyalcohol, hyaluronic acid, grape seed oil, Sensiva SC50 are mixed evenly, obtain B phase；
(3) A phase being cooled to 55-70 DEG C, then sequentially adds B phase, niacinamide, collagen, stirring makes to be uniformly dispersed,Obtain C phase；
(4) C phase 40 DEG C are cooled to extract hereinafter, then sequentially adding active peptide, aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flowerObject, peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roeSauce extract, superoxide dismutase, decoyl hydroximic acid, pH adjusting agent stir evenly to get the jelly film.
Aloe barbadensis Miller leaf juice, aloe barbadensis Miller (Aloe vera (L.) Burm.f.) is Liliaceae aloe plant.ToolShort stem, uprightly without branch, blade is big and thickness, fleshiness succulence, narrow lanceolar, base portion are wealthy, and blade two arranges raw when plant children, grows upIt is afterwards then in rosette-stape.Leaf can be used as medicine, and have the function of heat-clearing, defaecation, desinsection, extract juice for having in cosmeticsWhitening, moisturizing promote wound healing and prevent the effect that skin is tanned severely and sunburn generates.
Radix Malvae sylvestris flower extract, can releive dry skin, form water lock film in skin surface, increase skin defense function,Skin moisture metabolism is simultaneously participated in, absorption of the skin to moisture is promoted.
Peony extract, from the root of cohosh Chinese herbaceous peony paeonia lactiflora pall..For making upAcne are treated in product, and delay the aging of body tissue.
Honeysuckle flower extract can be effectively improved scytitis, and enhancing skin resists the ability of bacterium, while promoting poreConvergence, keeps skin moist.
German chamomile flower extract, can balanced fat secretion, press down rouge anti-acne, prevent acne, eliminate blackspot, skin whitening, togetherWhen, there is certain inhibiting effect to skin pathogenicity fungi.
Europe dandelion extract can effectively remove ultra-oxygen anion free radical, inhibit the oxidation of unsaturated acids, have simultaneouslyThere is stronger inhibition tyrosinase, the generation and calmness of melanin can be reduced.
Herba Violae extract is Violaceae (Violaceae) plant northeast violet ViolamandshuricaW.Beck.Herb, esters of the herb containing glucoside, flavonoids, wax, cerinic acid (Ceroticacid) and unsaturated acids etc..Also the content of wax in spending, waxIn contain saturated acid (predominantly cerinic acid) 34.9%, unsaturated acids 5.8%, alcohols 10.3%, hydrocarbon about 47%.Root is starch-containing about37%, and have alkaloid, flavones reaction.Herb contains glucoside, flavonoids, wax (for the esters of cerinic acid and unsaturated acids etc.).ToolThere is clearing heat and detoxicating, cool blood detumescence.
Grape seed oil contains linolenic acid and proanthocyanidin.Linolenic acid can resist free radical, anti-aging, help to inhaleVitamin C and E are received, the elasticity of the circulatory system is strengthened, reduces the injury of ultraviolet light, protects the collagen in skin, is improved quietArteries and veins swelling and oedema prevent melanin deposition.Proanthocyanidin has protection blood vessel elasticity, protects skin afflicting with great suffering torment from ultraviolet light,The destruction for preventing collagenous fibres and elastomer makes skin keep due elasticity and tension, and skin sagging and wrinkle is avoided to produceIt is raw.Penetration is strong, and salubrious non-greasy is easily absorbed by the skin, and any skin quality is applicable in.
Sturgeon roe sauce extract, from the fish-egg of sturgeon, vitamin and mineral rich in can nourish skinSkin mitigates the cardinal symptom of skin aging, including pachylosis, microgroove, wrinkle, sagging and pigmentation, while having skinThe effect of moisturizing.It can also promote collagen synthesis, reduce protein cross (fibronectin), improve mitochondrial function in turnHelp to improve skin appearance from cell level, and mitigates the inflammation symptom around aging skin histocyte.
Superoxide dismutase is a kind of active material derived from life entity, can fight and block because oxygen radical is to thinIt is damaged caused by born of the same parents, and repairs damaged cell in time, to cell damage caused by restoring because of free radical, eliminate organism new oldThe harmful substance generated in metabolic process, thus have the function of anti-aging.
