A kind of additive with tongue fur note style and features and include the cigarette of the additiveTechnical field
The invention belongs to technical field of tobacco, and in particular to a kind of additive with tongue fur note style and features and include thisThe cigarette of additive.
Background technique
As international smoking ban cry rises from all around and cigarette consumption person is to the growing interest of own health, Less harmful cigarette will be atFor the mainstream of future world cigarette, but cigarette flavor loss is necessarily accompanied with while harm reduction and comfort level is deteriorated, and cigarette addsPerfume, which feeds, to be set off, added volume cigarette perfume taste, increase flue gas concentration, and improvement is jealous, removes and cover miscellaneous gas, reduce irritation, alsoThe characteristic chicken flavor of product grace can be assigned, the personalized style of prominent cigarette product, the research and development and application of perfuming cigarette charging are justAs one of the most key technology for keeping cigarette flavor and taste in lowering harm and decreasing coking work.Promote cigarette sucks satisfaction and pleasedHappy degree, becomes technical problem urgently to be resolved in current cigarette flavouring humectation technology.
Natural tongue fur note fragrance mainly includes the medicinal extract and absolute oil product of tree moss or oak moss in the market, and there are soil, gasThe difference factor such as time, growing environment brings the difference of raw material variety, and stable product quality cannot ensure；Simultaneously as it is madeStandby process is more or less mingled in obtained product mainly by separation and concentrations means such as organic solvent extraction, steam distillationsInfluence the invalid components such as pigment and the vegetable wax of aroma quality；In addition also often lead to human body containing some in medicinal extract and absolute oilThe ingredient and heavy metal of allergy, the Product quality and safety for food and daily use chemicals industry have buried security risk.
Currently, being also prepared by the method that various ingredients compound in the prior art some special with tongue fur note styleThe additive of sign.
CN103333743A discloses the tongue fur faint scent essence of a kind of 17 kinds of standard items and 2 kinds of solvents composition, has tongue fur faint scentGas style, however wherein invalid ingredient is contributed containing some pairs of fragrance.
CN107354007A, CN107616547A and CN107510092A disclose 2,4- dihydroxy -3,6- dimethyl benzeneThe tree moss note additive of methyl formate, 2,4-, 2 kinds of standard items of dihydroxy -6- benzyl Ethyl formate and solvent composition, wherein2 kinds of standard items being related to all have apparent tree moss note.
Synthetic perfume technical manual (see " synthetic perfume technical manual ", Liu Shuwen etc., China Light Industry Press, 2009January in year, page 136) list " 25 parts of orcin monomethyl ether and 75 parts of 2,4- dihydroxy -3,6- dimethylbenzoate methyl esterFit over and be used together, the compound fragrance of preparation has natural oak moss fragrance true to nature ", however 2 kinds of marks with oak moss noteThe compound fragrance that quasi- product are prepared only has the style of similar oak moss fragrance, and fragrance is coarse, there is dense chemical breath.
Although the additive with tongue fur note style and features has also been prepared in above-mentioned technical proposal, its preparation processComplexity, be by multiple standards product and solvent complex, wherein containing obviously invalid ingredient is contributed to fragrance and what is obtained haveThe additive fragrance of tongue fur note style and features is coarse, there is dense chemical breath.
Detailed description of the invention
Nothing.
Summary of the invention
To solve the above-mentioned problems, the present invention is proposed.
First aspect present invention provides a kind of additive with tongue fur note style and features, is based on weight percent, packetIt includes:
2,4- dihydroxy -6- the methyl toluate of 0.05%-15.5%；
The 3,5- dihydroxytoluene of 0.01%-0.2%.
Preferably, the additive further includes solvent, and the solvent is selected from ethyl alcohol, glyceryl triacetate or propylene glycol and thirdThe mixture of triol.
Preferably, the volumetric concentration of the ethyl alcohol is 50%-65%；The propylene glycol and the volume ratio of the glycerine are3:1-1:1。
Preferably, the additive further includes the beta-cyclodextrin of 10%-20% or the pregelatinized starch of 10%-20%.
Preferably, the additive with tongue fur note style and features the preparation method comprises the following steps: press the additive compositionContent takes 2, the 4- dihydroxy -6- methyl toluate and 3, the 5- dihydroxytoluene, the solvent is added, in roomUnder the conditions of temperature vibrate 10-20min dissolve raw material sufficiently, be configured to barrelling after uniform solution, be placed in be protected from light, shady place, save12-48h obtains the additive with tongue fur note style and features.If solid spice to be made, β-can also be addedThe substances such as cyclodextrin or pregelatinized starch adsorb aforesaid liquid fragrance and become solid form.
Second aspect of the present invention provides a kind of cigarette comprising the additive with tongue fur note style and features.
Preferably, it is added in cigarette filter by the dosage of 1-3 μ L/ branch filter tip, using cloud and mist (purple) leaf group rolling cigarette sampleProduct, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared.
Preferably, it is sprayed into cigarette bobbin paper surface by the dosage of 1.0-3.0mL/ hectogram obbbin, using Hongta (1956)Leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared.
Preferably, it is sprayed into cigarette shreds surface by the dosage of 0.05-3.00mL/ hectogram pipe tobacco, it is (classical using Hongta100) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared.
Preferably, cigarette heating is sprayed by the dosage that 0.03-2.00mL/ hectogram heats the cigarette shreds that do not burn or notCigarette shreds surface heats the cigarette X pipe tobacco that do not burn in production using cigarette in Yunnan and rolls cigarette sample, remaining auxiliary material and additiveIt remains unchanged, cigarette sample is prepared.
