A kind of papermaking-method reconstituted tobaccos preparation methodTechnical field
The present invention relates to a kind of papermaking-method reconstituted tobaccos preparation methods, belong to papermaking-method reconstituted tobaccos technical field.
Background technique
Papermaking-method reconstituted tobaccos are a kind of raw materials in production of cigarettes, and preparation process mainly includes extracting, being beaten, manufacture paper with pulp intoType, wet end squeezing, drying, coating, rewinding, cutting etc..All the time, it is low to always exist fragrance level for papermaking-method reconstituted tobaccos,The problems such as miscellaneous gas is big, irritation weight, resist processing is low causes the use in cigarette composition to be restricted.
Summary of the invention
Present invention solves the technical problem that being to provide a kind of papermaking-method reconstituted tobaccos preparation method, which is directed to paper processReconstituted tobacco total sugar content is low, and humid keeping performance is poor, the not strong disadvantage of resist processing, carries out physical and chemical index to reconstituted tobacco and changesInto.
Further, the present invention also starts with from coating fluid constituent, improves bad present in papermaking-method reconstituted tobaccosBreath improves physical property, promotes papermaking-method reconstituted tobaccos pipe tobacco aesthetic quality and the compatibility with traditional pipe tobacco.
In order to solve the above technical problems, the technical solution adopted by the present invention are as follows:
A kind of papermaking-method reconstituted tobaccos preparation method, comprising the following steps: over dry slurry is taken, successively extract, be beaten,It manufactures paper with pulp molding, wet end squeezing, drying, coating, rewinding and dicing process；Specifically comprise the following steps:
S01, the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank are heated to 80-120 DEG C, and isothermal holding is simultaneouslyIt leaves and takes spare；
S02, is added a certain amount of polyhydroxy plant amylum in heating tank, and the dosage of polyhydroxy plant amylum is over dry slurry10-15%, keep the temperature 45-60min；After the completion of heat preservation, punching slurry plain boiled water is obtained；
Head box is added in the slurry plain boiled water that rushes of above-mentioned addition polyhydroxy plant amylum by S03；
S04, the slurry mix come out by head box is dried after wet end squeezing step dehydration to baking step, after dryingUp to piece cigarette, subsequently into application step；
The polyhydroxy plant amylum includes ganoderma lucidum polysaccharide and astragalus polyose.
The application step specifically comprises the following steps:
S05 takes appropriate piece cigarette, and at least 2h is balanced in climatic chamber, and the temperature of the climatic chamber is 20~30DEG C, humidity is 50~60%；
S06, the piece cigarette after balance are sieved after pulverization process, and mesh size is 100~120 mesh, obtain piece tobacco powder end；
S07 takes 3~5% tobacco powder ends, 1% carboxymethyl cellulose, 0.5% cigarette fumet B, 0.5% cigarette to be changed with pleasant impressionKind agent C, surplus are original production coating fluid A, form coating fluid after mixing；By coating fluid even application to blank chip base.
The addition point of the coating fluid is located in coating fluid concentration tank.
The spreading rate of the coating fluid is 37-39%.
In S03, the rate that head box is added in punching slurry plain boiled water is 10~30mL/min.
The original production is the concentrate of tobacco extraction liquid with coating fluid A.
The blank chip base the preparation method comprises the following steps: the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank heatingTo 80-120 DEG C, 45-60min is kept the temperature；After the completion of heat preservation, blank punching slurry plain boiled water is obtained；Above-mentioned blank is rushed into slurry plain boiled water, stream is addedStarch case；The slurry mix come out by head box is dried after wet end squeezing step dehydration to baking step, is had leisure after dryingWhite tiles base.
The ganoderma lucidum polysaccharide and the preparation method of astragalus polyose are the following steps are included: take the appropriate dry ganoderma lucidum medicine to constant weightThe quality of material and Milkvetch Root, ganoderma lucidum medicinal material and Milkvetch Root is 1:(2~3), medicinal material dry powder is obtained after common crushing, medicinal material is donePowder is extracted 3~5 times with 10~20% alcohol heat reflux, and each extraction time is 1~2h, and combined extract is concentrated under reduced pressure backReceive solution, be concentrated into concentrate weight be medicinal material dry powder 1/4~1/2 after, stop concentration, room temperature filters after cooling, filtrate95% ethyl alcohol of middle addition carries out alcohol precipitation operation, and the additional amount of 95% ethyl alcohol is 7~10 times of amounts of filtrate, and 95% ethyl alcohol side edged stirsIt mixes, after 95% ethyl alcohol adds, is filtered after standing at least 10h, filter residue is polysaccharide component, and polysaccharide component adds deionized water multipleMolten, the additional amount of deionized water is 10~20 times of amounts of polysaccharide component, adds and is equivalent to polysaccharide component weight 15~30%Acticarbon, after magnetic agitation at least 2h, filtering, up to ganoderma lucidum polysaccharide and astragalus polyose after filtrate is dry.