The invention has the benefit that
1, jelly film of the present invention is mentioned containing active peptide, collagen and including aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flowerTake object, peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeonA variety of natural plant extracts including sub- sauce extract, by the synergistic effect of these types of raw material, so that the jelly finally preparedFilm has stronger instant and long-acting moisturizing effects, thus both can be used as sleep mask, eye mask, lip film, cervacoria, hand film withMeet the needs repaired immediately, and may be used as bottoming before face cream, eye cream, restructuring compound for the neck, adornment to meet the needs of long-acting moisturizing.ThisOutside, jelly film of the present invention can remove the free radical being harmful to the human body, and reduce color spot, skin is allowed to become pale glossy.TogetherWhen by repair skin damaged cell, improve cell metabolism and have the function of significantly desalinating microgroove.Continuous use is originallyInvention is frozen film 28 days, skin can be made to shine naturally white, continued to use two months or more, microgroove can be made obviously to lighten, is thin out.
2, active peptide of the present invention by glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, oligopeptides -2,Oligopeptides -5, -1 copper of tripeptides are by weight 1-4:0.1-0.5:0.1-0.4:0.05-0.5:0.05-0.5:0.05-0.5:0.1-1.2Composition.The reason is that, present inventor is through a large number of experiments the study found that the active peptide of the specific composition, has optimalDesalinate microgroove effect, enables to microgroove naked eyes are visible lighten, is thin out, meanwhile, the specific proportion can significantly improve productWhole skin absorption rate so that the present invention freeze film compared with other existing products using salubriouser non-greasy.
Specific embodiment
Below by specific embodiment, the invention will be further described.
1g is represented in following embodiment with 1 parts by weight.
Embodiment 1
50 parts by weight of water, 14 parts by weight of polyalcohol, 1.45 parts by weight of active peptide, 0.05 parts by weight of hyaluronic acid, niacinamide 1Parts by weight, 0.3 parts by weight of collagen, 0.1 parts by weight of aloe barbadensis Miller leaf juice, 0.1 parts by weight of Radix Malvae sylvestris flower extract, Chinese herbaceous peony0.1 parts by weight of extract, 0.1 parts by weight of honeysuckle flower extract, 0.1 parts by weight of german chamomile flower extract, Europe dandelion extract 0.1Parts by weight, 0.1 parts by weight of Herba Violae extract, 0.1 parts by weight of grape seed oil, 0.1 parts by weight of sturgeon roe sauce extract, super oxygen0.05 parts by weight of compound mutase, 0.1 parts by weight of carbomer, 0.1 parts by weight of triethanolamine, 0.2 parts by weight of decoyl hydroximic acid, second0.1 parts by weight of base hexyl glycerol；The active peptide is glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, widowThe mixture that peptide -2, oligopeptides -5, -1 copper of tripeptides are formed by weight 1:0.1:0.1:0.05:0.05:0.05:0.1, the collagenAlbumen is the mixture that form by weight 0.1:0.2 of Isin glue collagen and deer-bone collagenous albumen, the polyalcohol be propylene glycol,The mixture that glycerol, 1,2- hexylene glycol are formed by weight 7:5:0.2.
Further, a kind of method preparing the jelly film is provided, is included the following steps:
(1) carbomer is added into water, is heated to 80 DEG C while stirring with the mixing speed of 2000r/min, heat preservation10min obtains A phase；
(2) polyalcohol, hyaluronic acid, grape seed oil, Sensiva SC50 are mixed evenly, obtain B phase；
(3) A phase is cooled to 55 DEG C, then sequentially adds B phase, niacinamide, collagen, stirring makes to be uniformly dispersed, obtainTo C phase；
(4) C phase is cooled to 40 DEG C, then sequentially add active peptide, aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flower extract,Peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roe sauce mentionObject, superoxide dismutase, decoyl hydroximic acid, triethanolamine are taken, is stirred evenly to get the jelly film.
Embodiment 2
The present embodiment provides a kind of jelly film, raw material components include:
85 parts by weight of water, 21 parts by weight of polyalcohol, 7.6 parts by weight of active peptide, 0.3 parts by weight of hyaluronic acid, 4 weight of niacinamideMeasure part, 1 parts by weight of collagen, 1.2 parts by weight of aloe barbadensis Miller leaf juice, 1.2 parts by weight of Radix Malvae sylvestris flower extract, Chinese herbaceous peony extraction1.2 parts by weight of object, 1.2 parts by weight of honeysuckle flower extract, 1.2 parts by weight of german chamomile flower extract, 1.2 weight of Europe dandelion extractPart, 1.2 parts by weight of Herba Violae extract, 1.2 parts by weight of grape seed oil, 0.5 parts by weight of sturgeon roe sauce extract, superoxides0.2 parts by weight of mutase, 0.3 parts by weight of carbomer, 0.2 parts by weight of triethanolamine, 0.6 parts by weight of decoyl hydroximic acid, ethyl hexyl0.5 parts by weight of base glycerol；The active peptide be glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, oligopeptides -2,The mixture that oligopeptides -5, -1 copper of tripeptides are formed by weight 4:0.5:0.4:0.5:0.5:0.5:1.2, the collagen are fishThe mixture that collagen and deer-bone collagenous albumen are formed by weight 0.5:0.5, the polyalcohol be propylene glycol, glycerol, 1,The mixture that 2- hexylene glycol is formed by weight 9:7:0.4.
