技术领域technical field
本发明涉及烟草技术领域，尤其涉及一种发烟制品及其制备方法。The invention relates to the technical field of tobacco, in particular to a smoking product and a preparation method thereof.
背景技术Background technique
加热不燃烧型烟草制品是一种新型的烟草制品，与抽吸传统卷烟相比，两者抽吸的烟草均包括烟丝、烟草碎片、烟草颗粒、烟末等。但是，加热不燃烧型烟草制品在抽吸时烟草部位温度较低，仅加热烟草而不燃烧烟草，因而能够极大降低甚至避免焦油的产生。消费者抽吸加热不燃烧型烟草制品时不会产生测流烟气，且几乎不产生进入环境的烟气，即所谓的“二手烟”，大大降低了环境污染。加热不燃烧型烟草制品正因其焦油量极低和环境友好而受到部分烟草消费者的欢迎，正逐步被大多数国家的卷烟消费者所接受。Heat-not-burn tobacco products are a new type of tobacco products. Compared with smoking traditional cigarettes, the tobacco smoked by both includes shredded tobacco, tobacco fragments, tobacco particles, tobacco powder, etc. However, the temperature of the tobacco part of the heat-not-burn tobacco product is relatively low during smoking, and only the tobacco is heated without burning the tobacco, so the production of tar can be greatly reduced or even avoided. When consumers smoke heat-not-burn tobacco products, no flue gas will be produced, and almost no smoke will enter the environment, that is, the so-called "second-hand smoke", which greatly reduces environmental pollution. Heat-not-burn tobacco products are being welcomed by some tobacco consumers because of their extremely low tar content and environmental friendliness, and are gradually being accepted by cigarette consumers in most countries.
目前，加热非燃烧型卷烟主要有电加热卷烟、碳质加热卷烟和化学加热卷烟三种类型：At present, there are three types of heat-not-burn cigarettes: electric heating cigarettes, carbonaceous heating cigarettes and chemical heating cigarettes:
(1)电加热卷烟。菲利普莫里斯生产公司先后推出的“Accord”、“Heatbar”、“EHP”三款电加热卷烟产品，均采用电加热器对卷烟制品进行加热的方式产生烟气，卷烟制品具有与传统卷烟类似的结构及外形；R.J.雷诺兹烟草公司的发明专利《含有烟草的吸烟物品》介绍了一种电加热卷烟，采用电阻加热元件对烟草进行加热而产生烟气，其中烟草通常为切丝填料；湖北中烟工业有限公司的实用新型专利《电加热式卷烟》公开了一种电加热卷烟，该卷烟通过多孔加热板和外加热壁对烟片进行加热发出烟气，但烟片的配方及其制作方法还未见公开。(1) Electrically heated cigarettes. Philip Morris Production Company has successively launched three electric heating cigarette products, "Accord", "Heatbar", and "EHP", all of which use electric heaters to heat cigarette products to generate smoke. Structure and shape; R.J. Reynolds Tobacco Company’s invention patent "Smoking Articles Containing Tobacco" introduces an electrically heated cigarette, which uses resistance heating elements to heat tobacco to generate smoke, in which tobacco is usually shredded filler; Hubei Zhong The utility model patent "Electric Heating Cigarette" of Tobacco Industry Co., Ltd. discloses an electric heating cigarette, which uses a porous heating plate and an external heating wall to heat the tobacco sheet to emit smoke, but the formula and production method of the tobacco sheet Not seen yet.