The present invention starts with from improvement papermaking-method reconstituted tobaccos physics and chemical quality, by forming step and the painting of manufacturing paper with pulpCloth step is added tobacco business and permits the chemical substance used, external quality in reconstituted tobacco is promoted, to reach from organoleptic qualityWith purpose more close with tobacco leaf in physical aspect.
Compared with traditional paper process is in reconstituted tobacco technique, the slave additive of the invention adds point and addsDosage sets out, and targetedly reduces bad breath present in papermaking-method reconstituted tobaccos, improves physical property, promotes paper processReconstituted tobacco pipe tobacco aesthetic quality, humectation and the compatibility with traditional pipe tobacco.
Certain carboxymethyl is added by adding certain proportion piece tobacco powder end in coating fluid in method of the invention whereinCellulose (CMC) is effectively improved papermaking-method reconstituted tobaccos aesthetic quality while improving nicotine content, and CMC on the one hand canIt avoids bringing impurity breath not pleasant in flue gas, on the one hand can play gluing coupling.
Specific embodiment
For clearer description the object, technical solutions and advantages of the present invention, below present invention is described, retouchedThe embodiment stated is a part of the embodiments of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, abilityDomain those of ordinary skill every other embodiment obtained without making creative work, belongs to the present inventionThe range of protection.
Embodiment 1
A kind of papermaking-method reconstituted tobaccos preparation method, comprising the following steps: over dry slurry is taken, successively extract, be beaten,It manufactures paper with pulp molding, wet end squeezing, drying, coating, rewinding and dicing process；Specifically comprise the following steps:
S01, the plain boiled water 1L for taking appropriate wet end squeezing step cycle to use, heating tank are heated to 100 DEG C, and isothermal holding simultaneously staysIt takes spare；
100g polyhydroxy plant amylum is added in heating tank, is dissolved in above-mentioned plain boiled water by S02, keeps the temperature 45min, makes its portionDivide hydrolysis；After the completion of heat preservation, punching slurry plain boiled water is obtained；
Head box is added in the slurry plain boiled water that rushes of above-mentioned addition polyhydroxy plant amylum by S03；
S04, the slurry mix come out by head box is dried after wet end squeezing step dehydration to baking step, after dryingUp to piece cigarette, subsequently into application step；
The polyhydroxy plant amylum includes ganoderma lucidum polysaccharide and astragalus polyose.
The application step specifically comprises the following steps:
S05 takes 3g piece cigarette, 2h is balanced in climatic chamber, the temperature of the climatic chamber is 22 DEG C, and humidity is60%；
S06, the piece cigarette after balance are sieved after pulverization process, and mesh size is 120 mesh, obtain piece tobacco powder end；
S07 takes 3g piece tobacco powder end, 1g carboxymethyl cellulose, 0.5g cigarette fumet B, 0.5g cigarette pleasant impression improver C,Mentioned component is dissolved in 32g original production coating fluid A, coating fluid is formed after mixing, by coating fluid even application to wherein01 sample is made in a 100g blank chip base.
The addition point of the coating fluid is located in coating fluid concentration tank.
The spreading rate of the coating fluid is 37%.
In S03, the rate that head box is added in punching slurry plain boiled water is 10mL/min.
The original production specific ingredient of coating fluid A are as follows: the concentrate of tobacco extraction liquid.
The blank chip base the preparation method comprises the following steps: the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank heatingTo 100 DEG C, 45min is kept the temperature；After the completion of heat preservation, blank punching slurry plain boiled water is obtained；Above-mentioned blank is rushed into slurry plain boiled water, head box is added；ByThe slurry mix that head box comes out is dried after wet end squeezing step dehydration to baking step, up to blank chip base after drying.
The ganoderma lucidum polysaccharide and the preparation method of astragalus polyose are the following steps are included: take the appropriate dry ganoderma lucidum medicine to constant weightThe quality of material and Milkvetch Root, ganoderma lucidum medicinal material and Milkvetch Root be 1:2~, it is common crush after medicinal material dry powder, by medicinal material dry powderIt is extracted 3 times with 10% alcohol heat reflux, each extraction time is 1h, and combined extract is concentrated under reduced pressure recycling solution, is concentrated intoAfter the weight of concentrate is the 1/4 of medicinal material dry powder, stop concentration, room temperature filters after cooling, and the progress of 95% ethyl alcohol is added in filtrateAlcohol precipitation operation, the additional amount of 95% ethyl alcohol are 7 times of amounts of filtrate, and 95% ethyl alcohol is stirring while adding, after 95% ethyl alcohol adds,Filtered after standing 10h, filter residue is polysaccharide component, and polysaccharide component adds deionized water to redissolve, the additional amount of deionized water be polysaccharide atPoint 10 times of amounts, add the acticarbon for being equivalent to polysaccharide component weight 15%, after magnetic agitation at least 2h, filtering,Up to ganoderma lucidum polysaccharide and astragalus polyose after filtrate is dry.