Compared with prior art, the invention has the following advantages:
1, of the invention by 2,4- dihydroxy -6- methyl toluate, the 3,5- bis- with pungent perfume with fertile soil tasteHydroxy-methylbenzene and solvent combination, are prepared the additive with tongue fur note style and features, and the additive has apparent tongue furNote, fragrance are abundant.
2, the additive with tongue fur note style and features of the invention, is added in cigarette, can increase cigarette perfumeTolerance assigns the apparent tongue fur note of cigarette, has and increases rich cigarette flavor, reduction stimulation, increase tongue fur note, promote cigaretteAspirate the effect of comfort and satisfaction.
3, the additive with tongue fur note style and features of the invention, most simple formula is only by 2 kinds of standard items and a kind of solvent groupAt constituent is simple, does not contribute fragrance invalid ingredient, and low in cost, preparation method is simple, is suitble to scaleProduction, has a good application prospect.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail, but is not limitation of the present invention, based on thisAny transformation or improvement that invention training centre is done, each fall within protection scope of the present invention.Be not specified in embodiment particular technique orCondition person described technology or conditions or carries out according to the literature in the art according to product description.Agents useful for same orProduction firm person is not specified in instrument, is the conventional products that can be obtained by purchase.
Comparative example 1
Take 0.05% 2,4- dihydroxy -6- methyl toluate and 99.95% triacetic acid sweet by mass percentageGrease mixing, vibrating 10min at room temperature dissolves raw material sufficiently, is configured to barrelling after uniform solution, is placed in and is protected from light, is negativeLiang Chu stores 12 hours, obtains additive A.
By the additive A, it is added in cigarette filter by the dosage of 1 μ L/ branch filter tip, is rolled using cloud and mist (purple) leaf groupCigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 1 is prepared, and compare and comment with cloud and mist (purple) productInhale discovery: fertile soil taste increases by 10%, and irritation reduces by 0.2%, and tongue fur note increases by 0%.
Comparative example 2
0.01% 3,5- dihydroxytoluene and the mixing of 99.99% glyceryl triacetate are taken by mass percentage, in room10min is vibrated under the conditions of temperature dissolves raw material sufficiently, is configured to barrelling after uniform solution, be placed in be protected from light, shady place, storage is 12 smallWhen, obtain additive B.
By the additive B, it is added in cigarette filter by the dosage of 1 μ L/ branch filter tip, is rolled using cloud and mist (purple) leaf groupCigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 2 is prepared, and compare and comment with cloud and mist (purple) productInhale discovery: Xin Xiang increases by 4%, and irritation reduces by 0.5%, and tongue fur note increases by 0%.
Embodiment 1
0.05% 2,4- dihydroxy -6- methyl toluate, 0.01% 3,5- dihydroxy are taken by mass percentageToluene, 99.94% glyceryl triacetate mixing, at room temperature vibrate 10min dissolve raw material sufficiently, be configured to uniformBarrelling after solution, be placed in be protected from light, shady place, store 12 hours, obtain addition of C.
By the addition of C, it is added in cigarette filter by the dosage of 1 μ L/ branch filter tip, is rolled using cloud and mist (purple) leaf groupCigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 3 is prepared, and compare and comment with cloud and mist (purple) productInhale discovery: fragrance is rich to increase by 2%, and irritation reduces by 1%, and tongue fur note increases by 3%.
Embodiment 2
0.2% 2,4- dihydroxy -6- methyl toluate, 0.05% 3,5- dihydroxy first are taken by mass percentageBenzene, 99.75% 60% alcohol of volumetric concentration mixing, at room temperature vibrate 10min dissolve raw material sufficiently, be configured toBarrelling after one solution, be placed in be protected from light, shady place, store 24 hours, obtain additive D.
By the additive D, it is sprayed into cigarette bobbin paper surface by the dosage of 1.0mL/ hectogram obbbin, using Hongta(1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 4 is prepared, with Hongta(1956) product compares discovery of smokeing panel test: fragrance is rich to increase by 3%, and irritation reduces by 3%, and tongue fur note increases by 5%, flue gasComfort promotes 1%.
Embodiment 3
10% 2,4- dihydroxy -6- methyl toluate, 0.1% 3,5- dihydroxy first are taken by mass percentageBenzene, 89.9% volume ratio be 3:1 glycol/propane triol mix, at room temperature vibrate 20min keep raw material sufficiently moltenSolution, be configured to barrelling after uniform solution, be placed in be protected from light, shady place, store 24 hours, obtain additive E.
By the additive E, it is sprayed into cigarette shreds surface by the dosage of 3.00mL/ hectogram pipe tobacco, using Hongta (warpAllusion quotation 100) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 5 is prepared, with Hongta(classics 100) product compares discovery of smokeing panel test: fragrance is rich to increase by 5%, and irritation reduces by 5%, and tongue fur note increases by 7%.
Embodiment 4
15.5% 2,4- dihydroxy -6- methyl toluate, 0.2% 3,5- dihydroxy first are taken by mass percentageBenzene, 64.3% volume ratio 3:1 glycol/propane triol, 20% pregelatinized starch mixing, stir at room temperature25min dissolves raw material sufficiently, is configured to barrelling after uniform solution, be placed in be protected from light, shady place, store 24 hours, addedAgent F.
By the additive F, it is non-ignitable that cigarette heating is sprayed by the dosage that 2.00mL/ hectogram heats the cigarette shreds that do not burnCigarette shreds surface is burnt, which is simultaneously rolled cigarette sample by certain, remaining auxiliary material and additive remain unchanged, and volume is preparedCigarette sample 6, compare discovery of smokeing panel test with the sample before applying the fragrance: fragrance is rich to increase by 7%, and irritation reduces5%, tongue fur note increases by 9%.