(2)碳质加热卷烟。R.J.雷诺兹烟草公司先后以商标Premier和Eclipse来销售该类型的卷烟，其中Eclipse卷烟采用碳质热源燃烧释放的热量加热膨胀烟草填料而产生烟气供人们抽吸，膨胀烟草填料为再造烟叶；日本烟草产业株式会社的发明专利《非燃烧型吸烟物品用碳质热源组成物和非燃烧型吸烟物品》公开了一种碳质加热卷烟，该卷烟也是采用碳质热源燃烧释放的热量加热烟片或烟丝。(3)化学加热卷烟。奥利格股份公司公开的发明专利《无烟香烟》属于化学加热卷烟，该卷烟采用可结晶物质结晶释放热量的原理来加热尼古丁储器释放出挥发性成分供消费者抽吸；斯泰格莫德有限公司公开了一项发明专利《吸烟制品》，该吸烟制品通过某些化合物的反应来提供热量加热烟草产生烟气，其中该烟草可以为许多不同方式加工的烟草。(2) Carbonaceous heating cigarettes. R.J. Reynolds Tobacco Company successively sells this type of cigarettes under the trademarks Premier and Eclipse. Among them, Eclipse cigarettes use the heat released by the combustion of carbonaceous heat sources to heat and expand the tobacco filler to generate smoke for people to smoke. The expanded tobacco filler is reconstituted tobacco leaves; Japan The invention patent of Tobacco Industry Co., Ltd. "Carbonaceous Heat Source Composition for Non-combustible Smoking Articles and Non-combustible Smoking Articles" discloses a carbonaceous heating cigarette. cut tobacco. (3) Chemically heated cigarettes. The invention patent "Smokeless Cigarette" disclosed by Olig AG belongs to chemically heated cigarettes, which use the principle of crystallization of crystallized substances to release heat to heat the nicotine reservoir and release volatile components for consumers to smoke; Stegmore Germany Co., Ltd. has disclosed an invention patent "Smoking Product". The smoking product provides heat to heat tobacco to generate smoke through the reaction of certain compounds, wherein the tobacco can be processed tobacco in many different ways.
由于加热不燃烧型烟草制品深受消费者欢迎，但是国内外却很少报道或记载加热不燃烧型烟草制品的发烟制品的制备方法，因此，研究一种适用于加热不燃烧型卷烟领域的发烟制品具有重要的意义。Since heat-not-burn tobacco products are very popular among consumers, but there are few reports or records at home and abroad on the preparation method of smoking products for heat-not-burn tobacco products. Smoking articles are of great importance.
发明内容Contents of the invention
鉴于以上所述现有技术的缺点，本发明的目的在于提供一种发烟制品及其制备方法，可用于加热不燃烧型卷烟领域，克服现有技术中存在缺陷。In view of the above-mentioned shortcomings of the prior art, the purpose of the present invention is to provide a smoking article and a preparation method thereof, which can be used in the field of heat-not-burn cigarettes and overcome the defects in the prior art.
为了实现上述目的或者其他目的，本发明是通过以下技术方案实现的。In order to achieve the above objects or other objects, the present invention is achieved through the following technical solutions.
一种发烟制品，所述发烟制品包括改性烟草、果胶、发泡剂、雾化剂和香精粉。A smoking product, the smoking product includes modified tobacco, pectin, foaming agent, atomizing agent and essence powder.
优选地，所述改性烟草、果胶、发泡剂、雾化剂和香精粉的质量比为(5～7)：(0.1～2)：(0.1～1)：(1～5)：(1～2)。Preferably, the mass ratio of the modified tobacco, pectin, foaming agent, atomizing agent and essence powder is (5-7):(0.1-2):(0.1-1):(1-5): (1~2).
更优选地，所述改性烟草、果胶、发泡剂、雾化剂和香精粉的质量比为5：(0.1～0.5)：(0.1～0.5)：(3～5)：(1～2)。More preferably, the mass ratio of the modified tobacco, pectin, foaming agent, atomizing agent and essence powder is 5: (0.1-0.5): (0.1-0.5): (3-5): (1-0.5): 2).