Further, a kind of method preparing the jelly film is provided, is included the following steps:
(1) carbomer is added into water, is heated to 85 DEG C while stirring with the mixing speed of 3000r/min, heat preservation20min obtains A phase；
(2) polyalcohol, hyaluronic acid, grape seed oil, Sensiva SC50 are mixed evenly, obtain B phase；
(3) A phase is cooled to 70 DEG C, then sequentially adds B phase, niacinamide, collagen, stirring makes to be uniformly dispersed, obtainTo C phase；
(4) C phase is cooled to 35 DEG C, then sequentially add active peptide, aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flower extract,Peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roe sauce mentionObject, superoxide dismutase, decoyl hydroximic acid, triethanolamine are taken, is stirred evenly to get the jelly film.
Embodiment 3
The present embodiment provides a kind of jelly film, raw material components include:
60 parts by weight of water, 16 parts by weight of polyalcohol, 3.2 parts by weight of active peptide, 0.1 parts by weight of hyaluronic acid, 2 weight of niacinamideAmount part, 0.5 parts by weight of collagen, 0.5 parts by weight of aloe barbadensis Miller leaf juice, 0.5 parts by weight of Radix Malvae sylvestris flower extract, Chinese herbaceous peony mentionTake 0.5 parts by weight of object, 0.5 parts by weight of honeysuckle flower extract, 0.5 parts by weight of german chamomile flower extract, 0.5 weight of Europe dandelion extractMeasure part, 0.5 parts by weight of Herba Violae extract, 0.5 parts by weight of grape seed oil, 0.2 parts by weight of sturgeon roe sauce extract, super oxygen0.1 parts by weight of object mutase, 0.12 parts by weight of carbomer, 0.12 parts by weight of triethanolamine, 0.3 parts by weight of decoyl hydroximic acid, second0.2 parts by weight of base hexyl glycerol；The active peptide is glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, widowThe mixture that peptide -2, oligopeptides -5, -1 copper of tripeptides are formed by weight 3:0.2:0.2:0.4:0.4:0.4:1.1, the collagen eggWhite mixture form by weight 0.3:0.4 for Isin glue collagen and deer-bone collagenous albumen, the polyalcohol is propylene glycol, sweetThe mixture that oil, 1,2- hexylene glycol are formed by weight 8:6:0.3.
Further, a kind of method preparing the jelly film is provided, is included the following steps:
(1) carbomer is added into water, is heated to 80 DEG C while stirring with the mixing speed of 2500r/min, heat preservation15min obtains A phase；
(2) polyalcohol, hyaluronic acid, grape seed oil, Sensiva SC50 are mixed evenly, obtain B phase；
(3) A phase is cooled to 60 DEG C, then sequentially adds B phase, niacinamide, collagen, stirring makes to be uniformly dispersed, obtainTo C phase；
(4) C phase is cooled to 30 DEG C, then sequentially add active peptide, aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flower extract,Peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roe sauce mentionObject, superoxide dismutase, decoyl hydroximic acid, triethanolamine are taken, is stirred evenly to get the jelly film.
Embodiment 4
The present embodiment provides a kind of jelly film, raw material components include:
70 parts by weight of water, 19 parts by weight of polyalcohol, 5.6 parts by weight of active peptide, 0.2 parts by weight of hyaluronic acid, 3 weight of niacinamideMeasure part, 0.8 parts by weight of collagen, 1 parts by weight of aloe barbadensis Miller leaf juice, 1 parts by weight of Radix Malvae sylvestris flower extract, peony extractIt is 1 parts by weight, 1 parts by weight of honeysuckle flower extract, 1 parts by weight of german chamomile flower extract, 1 parts by weight of Europe dandelion extract, pale reddish brown1 parts by weight of fourth extract, 1 parts by weight of grape seed oil, 0.4 parts by weight of sturgeon roe sauce extract, 0.18 weight of superoxide dismutaseMeasure part, 0.2 parts by weight of carbomer, 0.18 parts by weight of pH adjusting agent, 0.5 parts by weight of decoyl hydroximic acid, 0.4 weight of Sensiva SC50Measure part；The active peptide is glutathione, Argireline, acetyl group tetrapeptide -5, oligopeptides -1, oligopeptides -2, oligopeptides -5, threeThe mixture that -1 copper of peptide is formed by weight 2:0.3:0.2:0.3:0.5:0.4:0.6, the collagen are Isin glue collagenThe mixture formed with deer-bone collagenous albumen by weight 0.3:0.2, the polyalcohol are propylene glycol, glycerol, 1,2- hexylene glycolBy weight the mixture of 8:6:0.3 composition.
