(1) water phase: adding transparent xanthan gum, gellan gum and sodium hyaluronate into glycerol, premixing uniformly to obtain a premixed phase, adding water into a main kettle, adding the premixed phase and methyl hydroxybenzoate into room-temperature water, stirring and heating to 80-85 ℃, fully swelling, cooling to 60-65 ℃, adding calcium chloride, cooling to 40-45 ℃, adding bis (hydroxymethyl) imidazolidinyl urea, caprylyl glycol and ethanol, and detecting the density of an aqueous phase;

(2) oil phase: according to the density of the water phase, calculating the dosage of each liquid grease in the oil phase, and controlling rho_{Oil phase}＝ρ_{Aqueous phase}+/-0.01, then adding propyl hydroxybenzoate and butylated hydroxytoluene, heating to over 75 ℃ until the mixture is dissolved and transparent, and cooling to about 40 ℃;

(3) and (3) finished product: and adding the oil phase into the water phase of the main kettle under the stirring condition until oil drops are suspended in the water phase, wherein the particle size of the oil drops is within the range of 0.6mm +/-0.2, and discharging after the detection is qualified.

TABLE 2 examples 3-5 the proportions of the ingredients (in weight percent)

The preparation method comprises the following steps:

(1) adding water into a main kettle, adding dehydro xanthan gum and gellan gum into glycerol, premixing uniformly to obtain a premixed phase, adding water into the main kettle, then adding the premixed phase, methyl hydroxybenzoate and electrolyte into the water at room temperature, stirring and heating to 80-85 ℃, fully swelling, cooling to 60-65 ℃, adding the electrolyte, cooling to 40-45 ℃, adding bis (hydroxymethyl) imidazolidinyl urea, ethanol, caprylyl glycol and sodium hyaluronate, and detecting the density of the water phase;

(2) according to the density of the water phase, calculating the dosage of each liquid grease in the oil phase, and controlling rho_{Oil phase}＝ρ_{Aqueous phase}+/-0.01, then adding propyl hydroxybenzoate and butylated hydroxytoluene, heating to over 75 ℃ until the mixture is dissolved and transparent, cooling to 40-45 ℃, adding a color additive, and uniformly stirring;

(3) and adding the oil phase into the water phase of the main kettle under the stirring condition until oil drops are suspended in the water phase, wherein the particle size of the oil drops is within the range of 0.6mm +/-0.2, and discharging after the detection is qualified.

Table 3 examples 6-7:

the preparation method comprises the following steps:

(1) water phase: adding dehydroxanthan gum and gellan gum into glycerol, and premixing to obtain a premixed phase; adding water into the main kettle, adding the premixed phase, methyl hydroxybenzoate and calcium chloride into room-temperature water, stirring and heating to 80-85 ℃, fully swelling, cooling to 60-65 ℃, adding electrolyte, cooling to 40-45 ℃, adding bis (hydroxymethyl) imidazolidinyl urea and ethanol, and detecting the density of the water phase;

(2) oil phase: according to the density of the water phase, calculating the dosage of each liquid grease in the oil phase, and controlling rho_{Oil phase}＝ρ_{Aqueous phase}Plus or minus 0.01, then adding propyl hydroxybenzoate and butylated hydroxytolueneHeating to above 75 deg.C for dissolving and transparency, cooling to 40-45 deg.C, adding color additive, and stirring;

Table 4 examples 8-12:

the preparation method comprises the following steps:

step (1) water phase: adding a thickening agent into a humectant, premixing uniformly to obtain a premixed phase, adding water into a main kettle, adding the premixed phase and an aqueous preservative into water at room temperature, stirring and heating to 80-85 ℃, fully swelling, cooling to 60-65 ℃, adding an electrolyte, cooling to 40-45 ℃, adding a skin conditioning agent, and detecting the density of an aqueous phase;

and (3) finishing: and adding the oil phase into the water phase of the main kettle under the stirring condition until oil drops are suspended in the water phase, wherein the particle size of the oil drops is within the range of 0.6mm +/-0.2, and discharging after the detection is qualified.

Table 5 examples 13-14:

preparation process

step (2) oil phase: according to the density of the water phase, the usage amount of sucrose acetate isobutyrate and other liquid oil in the oil phase is calculated, and rho is adjusted_{Oil phase}＝ρ_{Aqueous phase}+/-0.01, adding the oil phase preservative and the antioxidant, then adding the oil phase preservative and the antioxidant, heating to the temperature of over 75 ℃ until the mixture is dissolved and transparent, cooling to the temperature of 40 +/-5 ℃, adding the color additive, and uniformly stirring;

Table 6 examples 15-16:

the preparation method comprises the following steps:

Test example-stability and comparative test

The method comprises the following steps: the oil phase formulation of example 3 and the oil phase formulation of the comparative example are shown in Table 7, and the stability of the oil phase of the cosmetic water for suspended oil globules prepared is compared at low temperature of-18 ℃.

As a result: as shown in FIG. 1, the oil phase of the oil emulsion type make-up water emulsion prepared by adding an oily preservative and sucrose acetate isobutyrate to the oil phase formulation of example 3 was yellow and no precipitation was observed at-18 ℃ and the oil phase of the oil emulsion type make-up water emulsion prepared by adding an oily preservative to the system containing trimethylpentaphenyltrisiloxane oil and fat in the comparative example was transparent and no precipitation was observed at-18 ℃. The solubility of the mixed grease (containing synthetic grease, vegetable grease and the like) adopted by the invention on the propylparaben (oil-soluble solid) is proved to be greatly superior to that of a mixed silicone oil system. Therefore, the suspension toning lotion formula system of the invention has stronger practicability.