优选地，所述改性烟草是指对烟草进行膨胀或者造孔处理后所得到的烟草，其目的是提高烟草中的空隙率，增强对雾化剂的吸附能力；所述烟草选自烤烟、香料烟、白肋烟、晾晒烟、烟草薄片中的一种。其中，膨胀处理主要采用传统的烟草膨胀烟丝使用的工艺；造孔处理主要是通过使烟草吸附发泡剂溶液，然后进行干燥处理，由于干燥处理的温度为100℃以上，发泡剂会受热分解，产生气体，气体逸出时烟草内部会造成孔微观隙。Preferably, the modified tobacco refers to the tobacco obtained after the tobacco is expanded or pore-forming, the purpose of which is to increase the porosity in the tobacco and enhance the adsorption capacity of the aerosol; the tobacco is selected from flue-cured tobacco, One of oriental tobacco, burley tobacco, air-cured tobacco, and tobacco flakes. Among them, the expansion treatment mainly adopts the traditional process of tobacco expanded shredded tobacco; the pore-forming treatment mainly uses the tobacco to absorb the foaming agent solution, and then performs drying treatment. Since the temperature of the drying treatment is above 100°C, the foaming agent will be decomposed by heat. , gas is generated, and when the gas escapes, pores and microscopic pores will be formed inside the tobacco.
更优选地，所述改性烟草的制备方法为：将烟草与碳酸氢钠水溶液混合，密封存放，然后进行热处理，处理结束后获得改性烟草。优选地，碳酸氢钠水溶液与烟草的质量比为(0.1～1)：1。优选地，碳酸氢钠水溶液的质量分数为1％～15％。优选地，密封存放时间为1h～360h，密封存放温度不大于35℃。优选地，热处理温度为130～170℃，处理时间为10min～120min。More preferably, the preparation method of the modified tobacco is as follows: mixing the tobacco with an aqueous solution of sodium bicarbonate, storing it in a sealed manner, and then performing heat treatment, and obtaining the modified tobacco after the treatment. Preferably, the mass ratio of sodium bicarbonate aqueous solution to tobacco is (0.1-1):1. Preferably, the mass fraction of the aqueous sodium bicarbonate solution is 1% to 15%. Preferably, the sealed storage time is 1 h to 360 h, and the sealed storage temperature is not higher than 35°C. Preferably, the heat treatment temperature is 130-170° C., and the treatment time is 10 min-120 min.
更优选地，碳酸氢钠水溶液与烟草的质量比为(0.5～1)：1。碳酸氢钠水溶液的质量分数为10％～15％。密封存放时间为1d～7d，密封存放温度20℃～30℃。热处理温度为130～170℃，处理时间为10min～120min。More preferably, the mass ratio of sodium bicarbonate aqueous solution to tobacco is (0.5-1):1. The mass fraction of the sodium bicarbonate aqueous solution is 10% to 15%. The sealed storage time is 1d to 7 days, and the sealed storage temperature is 20°C to 30°C. The heat treatment temperature is 130-170°C, and the treatment time is 10min-120min.
优选地，所述果胶是烟草的细胞壁组成成分，根据文献报道，果胶占烟草的质量百分比约为5％～9％之间。本发明中采用烟草的组成物质果胶作为粘接剂，可以尽可能的不引入新的物质，有利于维持烟草加热时的口味。本发明中所选用果胶为食品级果胶，可通过一般商业手段获得。Preferably, the pectin is a cell wall component of tobacco, and according to literature reports, the pectin accounts for about 5%-9% by mass of tobacco. In the present invention, pectin, a component substance of tobacco, is used as the binder, so that no new substances are introduced as much as possible, which is beneficial to maintaining the taste of tobacco when it is heated. The pectin selected in the present invention is food-grade pectin, which can be obtained by general commercial means.
优选地，所述发泡剂主要以固体形态进行施加，选自碳酸氢钠、碳酸氨中的一种或两种。Preferably, the blowing agent is mainly applied in solid form, and is selected from one or both of sodium bicarbonate and ammonium carbonate.
优选地，所述雾化剂为多元醇。所述雾化剂能够使使用者获得更多的烟雾感。Preferably, the atomizing agent is polyhydric alcohol. The atomizing agent can enable users to obtain more smoke sensation.
更优选地，所述多元醇选自丙三醇(甘油)、丙二醇、丁二醇、丁三醇中的一种或多种。More preferably, the polyhydric alcohol is selected from one or more of glycerol (glycerol), propylene glycol, butanediol, and butanetriol.