Further, a kind of method preparing the jelly film is provided, is included the following steps:
(1) carbomer is added into water, is heated to 80 DEG C while stirring with the mixing speed of 2500r/min, heat preservation15min obtains A phase；
(2) polyalcohol, hyaluronic acid, grape seed oil, Sensiva SC50 are mixed evenly, obtain B phase；
(3) A phase is cooled to 65 DEG C, then sequentially adds B phase, niacinamide, collagen, stirring makes to be uniformly dispersed, obtainTo C phase；
(4) C phase is cooled to 30 DEG C, then sequentially add active peptide, aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flower extract,Peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roe sauce mentionObject, superoxide dismutase, decoyl hydroximic acid, triethanolamine are taken, is stirred evenly to get the jelly film.
Embodiment 5
The present embodiment provides a kind of jelly film, raw material components include:
70 parts by weight of water, 17.5 parts by weight of polyalcohol, 4.35 parts by weight of active peptide, 0.15 parts by weight of hyaluronic acid, nicotinoyl2.5 parts by weight of amine, 0.65 parts by weight of collagen, 0.8 parts by weight of aloe barbadensis Miller leaf juice, 0.8 weight of Radix Malvae sylvestris flower extractPart, 0.8 parts by weight of peony extract, 0.8 parts by weight of honeysuckle flower extract, 0.8 parts by weight of german chamomile flower extract, Europe dandelion mentionTake 0.8 parts by weight of object, 0.8 parts by weight of Herba Violae extract, 0.8 parts by weight of grape seed oil, 0.35 weight of sturgeon roe sauce extractMeasure part, 0.15 parts by weight of superoxide dismutase, 0.15 parts by weight of carbomer, 0.15 parts by weight of pH adjusting agent, decoyl hydroximic acid0.4 parts by weight, 0.3 parts by weight of Sensiva SC50；The active peptide is glutathione, Argireline, acetyl group tetrapeptide-5, the mixing that oligopeptides -1, oligopeptides -2, oligopeptides -5, -1 copper of tripeptides are formed by weight 1:0.3:0.3:0.08:0.08:0.08:0.7Object, the collagen is the mixture that Isin glue collagen and deer-bone collagenous albumen are formed by weight 0.2:0.5, described polynaryThe mixture that alcohol is propylene glycol, glycerol, 1,2- hexylene glycol are formed by weight 8:6:0.3.
Further, a kind of method preparing the jelly film is provided, is included the following steps:
(1) carbomer is added into water, is heated to 80 DEG C while stirring with the mixing speed of 2500r/min, heat preservation15min obtains A phase；
(2) polyalcohol, hyaluronic acid, grape seed oil, Sensiva SC50 are mixed evenly, obtain B phase；
(3) A phase is cooled to 60 DEG C, then sequentially adds B phase, niacinamide, collagen, stirring makes to be uniformly dispersed, obtainTo C phase；
(4) C phase is cooled to 30 DEG C, then sequentially add active peptide, aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flower extract,Peony extract, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roe sauce mentionObject, superoxide dismutase, decoyl hydroximic acid, triethanolamine are taken, is stirred evenly to get the jelly film.
Comparative example 1
Difference with embodiment 5, which is only that, removes active peptide.
Comparative example 2
Difference with embodiment 5 is only that remove and extract including aloe barbadensis Miller leaf juice, Radix Malvae sylvestris flower extract, Chinese herbaceous peonyIncluding object, honeysuckle flower extract, german chamomile flower extract, Europe dandelion extract, Herba Violae extract, sturgeon roe sauce extractNatural plant extracts.
Comparative example 3
Difference with embodiment 5, which is only that, removes collagen.
Efficacy assessments test
One, moistening effect evaluation test
1, test specimen: 1~3 sample of Examples 1 to 5 and comparative example.