TABLE 7 oil phase composition

Test example two moisture retention test

Subject: see the formulation in Table 8

TABLE 8 moisture retention experiment ingredient table

The experimental method comprises the following steps: about 0.25g of each sample was applied to a 7.5cm × 7.5cm glass plate to which a 3M adhesive tape was attached, placed in a desiccator containing a saturated solution of sodium chloride (relative humidity: 78.5 ± 1%), allowed to stand for a certain period of time, weighed, and the moisture retention rates at different times were calculated.

Moisture retention rate%_t/M₀×100

M_t- -mass of water remaining after standing th;

M₀- -mass of water before standing;

as a result: table 9 the non-silicone oil type oil-water mixed non-emulsified aqueous solution of the present invention has a slightly superior moisturizing effect compared to commercially available silicone oil type oil-water mixed non-emulsified aqueous solution products, and achieves rapid and lasting moisturizing.

Table 9 results of the moisture retention test

The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. It is not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain certain principles of the invention and its practical application to enable one skilled in the art to make and use various exemplary embodiments of the invention and various alternatives and modifications as are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the claims and their equivalents.

Claims

1. A suspended oil bead toning lotion containing sucrose acetate isobutyrate is characterized by comprising 2-8% of grease, 0-1.2% of preservative, 0-2% of thickening agent, 2-10% of humectant, 1-5% of auxiliary component and the balance of water by weight percentage; the grease is prepared from sucrose acetate isobutyrate and synthetic grease, vegetable grease or animal oil or mineral oil according to the weight ratio of (1.96-2.35) to (1.05-1.44): (0.3-0.9) or the grease is prepared by mixing sucrose acetate isobutyrate and synthetic oil according to the weight ratio of (2.23-2.75): (1.25-1.75).

2. The water according to claim 1, which comprises 3 to 6% by weight of the oil, 0.3 to 1% by weight of a preservative, 0.2 to 1% by weight of a thickener, 5 to 9% by weight of a humectant, 1.5 to 5% by weight of an auxiliary component, and the balance water.

3. The water according to claim 2, which comprises 3 to 4% by weight of the raw material oil, 0.35 to 0.65% by weight of a preservative, 0.2 to 0.6% by weight of a thickener, 7 to 8% by weight of a humectant, 1.5 to 3% by weight of an auxiliary component, and the balance of water.

4. The cosmetic water of suspended oil globules as claimed in any of claims 1 to 3, wherein the ratio by weight of sucrose acetate isobutyrate to synthetic, vegetable or animal or mineral oils (1.96-2.35) is (1.05-1.44): 0.6.

5. the water according to any one of claims 1 to 3, wherein the thickener is one or more selected from the group consisting of sodium/lithium magnesium silicate, xanthan gum, gellan gum, dehydroxanthan gum, gum arabic, tragacanth gum, guar gum.

6. The water according to claim 5, wherein the thickener is any two of sodium/lithium magnesium silicate, dehydroxanthan gum, gellan gum, and xanthan gum according to (1-10): 1, compounding.

7. The water according to any one of claims 1 to 3, wherein the humectant is at least one of 1, 3-propanediol, 1, 3-butanediol, PEG-400, glyceryl polyether-26, dipropylene glycol, glycerin, ethylhexyl glycerin, sodium hyaluronate, and caprylyl glycol.

8. The water according to any one of claims 1 to 3, wherein the auxiliary component is one or more of a skin conditioner, an antioxidant, an electrolyte, a perfume, a chelating agent, a color additive, and the like.

9. The cosmetic water as claimed in any one of claims 1 to 3, wherein the synthetic oil or fat is liquid paraffin, isopropyl myristate, isopropyl palmitate, 2-ethylhexyl palmitate, unsaturated fatty acids, palmitic acid oleate, linoleic acid, isotridecanol isononanoate, isononyl isononanoate, isodecyl neopentanoate, neopentyl glycol diheptanoate, ethylhexyl methoxycinnamate, diisostearyl malate, tris (ethylhexanoate) myristate, isopropyl myristate, caprylic/capric triglyceride, ethylhexyl palmitate, caprylic/dicaprate octanediol dioctanoate, octyldodecanol or squalane.

10. The suspended oil bead lotion according to claim 9, wherein the synthetic oil is caprylic/capric triglyceride, neopentyl glycol diheptanoate or octanediol dioctanoate/dicaprate.

11. The cosmetic water of any one of claims 1 to 3, wherein the vegetable oil is olive oil, rice bran oil, palm oil, soybean oil, sesame oil, persic oil, jojoba oil, cottonseed oil, coconut oil, babassu oil, almond oil, avocado oil, wheat germ oil, or macadamia nut oil.

12. The water according to claim 11, wherein the vegetable oil is jojoba oil or macadamia nut oil.

13. The water according to any one of claims 1 to 3, wherein the animal oil is whale oil or fish oil.

14. The cosmetic water according to any one of claims 1 to 3, wherein the preservative is a water-soluble preservative or an oily aqueous preservative, and the oily preservative is used in combination, and the preservative is one or more of propylparaben, methylparaben, phenoxyethanol, and bis-hydroxymethyl imidazolidinyl urea.

15. The method for preparing the suspended oil bead lotion containing sucrose acetate isobutyrate as set forth in claim 1, comprising the steps of:

step (1) water phase: adding the thickening agent into the room temperature humectant, and uniformly premixing to obtain a premixed phase; adding water into the main kettle, adding the premixed phase and the aqueous preservative into water at room temperature, stirring and heating to 80-85 ℃, fully swelling, cooling to 60-65 ℃, adding electrolyte, cooling to 40-45 ℃, adding a skin regulator, and detecting the density of the water phase;