优选地，所述香精粉选自天然香精粉、烟草用香精粉中的一种或两种。更优选地，所述香精粉可选自可可粉、薄荷粉、干燥的烟草提取物粉、香豆素、香兰素、坚果粉、花粉的一种或多种。其中，所述干燥的烟草提取物粉是指将通过一般商业手段获得的烟草提取物进行干燥后所获得的烟草提取物粉。所述烟草提取物可以是购于曼氏(ManeSA)集团、华宝食用香精香料有限公司的不同种类的烟草提取物。Preferably, the flavor powder is selected from one or both of natural flavor powder and tobacco flavor powder. More preferably, the flavor powder can be selected from one or more of cocoa powder, peppermint powder, dried tobacco extract powder, coumarin, vanillin, nut powder, and pollen. Wherein, the dried tobacco extract powder refers to the tobacco extract powder obtained by drying the tobacco extract obtained by general commercial means. The tobacco extracts can be different types of tobacco extracts purchased from ManeSA Group and Huabao Food Flavors and Fragrances Co., Ltd.
本发明还公开了如上述所述发烟制品的制备方法，将改性烟草、果胶、发泡剂和香精粉混合均匀，然后加入雾化剂混合均匀。The invention also discloses a method for preparing a smoking product as described above. The modified tobacco, pectin, foaming agent and essence powder are uniformly mixed, and then an atomizing agent is added and mixed uniformly.
优选地，所述发烟制品的制备方法还包括吸湿处理步骤，将混合均匀的物料放置在恒温恒湿条件下进行吸湿处理，温度为18～35℃，相对湿度为70％～90％，放置时间为2h～24h。Preferably, the preparation method of the smoking article further includes a moisture absorption treatment step, placing the uniformly mixed material under constant temperature and humidity conditions for moisture absorption treatment, the temperature is 18-35°C, and the relative humidity is 70%-90%. The time is 2h ~ 24h.
更优选地，恒温恒湿条件为：温度为25～30℃，相对湿度为75～90％，放置时间为4～8h。More preferably, the constant temperature and humidity conditions are as follows: the temperature is 25-30° C., the relative humidity is 75-90%, and the standing time is 4-8 hours.
优选地，所述发烟制品的制备方法还包括成型步骤和酥松处理步骤。Preferably, the manufacturing method of the smoking article further includes a shaping step and a crispy treatment step.
更优选地，成型步骤是指将混合后的物料或经过吸湿处理后的物料用模具成型。进一步地，为了提高成型体致密度和强度，也可配套使用挤出机。优选地，挤出机可以是螺杆挤出机或液压机。优选地，成型后获得成型体的形状可以是圆柱体或长方体。更优选地，成型体中间有孔洞，可以供抽吸时的气流通过，使抽吸阻力减小。本发明中孔洞只需保证在气流通过方向上贯通即可，没有形状或位置的要求，可以按需选用具有合适孔洞的模具进行成型。More preferably, the forming step refers to forming the mixed material or the material after moisture absorption treatment with a mold. Further, in order to improve the density and strength of the molded body, an extruder can also be used in conjunction with it. Preferably, the extruder may be a screw extruder or a hydraulic press. Preferably, the shape of the molded body obtained after molding may be a cylinder or a cuboid. More preferably, there is a hole in the middle of the molded body, which can allow the airflow during suction to pass through, so as to reduce the suction resistance. In the present invention, the hole only needs to be ensured to pass through in the direction of air flow, and there is no requirement for shape or position, and a mold with a suitable hole can be selected for molding as required.
更优选地，酥松处理是指经过成型步骤获得的成型体，在一定热处理条件下进行酥松处理，其作用是增加物料间的空隙率，使得抽吸发烟制品时烟雾更容易逸出，而且还进一步干燥物料中的水分。优选地，酥松处理的温度条件为110℃～200℃，时间为10min～120min。更优选的酥松处理的温度条件为130℃～170℃，时间为15min～30min。More preferably, the crisp treatment refers to the molded body obtained through the molding step. The crisp treatment is performed under certain heat treatment conditions. Further dry the moisture in the material. Preferably, the temperature condition of the crisping treatment is 110° C. to 200° C., and the time is 10 minutes to 120 minutes. More preferably, the temperature condition of the crisping treatment is 130° C. to 170° C. and the time is 15 minutes to 30 minutes.
