技术领域technical field
本发明涉及一种含吸附剂的低温卷烟用烟芯材料的制备方法，属于新型烟草制备技术领域。The invention relates to a method for preparing a low-temperature cigarette core material containing an adsorbent, and belongs to the technical field of novel tobacco preparation.
背景技术Background technique
纵观全球，传统卷烟消费日趋下降、全球控烟法规层出不穷、人们越来越重视健康，使得烟草行业的发展之路更加举步维艰。国际跨国烟草公司无一例外都从战略和长远角度对新型烟草制品的研发予以高度重视，新型烟草制品迅猛发展。低温卷烟作为新型烟草制品中的一类主要产品，其研究与开发受到烟草行业的高度重视。低温卷烟采用低温烘烤烟丝产生烟气，其抽吸感受最接近传统卷烟，对消费者而言，低温卷烟一方面在最大限度还原常规卷烟的吸食口感的同时，减少了对吸食者身体的危害和对周边环境的影响。菲莫国际、英美烟草、日本烟草上市的几款低温卷烟产品在日本一经推出都大获好评。Throughout the world, the consumption of traditional cigarettes is declining, global tobacco control laws and regulations are emerging one after another, and people are paying more and more attention to health, which makes the development of the tobacco industry more difficult. Without exception, international multinational tobacco companies have attached great importance to the research and development of new tobacco products from a strategic and long-term perspective, and new tobacco products have developed rapidly. Low-temperature cigarettes are one of the main types of new tobacco products, and their research and development have been highly valued by the tobacco industry. Low-temperature cigarettes use low-temperature cured tobacco to produce smoke, and their smoking experience is closest to that of traditional cigarettes. For consumers, low-temperature cigarettes can restore the taste of conventional cigarettes to the greatest extent while reducing the harm to the smoker’s body. and impact on the surrounding environment. Several low-temperature cigarette products launched by Philip Morris International, British American Tobacco, and Japan Tobacco were well received in Japan once they were launched.
发明内容Contents of the invention
当前，市场上的低温卷烟主要是利用在特制电加热装置中填充烟草材料，如烟支、烟丝或烟片等，通过加热使烟草材料烘烤发出烟气，从而使抽烟者获得类似传统卷的抽吸感受。然而，由于电加热温度远低于传统卷烟温度，导致烟草材料产生烟雾量低，因此烟草材料中要加入发烟剂增加烟草材料的发烟量。低温卷烟用发烟剂一般为多元醇，主要为丙三醇和丙二醇。然而，当发烟剂添加量较高时，尤其是丙三醇含量较高时，会使烟草材料吸潮严重，造成烟支软化、卷烟纸发黄；而且还会因丙三醇黏度大使烟草材料粘结成块，造成烟草材料受热不均匀以及抽吸阻力加大，影响抽吸效果。而发烟剂含量较低时，尤其是丙三醇的含量低时，烟草材料烟雾量低而得不到抽吸卷烟的感觉。因此如何克服现有技术的不足是目前低温卷烟技术领域亟需解决的问题。At present, low-temperature cigarettes on the market are mainly filled with tobacco materials, such as cigarettes, shredded tobacco or tobacco sheets, etc., in special electric heating devices, and the tobacco materials are baked to emit smoke through heating, so that smokers can obtain cigarettes similar to traditional cigarettes. Pumping sensation. However, since the temperature of electric heating is much lower than that of traditional cigarettes, the amount of smoke produced by the tobacco material is low, so a smoking agent should be added to the tobacco material to increase the amount of smoke generated by the tobacco material. Smokers for low-temperature cigarettes are generally polyols, mainly glycerol and propylene glycol. However, when the amount of smoking agent added is high, especially when the content of glycerin is high, the tobacco material will absorb moisture seriously, causing softening of cigarettes and yellowing of cigarette paper; The material sticks into blocks, causing uneven heating of the tobacco material and increased suction resistance, which affects the suction effect. And when the content of smoking agent is low, especially when the content of glycerin is low, the smoke amount of the tobacco material is low and the feeling of smoking a cigarette cannot be obtained. Therefore, how to overcome the deficiencies of the prior art is an urgent problem to be solved in the field of low-temperature cigarette technology.