2, testing standard: QB/T4256-2001 cosmetics moisture-keeping efficacy evaluation guide
3, test equipment: the skin elasticity Cotometer of German Courage+Khazaka company (German CK company) manufactureMPA580 host, skin moisture content Cornemeter CM825 test probe.
4, test process: 26 ages of selection, men and women was fifty-fifty, health, people's conduct of no skin disease at 20-35 years oldSubject.Subject cleans both hands forearm with unified cleaning products, while in the region both hands inner forearm 5 × 5cm of label,Adaptability is sat quietly 30min in the constant environment that temperature is 20 ± 1 DEG C, humidity is 50 ± 10%, and skin is made to be in stable stateAfterwards, the initial hydrauture of skin is measured, test specimen is uniformly then applied to marked region, smearing dosage is (2.0 ± 0.1)mg/cm2, skin hydration degree state is measured respectively at 0.5h, 2h, 8h later, evaluation result is indicated with hydrauture average value, is tiedFruit is shown in Table 1.
1 skin hydration degree test result of table
As can be seen that as time went on, skin hydration degree is on a declining curve, in 0.5h, embodiment and comparative exampleSkin hydration degree difference is little, but as time went on, and comparative example hydrauture downward trend is more significant, illustrate comparative example andEmbodiment is in terms of instant moistening effect and no significant difference, but significant difference in terms of long-acting moistening effect, length of the inventionEffect moistening effect is substantially better than comparative example.
Two, desalination microgroove effect assessment test
1, test specimen: 1~3 sample of Examples 1 to 5 and comparative example.
2, test equipment: the skin elasticity Cotometer of German Courage+Khazaka company (German CK company) manufactureMPA580 host, skin elasticity PVM600 test probe.
3, test process: subject of 30 ages of selection at 35-50 years old, men and women are fifty-fifty.Subject is selected into standard: canthusThere are the visible microgroove of naked eyes, health, no skin allergy history.Subject cleans face using unified facial cleanser, in right and left eyesAngle symmetric position marks the region 3cm × 3cm as test area, test badge region elasticity number, then respectively at marked regionTest specimen is smeared, smearing dosage is (2.0 ± 0.1) mg/cm2, it is sooner or later each to smear once, it is continuous to smear 28 days.Respectively at the 0thIts (smear for the first time before) and the 28th day detection test area elastic stage, evaluation result indicate with elasticity number average value, as a resultIt is shown in Table 2.
2 skin elasticity test result of table
| Elasticity indexes | Skin elasticity growth rate |
| Blank value | 0.57 | -- |
| Embodiment 1 | 0.76 | 33.33% |
| Embodiment 2 | 0.79 | 38.60% |
| Embodiment 3 | 0.83 | 45.61% |
| Embodiment 4 | 0.80 | 40.35% |
| Embodiment 5 | 0.85 | 49.12% |
| Comparative example 1 | 0.63 | 10.53% |
| Comparative example 2 | 0.69 | 21.05% |
| Comparative example 3 | 0.72 | 26.32% |
As can be seen that continuous use test specimen 28 days, subject canthus skin elasticity value is obviously improved, and realExample is applied better than comparative example, illustrates that the present invention can increase canthus elasticity of skin, plays the role of desalinating microgroove, further, comparisonThe skin elasticity growth rate of example 1 is significantly lower than other comparative examples and experimental example, illustrates the active peptide pair of special ratios of the present inventionIt is significant to desalinate microgroove influential effect.
Three, sensory evaluation
Female test person of 270 ages at 20-35 years old is randomly choosed, is equally divided into 9 groups, every group of 30 people, each group is distinguishedUsing Examples 1 to 5, comparative example 1~3 and commercially available jelly film (Ou Shiman pearl water oxygen shining adopt good night freezes film), application method isFace is uniformly smeared after face cleaning, is washed away after 20min, and all experimenters use salubrious degree, infiltration rate, comfort, thorn to productSwashing property and carries out satisfaction scoring, above each scoring item full marks 25 divide, and satisfaction is higher, and score value is higher, and appraisal result is averaged,It the results are shown in Table 3.
3 sensory evaluation satisfaction appraisal result of table
The result shows that user experience of the present invention in terms of salubrious degree and infiltration rate is substantially better than comparative example and commercially available productionProduct, further according to the analysis, the specific proportion active peptide of the present invention can significantly improve the skin absorption rate of product entirety, so thatThe present invention freeze film compared with other existing products using salubriouser non-greasy.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, anyThose familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all containLid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.