本发明第三方面还提供了如上述所述发烟制品在加热不燃烧型卷烟中的用途。本发明所述的发烟制品，在加热不燃烧型卷烟领域中，将发烟制品加入到加热不燃烧装置中，在150℃～400℃温度下加热使用。The third aspect of the present invention also provides the use of the aforementioned smoking article in heat-not-burn cigarettes. In the field of heat-not-burn cigarettes, the smoking product described in the present invention is used by adding the smoking product into a heat-not-burn device and heating it at a temperature of 150°C to 400°C.
如上所述，本发明提供的一种发烟制品及其制备方法，制备获得的发烟制品具有很大的雾化剂吸附量，粘接剂采用烟草中含量较多的果胶不会引入杂味，利于保持烟草原味，采用的香精粉(传统采用香精溶液)能够有效增大香气量，而发泡剂可以改善发烟制品的微观结构，易于雾化剂和烟草香味成分的加热逸出。As mentioned above, the present invention provides a smoking product and its preparation method. The prepared smoking product has a large amount of atomizing agent adsorption, and the pectin with a large content in tobacco is used as the binder without introducing impurities. Flavor, which is beneficial to maintain the original flavor of tobacco, the flavor powder used (traditionally used flavor solution) can effectively increase the amount of aroma, and the foaming agent can improve the microstructure of smoking products, and facilitate the heating and escape of atomizers and tobacco flavor components.
总之，本发明所提供的发烟制品具有较大的发烟量，且没有杂味、刺激性小，香气风格保持了烟草本香，香气浓郁；本发明制备的发烟制品制成一体化构造，应用于加热不燃烧型烟草制品，方便置入和取出加热不燃烧装置，也不会产生粉末和颗粒，便于清洁。本发明所述的制备方法有别于已披露的制备方法，简便易行，效果显著。In a word, the smoking product provided by the present invention has a large amount of smoke, has no miscellaneous smell, is less irritating, and maintains the aroma style of tobacco, and has a strong aroma; the smoking product prepared by the present invention is made into an integrated structure , Applied to heat-not-burn tobacco products, it is convenient to put in and take out the heat-not-burn device, and it will not produce powder and particles, which is easy to clean. The preparation method described in the present invention is different from the disclosed preparation methods, and is simple and easy to implement and has remarkable effect.
具体实施方式detailed description
以下由特定的具体实施例说明本发明的实施方式，熟悉此技术的人士可由本说明书所揭露的内容轻易地了解本发明的其他优点及功效。The implementation of the present invention will be illustrated by specific specific examples below, and those skilled in the art can easily understand other advantages and effects of the present invention from the contents disclosed in this specification.
在进一步描述本发明具体实施方式之前，应理解，本发明的保护范围不局限于下述特定的具体实施方案；还应当理解，本发明实施例中使用的术语是为了描述特定的具体实施方案，而不是为了限制本发明的保护范围。下列实施例中未注明具体条件的试验方法，通常按照常规条件，或者按照各制造商所建议的条件。Before further describing the specific embodiments of the present invention, it should be understood that the protection scope of the present invention is not limited to the following specific specific embodiments; it should also be understood that the terms used in the examples of the present invention are to describe specific specific embodiments, It is not intended to limit the protection scope of the present invention. The test methods for which specific conditions are not indicated in the following examples are usually in accordance with conventional conditions, or in accordance with the conditions suggested by each manufacturer.
当实施例给出数值范围时，应理解，除非本发明另有说明，每个数值范围的两个端点以及两个端点之间任何一个数值均可选用。除非另外定义，本发明中使用的所有技术和科学术语与本技术领域技术人员通常理解的意义相同。除实施例中使用的具体方法、设备、材料外，根据本技术领域的技术人员对现有技术的掌握及本发明的记载，还可以使用与本发明实施例中所述的方法、设备、材料相似或等同的现有技术的任何方法、设备和材料来实现本发明。When the examples give numerical ranges, it should be understood that, unless otherwise stated in the present invention, the two endpoints of each numerical range and any value between the two endpoints can be selected. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art. In addition to the specific methods, equipment, and materials used in the embodiments, according to those skilled in the art's grasp of the prior art and the description of the present invention, the methods, equipment, and materials described in the embodiments of the present invention can also be used Any methods, apparatus and materials of the prior art similar or equivalent to the practice of the present invention.