本发明的目的就是要解决现有技术存在的不足，提供一种含吸附剂的低温卷烟用烟芯材料的制备方法。为实现上述技术目的，本发明采用的技术方案如下：The object of the present invention is to solve the deficiencies in the prior art, and provide a method for preparing an adsorbent-containing low-temperature cigarette core material. For realizing above-mentioned technical purpose, the technical scheme that the present invention adopts is as follows:
一种含吸附剂的低温卷烟用烟芯材料的制备方法，其特征在于，具体包括如下步骤：A method for preparing an adsorbent-containing low-temperature cigarette core material, characterized in that it specifically comprises the following steps:
步骤SS1：将烟草原料烘干磨碎成粉末；Step SS1: drying and grinding the tobacco raw material into powder;
步骤SS2：向所述步骤SS1中制得的烟草原料施加含烟用香精的无水乙醇溶液，并在密封状态下放置24～48h，自然风干；Step SS2: Apply an absolute ethanol solution containing tobacco essence to the tobacco raw material prepared in the step SS1, place it in a sealed state for 24-48 hours, and let it dry naturally;
步骤SS3：将吸附了发烟介质的吸附剂加入所述步骤SS2制得的烟草原料中，混合均匀；Step SS3: adding the adsorbent that has adsorbed the smoking medium to the tobacco raw material prepared in the step SS2, and mixing evenly;
步骤SS4：向所述步骤SS3制得的烟草原料中加入增稠剂使形成粘稠状混合物；Step SS4: adding a thickener to the tobacco raw material prepared in the step SS3 to form a viscous mixture;
步骤SS5：将所述步骤SS4所得到的粘稠状混合物低温烘干成薄片，制得烟芯材料。Step SS5: drying the viscous mixture obtained in the step SS4 at a low temperature into thin sheets to obtain a cigarette core material.
作为一种较佳的实施例，所述步骤SS1具体包括：将烟草原料烘干磨碎成粉末，所述粉末粒径≤40目。As a preferred embodiment, the step SS1 specifically includes: drying and grinding the tobacco raw material into powder, and the particle size of the powder is ≤40 mesh.
作为一种较佳的实施例，所述步骤SS2中的烟用香精为丁香酚、菠萝酮、乙基香兰素中的一种或几种的混合。As a preferred embodiment, the tobacco flavor in the step SS2 is one or a mixture of eugenol, pineapple ketone and ethyl vanillin.
作为一种较佳的实施例，所述步骤SS3中的所述吸附剂为活性炭、硅胶、海泡石、蒙脱石、麦饭石、分子筛中的一种或几种的混合。As a preferred embodiment, the adsorbent in the step SS3 is one or a combination of activated carbon, silica gel, sepiolite, montmorillonite, medical stone, and molecular sieve.
作为一种较佳的实施例，所述步骤SS3中的所述发烟介质为丙三醇。As a preferred embodiment, the smoking medium in the step SS3 is glycerol.
作为一种较佳的实施例，所述步骤SS3中的所述发烟介质吸附在所述吸附剂上。As a preferred embodiment, the smoke-generating medium in the step SS3 is adsorbed on the adsorbent.
作为一种较佳的实施例，所述步骤SS4中的所述增稠剂为瓜尔胶、黄原胶、卡拉胶、琼脂、明胶中的一种或几种的混合。As a preferred embodiment, the thickener in the step SS4 is one or a mixture of guar gum, xanthan gum, carrageenan, agar, and gelatin.
作为一种较佳的实施例，所述步骤SS5还包括：烟草原料低温烘干温度为40～70℃。As a preferred embodiment, the step SS5 further includes: the low-temperature drying temperature of the tobacco raw material is 40-70°C.