Embodiment 2
A kind of papermaking-method reconstituted tobaccos preparation method, comprising the following steps: over dry slurry is taken, successively extract, be beaten,It manufactures paper with pulp molding, wet end squeezing, drying, coating, rewinding and dicing process；Specifically comprise the following steps:
S01, the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank are heated to 80 DEG C, and isothermal holding is simultaneously left and takenIt is spare；
150g polyhydroxy plant amylum is added in S02 in heating tank, keeps the temperature 60min；After the completion of heat preservation, it is white to obtain punching slurryWater；
Head box is added in the slurry plain boiled water that rushes of above-mentioned addition polyhydroxy plant amylum by S03；
S04, the slurry mix come out by head box is dried after wet end squeezing step dehydration to baking step, after dryingUp to piece cigarette, subsequently into application step；
The polyhydroxy plant amylum includes ganoderma lucidum polysaccharide and astragalus polyose.
The application step specifically comprises the following steps:
S05 takes 5g piece cigarette, 3h is balanced in climatic chamber, the temperature of the climatic chamber is 30 DEG C, and humidity is50%；
S06, the piece cigarette after balance are sieved after pulverization process, and mesh size is 100 mesh, obtain piece tobacco powder end；
S07 takes 5g piece tobacco powder end, 1g carboxymethyl cellulose, 0.5g cigarette fumet B, 0.5% cigarette pleasant impression improver C,Mentioned component is dissolved in 32g original production coating fluid A, forms coating fluid after mixing, by coating fluid even application to another02 sample is made in piece 100g blank chip base.
The addition point of the coating fluid is located in coating fluid concentration tank.
The spreading rate of the coating fluid is 39%.
In S03, the rate that head box is added in punching slurry plain boiled water is 30mL/min.
The original production specific ingredient of coating fluid A are as follows: the concentrate of tobacco extraction liquid.
The blank chip base the preparation method comprises the following steps: the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank heatingTo 80 DEG C, 60min is kept the temperature；After the completion of heat preservation, blank punching slurry plain boiled water is obtained；Above-mentioned blank is rushed into slurry plain boiled water, head box is added；ByThe slurry mix that head box comes out is dried after wet end squeezing step dehydration to baking step, up to blank chip base after drying.
The ganoderma lucidum polysaccharide and the preparation method of astragalus polyose are the following steps are included: take the appropriate dry ganoderma lucidum medicine to constant weightThe quality of material and Milkvetch Root, ganoderma lucidum medicinal material and Milkvetch Root is 1:3, obtains medicinal material dry powder after common crushing, medicinal material dry powder is used20% alcohol heat reflux extracts 5 times, and each extraction time is 2h, and combined extract is concentrated under reduced pressure recycling solution, is concentrated into denseAfter the weight of contracting liquid is the 1/2 of medicinal material dry powder, stop concentration, room temperature filters after cooling, and 95% ethyl alcohol is added in filtrate and carries out alcoholHeavy operation, the additional amount of 95% ethyl alcohol are 10 times of amounts of filtrate, and 95% ethyl alcohol is stirring while adding, after 95% ethyl alcohol adds,Filtered after standing 14h, filter residue is polysaccharide component, and polysaccharide component adds deionized water to redissolve, the additional amount of deionized water be polysaccharide atPoint 20 times of amounts, add the acticarbon for being equivalent to polysaccharide component weight 30%, after magnetic agitation 3h, filtering, filtrateUp to ganoderma lucidum polysaccharide and astragalus polyose after drying.
Embodiment 3
A kind of papermaking-method reconstituted tobaccos preparation method, comprising the following steps: over dry slurry is taken, successively extract, be beaten,It manufactures paper with pulp molding, wet end squeezing, drying, coating, rewinding and dicing process；Specifically comprise the following steps:
S01, the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank are heated to 120 DEG C, and isothermal holding is simultaneously left and takenIt is spare；
130g polyhydroxy plant amylum is added in S02 in heating tank, keeps the temperature 50min；After the completion of heat preservation, it is white to obtain punching slurryWater；
Head box is added in the slurry plain boiled water that rushes of above-mentioned addition polyhydroxy plant amylum by S03；
S04, the slurry mix come out by head box is dried after wet end squeezing step dehydration to baking step, after dryingUp to piece cigarette, subsequently into application step；
The polyhydroxy plant amylum includes ganoderma lucidum polysaccharide and astragalus polyose.