实施例1Example 1
本实施例中，将50g碳酸氢钠溶解于450g水中，然后加入500g云南烤烟烟粉，混合均匀后在25℃条件下密封存放3天，然后于130℃的鼓风干燥箱中进行鼓风干燥1h，制得改性烟草A。In this example, 50g of sodium bicarbonate was dissolved in 450g of water, then 500g of Yunnan flue-cured tobacco powder was added, after mixing evenly, it was sealed and stored at 25°C for 3 days, and then blast-dried in a blast drying oven at 130°C 1h, Modified Tobacco A was prepared.
将500g改性烟草、25g果胶、50g碳酸氢钠和100g香兰素混合均匀后，加入200g甘油均匀混合制得固液混合物。将固液混合物放置于25℃、相对湿度90％的恒温恒湿环境中6h。将吸湿处理后的物料放入模具中，挤成直径7mm、长16mm的圆柱体。然后将圆柱体放置于130℃的鼓风干燥箱中鼓风干燥30分钟。最终制得发烟制品AA。After 500g of modified tobacco, 25g of pectin, 50g of sodium bicarbonate and 100g of vanillin are uniformly mixed, 200g of glycerin is added and uniformly mixed to prepare a solid-liquid mixture. The solid-liquid mixture was placed in a constant temperature and humidity environment at 25° C. and a relative humidity of 90% for 6 hours. The material after the moisture absorption treatment is put into a mold and extruded into a cylinder with a diameter of 7 mm and a length of 16 mm. Then the cylinder was placed in a blast drying oven at 130° C. for 30 minutes by blast drying. The smoking article AA is finally produced.
本实施例制得的发烟制品为直径为7mm，长度为16mm的圆柱形发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至150℃，即可抽吸烟气。The smoking product prepared in this example is a cylindrical smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, and the heating function is activated , heated to 150 ° C, you can smoke the gas.
抽吸烟气有明显的烟草本香，香气浓郁，烟雾量充足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has obvious tobacco aroma, strong aroma, and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be produced, and it will not cause pollution to the device.
实施例2Example 2
在本实施例中，将5g碳酸氢钠溶解于495g水中，然后加入2000g白肋烟烟粉，混合均匀后在30℃条件下密封存放1天，然后于200℃的鼓风干燥箱中进行鼓风干燥10分钟，制得改性烟草B。In this example, 5 g of sodium bicarbonate was dissolved in 495 g of water, and then 2000 g of Burley tobacco powder was added, mixed evenly, and sealed and stored at 30°C for 1 day, and then dried in a blast drying oven at 200°C. Air-dried for 10 minutes to obtain Modified Tobacco B.
将500g改性烟草、10g果胶、50g碳酸氢钠和200g可可粉混合均匀后，加入100g甘油均匀混合制得固液混合物。将固液混合物放置于25℃、相对湿度90％环境中6h。将吸湿处理后的物料放入模具中，挤成直径7mm、长16mm，且内部开4个1mm孔的圆柱体。最后将圆柱体放置于170℃的鼓风干燥箱中鼓风干燥15分钟。最终制得发烟制品BB。After 500g of modified tobacco, 10g of pectin, 50g of sodium bicarbonate and 200g of cocoa powder are uniformly mixed, 100g of glycerin is added and uniformly mixed to obtain a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 25° C. and a relative humidity of 90% for 6 hours. Put the moisture-absorbing material into a mold, and extrude it into a cylinder with a diameter of 7mm and a length of 16mm, and four holes of 1mm inside. Finally, the cylinder was placed in a blast drying oven at 170° C. for 15 minutes by blast drying. Finally, a smoking article BB is produced.
本实施例制得的发烟制品为直径为7mm，长度为16mm的圆柱形发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至200℃，即可抽吸烟气。The smoking product prepared in this example is a cylindrical smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, and the heating function is activated , heated to 200 ° C, you can smoke the gas.