本发明所达到的有益效果：第一，本发明利用吸附剂来吸附发烟剂，避免烟草材料中直接加入发烟剂造成的烟草材料粘结问题；第二，本发明利用吸附剂来吸附发烟剂，避免烟草材料中直接加入大量发烟剂使烟草材料因吸潮严重造成烟支软化、卷烟纸发黄的问题；第三，本发明利用吸附剂来吸附发烟剂，可以通过施加吸附剂的量来调控烟草材料的发烟量，方便烟草材料进行配方调整；第四，本发明制作的含吸附剂的低温卷烟用烟芯材料，利用吸附剂来吸附发烟剂，从而使烟芯材料的表观干燥感增加，增加烟芯材料之间的松散度，使烟芯材料之间的热量更好的传递，增加烟草材料的受热均匀性；第五，本发明制作的含吸附剂的低温卷烟用烟芯材料，利用吸附剂来吸附发烟剂，从而使烟芯材料的表观干燥感增加，增加烟芯材料之间的松散度，使烟气能更好的透发；第六，本发明利用吸附剂来吸附发烟剂，可以施加更高用量的发烟剂，从而使得低温卷烟的烟雾量高，同时产生的高烟雾量透过烟草材料时，热气流能将烟草材料的香味物质带出，增加烟气的丰满度；第七，本发明制作的含吸附剂的低温卷烟用烟芯材料制备方法简单，抽吸效果好：烟气刺激性低、烟雾量大、烟气浓度高，感官舒适度显著提升。The beneficial effects achieved by the present invention are as follows: first, the present invention uses an adsorbent to adsorb the fuming agent, avoiding the tobacco material bonding problem caused by directly adding the fuming agent to the tobacco material; second, the present invention uses the adsorbent to adsorb the fuming agent smoke agent, to avoid directly adding a large amount of smoke agent to the tobacco material to cause the tobacco material to soften the cigarette and cause the cigarette paper to turn yellow due to moisture absorption; third, the present invention uses an adsorbent to absorb the smoke agent, which can be achieved by applying adsorption The amount of sorbent is used to regulate the amount of smoke generated by the tobacco material, which is convenient for the formulation adjustment of the tobacco material; fourth, the low-temperature cigarette core material containing adsorbent produced by the present invention uses the adsorbent to absorb the smoke-generating agent, so that the smoke core The apparent dryness of the material increases, the looseness between the tobacco core materials is increased, the heat transfer between the tobacco core materials is better, and the heating uniformity of the tobacco material is increased; The core material for low-temperature cigarettes uses an adsorbent to absorb the smoke-generating agent, thereby increasing the apparent dryness of the core material, increasing the looseness between the core materials, and making the smoke more transparent; sixth , the present invention uses an adsorbent to adsorb the fuming agent, and can apply a higher amount of fuming agent, so that the smoke volume of the low-temperature cigarette is high, and at the same time, when the high smoke volume produced passes through the tobacco material, the hot air flow can dissipate the smoke content of the tobacco material. Flavor substances are brought out to increase the fullness of smoke; seventh, the preparation method of the low-temperature cigarette core material containing adsorbent produced by the present invention is simple, and the suction effect is good: the smoke is low in irritation, the amount of smoke is large, and the smoke The concentration is high, and the sensory comfort is significantly improved.
附图说明Description of drawings
图1是本发明的方法流程图。Fig. 1 is a flow chart of the method of the present invention.
具体实施方式Detailed ways
下面结合附图对本发明作进一步描述。以下实施例仅用于更加清楚地说明本发明的技术方案，而不能以此来限制本发明的保护范围。The present invention will be further described below in conjunction with the accompanying drawings. The following examples are only used to illustrate the technical solution of the present invention more clearly, but not to limit the protection scope of the present invention.
实施例1：Example 1:
一种含吸附剂的低温卷烟用烟芯材料的制备方法，依次包括以下步骤：A method for preparing an adsorbent-containing low-temperature cigarette core material, comprising the following steps in sequence:
将烟草原料烘干磨碎成粉末，过40目筛；向其中施加含烟用香精的无水乙醇溶液，施加量为M烟丝：V乙醇＝1.0g：1.0mL，于密封状态下放置24～48h后自然风干；将吸附了丙三醇的硅胶加入烟草原料中，混合均匀；以瓜尔胶为增稠剂使烟草原料和硅胶形成粘稠状混合物；将所得到的粘稠状混合物于60℃烘干成薄片。Dry and grind the tobacco raw materials into powder, pass through a 40-mesh sieve; apply an anhydrous ethanol solution containing tobacco essence to it, the application amount is M shredded tobacco: V ethanol = 1.0g: 1.0mL, and place it in a sealed state for 24~ Naturally air-dry after 48h; Add the silica gel that has absorbed glycerol in the tobacco raw material, mix evenly; Make tobacco raw material and silica gel form viscous mixture with guar gum as thickener; ℃ and dried into flakes.