The application step specifically comprises the following steps:
S05 takes 5g piece cigarette, 4h is balanced in climatic chamber, the temperature of the climatic chamber is 20 DEG C, and humidity is55%；
S06, the piece cigarette after balance are sieved after pulverization process, and mesh size is 120 mesh, obtain piece tobacco powder end；
S07 takes 5g piece tobacco powder end, 1g carboxymethyl cellulose, 0.5g cigarette fumet B, 0.5% cigarette pleasant impression improver C,Mentioned component is dissolved in 32g original production coating fluid A, forms coating fluid after mixing, by coating fluid even application to another03 sample is made in piece 100g blank chip base.
The addition point of the coating fluid is located in coating fluid concentration tank.
The spreading rate of the coating fluid is 39%.
In S03, the rate that head box is added in punching slurry plain boiled water is 20mL/min.
The original production specific ingredient of coating fluid A are as follows: the concentrate of tobacco extraction liquid.
The blank chip base the preparation method comprises the following steps: the plain boiled water for taking appropriate wet end squeezing step cycle to use, heating tank heatingTo 120 DEG C, 50min is kept the temperature；After the completion of heat preservation, blank punching slurry plain boiled water is obtained；Above-mentioned blank is rushed into slurry plain boiled water, head box is added；ByThe slurry mix that head box comes out is dried after wet end squeezing step dehydration to baking step, up to blank chip base after drying.
The ganoderma lucidum polysaccharide and the preparation method of astragalus polyose are the following steps are included: take the appropriate dry ganoderma lucidum medicine to constant weightThe quality of material and Milkvetch Root, ganoderma lucidum medicinal material and Milkvetch Root is 1:3, obtains medicinal material dry powder after common crushing, medicinal material dry powder is used15% alcohol heat reflux extracts 4 times, and each extraction time is 1.5h, and combined extract is concentrated under reduced pressure recycling solution, is concentrated intoAfter the weight of concentrate is the 1/2 of medicinal material dry powder, stop concentration, room temperature filters after cooling, and the progress of 95% ethyl alcohol is added in filtrateAlcohol precipitation operation, the additional amount of 95% ethyl alcohol are 8 times of amounts of filtrate, and 95% ethyl alcohol is stirring while adding, after 95% ethyl alcohol adds,Filtered after standing 20h, filter residue is polysaccharide component, and polysaccharide component adds deionized water to redissolve, the additional amount of deionized water be polysaccharide atPoint 15 times of amounts, add the acticarbon for being equivalent to polysaccharide component weight 20%, after magnetic agitation 4h, filtering, filtrateUp to ganoderma lucidum polysaccharide and astragalus polyose after drying.
01 sample stimulus of papermaking-method reconstituted tobaccos of discovery above method preparation after professional tobacco sense organ judging panel evaluationDeclined, micro- to have miscellaneous gas, wooden breath is more prominent, and the declines such as 02 sample stimulus and xylon gas are obvious, improvement compared with01 sample is more preferable, more closely, 03 sample perfume quantity is prominent, aroma quality is richer for aesthetic quality and tobacco leaf.It mixes and matches in the tobaccoUniformity testing result see the table below 1.The proximate analysis of papermaking-method reconstituted tobaccos sample chemical, which is made, in this method the results are shown in Table 2.
The blending uniformity testing result in the tobacco of table 1
Mixing situation of the reconstituted tobacco silk in cut tobacco, seen from table 1,01,02 and 03 are characterized using uniformity coefficientMixing uniformity of the sample in cut tobacco is apparently higher than common reconstituted tobacco, and the reconstituted tobacco for showing that this method is prepared existsIn physical behavior, with cut tobacco more closely, so as to be preferably uniformly mixed with the cut tobacco in cigarette composition.
Papermaking-method reconstituted tobaccos sample chemical proximate analysis result is made in 2 this method of table
As can be seen from Table 2, the papermaking-method reconstituted tobaccos after the method improvement of the present embodiment, total sugar content and nicotine content are equalIt significantly improves, can reduce bad breath present in papermaking-method reconstituted tobaccos, improve physical property, promote paper-making method reconstructed cigaretteLeaf pipe tobacco aesthetic quality, humid keeping performance and the compatibility with traditional pipe tobacco.
The above is only a preferred embodiment of the present invention, it should be pointed out that: for the ordinary skill people of the artFor member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answeredIt is considered as protection scope of the present invention.