抽吸烟气有明显的烟草本香，香气浓郁，烟雾量充足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has obvious tobacco aroma, strong aroma, and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be produced, and it will not cause pollution to the device.
实施例3Example 3
将75g碳酸氢钠溶解于425g水中，然后加入5000g巴西烤烟烟粉，混合均匀后在25℃条件下密封存放3天，然后于150℃的鼓风干燥箱中进行鼓风干燥1.5h，制得改性烟草C。Dissolve 75g of sodium bicarbonate in 425g of water, then add 5000g of Brazilian flue-cured tobacco powder, mix well, store in a sealed container at 25°C for 3 days, and then carry out blast drying in a blast drying oven at 150°C for 1.5h to obtain Modified Tobacco C.
将500g改性烟草、200g果胶、50g碳酸氢钠和100g茉莉花粉混合均匀后，加入100g甘油均匀混合制得固液混合物。将固液混合物放置于28℃、相对湿度75％环境中8h。将吸湿处理后的物料加入模具中，挤成长宽高分别为10mm*10mm*1mm的长方体。最后将长方体放置于130℃的鼓风干燥箱中鼓风干燥30分钟，最终制得发烟制品CC。After 500g of modified tobacco, 200g of pectin, 50g of sodium bicarbonate and 100g of jasmine powder were mixed uniformly, 100g of glycerin was added and uniformly mixed to obtain a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 28° C. and a relative humidity of 75% for 8 hours. Add the moisture-absorbing material into the mold and extrude it into a cuboid whose length, width and height are 10mm*10mm*1mm respectively. Finally, the cuboid was placed in a blast drying oven at 130° C. for 30 minutes to be blast-dried to finally obtain a smoking product CC.
本实施例制得的发烟制品为10mm*10mm*1mm的长方体发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至400℃，即可抽吸烟气。The smoking product prepared in this example is a cuboid smoking body of 10mm*10mm*1mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, the heating function is activated, and heated to 400 ℃, you can smoke the gas.
抽吸烟气有明显的类似传统烟气的感觉，香气浓郁，烟雾量充足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has an obvious feeling similar to traditional smoke, with strong aroma and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be generated, and it will not cause pollution to the device. .
实施例4Example 4
将50g碳酸氢钠溶解于450g水中，然后加入500g云南烤烟烟粉，混合均匀后在25℃条件下密封存放3天，然后于110℃的鼓风干燥箱中进行鼓风干燥2h，制得改性烟草D。Dissolve 50g of sodium bicarbonate in 450g of water, then add 500g of Yunnan flue-cured tobacco powder, mix well, store in a sealed container at 25°C for 3 days, and then dry in a blast drying oven at 110°C for 2 hours to obtain the modified Sexual Tobacco D.
将500g改性烟草、25g果胶、40g碳酸铵和100g薄荷粉混合均匀后，加入200g丙二醇均匀混合制得固液混合物。将固液混合物放置于30℃、相对湿度80％环境中4h。将吸湿处理后的物料加入模具中，挤成直径7mm、长16mm的圆柱体。最后将圆柱体放置于130℃的鼓风干燥箱中鼓风干燥30分钟。最终制得发烟制品DD。After mixing 500g of modified tobacco, 25g of pectin, 40g of ammonium carbonate and 100g of mint powder evenly, add 200g of propylene glycol and mix evenly to prepare a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 30° C. and a relative humidity of 80% for 4 hours. Add the moisture-absorbing material into the mold and extrude it into a cylinder with a diameter of 7 mm and a length of 16 mm. Finally, the cylinder was placed in a blast drying oven at 130° C. for 30 minutes by blast drying. A smoking article DD is finally produced.
本实施例制得的发烟制品为直径为7mm，长度为16mm的圆柱形发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至400℃，即可抽吸烟气。The smoking product prepared in this example is a cylindrical smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, and the heating function is activated , heated to 400 ° C, you can smoke the gas.
抽吸烟气有明显的类似传统烟气的感觉，香气浓郁，烟雾量较足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has an obvious feeling similar to traditional smoke, with strong aroma and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be generated, which will not cause damage to the device. pollute.