本发明对所述烟用香精的种类和来源没有特殊的限制，采用本领域技术人员熟知的烟用香精即可。在本发明中，所述烟用香精的无水乙醇溶液优先包括重量百分比的如下组成：丁香酚0.2‰、菠萝酮0.5‰、乙基香兰素1‰，其余为无水乙醇，各组分总和为100，混匀后制成。The present invention has no special limitation on the type and source of the tobacco flavor, and the tobacco flavor well known to those skilled in the art can be used. In the present invention, the dehydrated ethanol solution of the flavoring essence for tobacco preferably includes the following composition by weight percentage: eugenol 0.2‰, pineapple 0.5‰, ethyl vanillin 1‰, and the rest is dehydrated ethanol, each component The sum is 100, made after mixing.
本发明中，M硅胶：M丙三醇＝2：3；In the present invention, Msilica gel : Mglycerol = 2:3;
本发明中，M烟草原料：M硅胶＝5：3。In the present invention, Mtobacco raw material : Msilica gel = 5:3.
实施例2：Example 2:
同实施例1，区别在于吸附剂采用活性炭。With embodiment 1, difference is that adsorbent adopts active carbon.
本发明中，M活性炭：M丙三醇＝4：5；In the present invention, Mactivated carbon : Mglycerol =4:5;
本发明中，M烟草原料：M活性炭＝1：1。In the present invention, Mtobacco raw material : Mactivated carbon = 1:1.
实施例3：Example 3:
同实施例1，区别在于增稠剂为黄原胶。With embodiment 1, the difference is that the thickener is xanthan gum.
效果评价：Evaluation:
将采用实施例1、实施例2、实施例3方法制备的烟芯材料与未添加吸附材料的烟芯材料(对比样)添加到低温烟具中进行感官质量评价，评价结果见表1。Add the cigarette core materials prepared by the methods of Example 1, Example 2, and Example 3 and the cigarette core materials without adsorption material (comparative sample) into low-temperature smoking appliances for sensory quality evaluation. The evaluation results are shown in Table 1.
检验程序：向6名评吸专家提供试样和检验表，要求评吸员按照表格要求对各项指标进行评吸。Inspection procedure: Provide samples and inspection forms to 6 suction evaluation experts, and require the evaluation staff to evaluate various indicators according to the requirements of the form.
表1本发明实施例评吸结果Table 1 embodiment of the present invention evaluates suction result
注：丙三醇％＝(M丙三醇/M烟芯材料)*100％。Note: glycerol%=(Mglycerol /Mcigarette core material )*100%.
由表1可知，运用本发明制备的烟芯材料在加热非燃烧状态下的烟气释放性能和所释放烟气的感官品质明显得到改善，烟气舒适性提高。It can be seen from Table 1 that the smoke release performance and the sensory quality of the released smoke are significantly improved by using the smoke core material prepared by the present invention in the heating and non-combustion state, and the comfort of the smoke is improved.
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明技术原理的前提下，还可以做出若干改进和变形，这些改进和变形也应视为本发明的保护范围。The above is only a preferred embodiment of the present invention, it should be pointed out that for those of ordinary skill in the art, without departing from the technical principle of the present invention, some improvements and modifications can also be made. It should also be regarded as the protection scope of the present invention.
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711019523.0ACN107802024B (en) | 2017-10-25 | 2017-10-25 | A kind of preparation method of low temperature cigarette wick material containing adsorbent |
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711019523.0ACN107802024B (en) | 2017-10-25 | 2017-10-25 | A kind of preparation method of low temperature cigarette wick material containing adsorbent |
| Publication Number | Publication Date |
|---|---|
| CN107802024Atrue CN107802024A (en) | 2018-03-16 |
| CN107802024B CN107802024B (en) | 2020-04-28 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711019523.0AActiveCN107802024B (en) | 2017-10-25 | 2017-10-25 | A kind of preparation method of low temperature cigarette wick material containing adsorbent |
| Country | Link |
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| CN (1) | CN107802024B (en) |
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| CN114009826A (en)* | 2021-12-06 | 2022-02-08 | 云南中烟新材料科技有限公司 | A kind of heating cigarette wick material and preparation method thereof |
| CN114009826B (en)* | 2021-12-06 | 2023-03-10 | 云南中烟新材料科技有限公司 | Heating cigarette core material and preparation method thereof |
| Publication number | Publication date |
|---|---|
| CN107802024B (en) | 2020-04-28 |
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