实施例5Example 5
将5g碳酸氢钠溶解于495g水中，然后加入5000g山东烤烟烟粉，混合均匀后在18℃条件下密封存放30天，然后于110℃的鼓风干燥箱中进行鼓风干燥2h，制得改性烟草E。Dissolve 5g of sodium bicarbonate in 495g of water, then add 5000g of Shandong flue-cured tobacco powder, mix evenly, store in sealed condition at 18°C for 30 days, and then carry out blast drying in a blast drying oven at 110°C for 2 hours to obtain the modified Sexual Tobacco E.
将500g改性烟草、10g果胶、10g碳酸氢钠和50g罗汉果粉及50g可可粉混合均匀后，加入100g甘油均匀混合制得固液混合物。将固液混合物放置于18℃、相对湿度70％环境中24h。将吸湿处理后的物料加入模具中，挤成直径7mm、长16mm的圆柱体。最后将圆柱体放置于110℃的鼓风干燥箱中鼓风干燥2h。最终制得发烟制品EE。500g of modified tobacco, 10g of pectin, 10g of sodium bicarbonate, 50g of Momordica grosvenori powder and 50g of cocoa powder were uniformly mixed, and then 100g of glycerin was added and uniformly mixed to obtain a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 18° C. and a relative humidity of 70% for 24 hours. Add the moisture-absorbing material into the mold and extrude it into a cylinder with a diameter of 7 mm and a length of 16 mm. Finally, the cylinder was placed in a blast drying oven at 110° C. for 2 h. Finally, the smoking article EE is obtained.
本实施例制得的发烟制品为直径为7mm，长度为16mm的圆柱形发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至400℃，即可抽吸烟气。The smoking product prepared in this example is a cylindrical smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, and the heating function is activated , heated to 400 ° C, you can smoke the gas.
抽吸烟气有明显的类似传统烟气的感觉，香气浓郁，烟雾量较足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has an obvious feeling similar to traditional smoke, with strong aroma and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be generated, which will not cause damage to the device. pollute.
实施例6Example 6
将75g碳酸氢钠溶解于425g水中，然后加入500g晒烟烟粉，混合均匀后在35℃条件下密封存放1h，然后于200℃的鼓风干燥箱中进行鼓风干燥5min，制得改性烟草F。Dissolve 75g of sodium bicarbonate in 425g of water, then add 500g of sun-cured tobacco powder, mix evenly, store in a sealed container at 35°C for 1 hour, then dry in a blast drying oven at 200°C for 5 minutes to obtain the modified Tobacco F.
将700g改性烟草、200g果胶、100g碳酸氢钠和200g烤烟提取物粉混合均匀后，加入200g丁三醇和300g甘油均匀混合制得固液混合物。将固液混合物放置于35℃、相对湿度90％环境中2h。将吸湿处理后的物料加入模具中，挤成直径5mm、长10mm的圆柱体。最后将圆柱体放置于200℃的鼓风干燥箱中鼓风干燥10分钟。最终制得发烟制品FF。After mixing 700g of modified tobacco, 200g of pectin, 100g of sodium bicarbonate and 200g of flue-cured tobacco extract powder evenly, add 200g of butanetriol and 300g of glycerin and mix evenly to prepare a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 35° C. and a relative humidity of 90% for 2 hours. Add the moisture-absorbing material into the mold and extrude it into a cylinder with a diameter of 5 mm and a length of 10 mm. Finally, the cylinder was placed in a blast drying oven at 200° C. for 10 minutes to be air-dried. Finally, the smoking article FF is obtained.
本实施例制得的发烟制品为直径为7mm，长度为16mm的圆柱形发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至400℃，即可抽吸烟气。The smoking product prepared in this example is a cylindrical smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, and the heating function is activated , heated to 400 ° C, you can smoke the gas.
抽吸烟气有明显的类似传统烟气的感觉，香气浓郁，烟雾量充足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has an obvious feeling similar to traditional smoke, with strong aroma and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be generated, and it will not cause pollution to the device. .
实施例7Example 7
将5g碳酸氢钠溶解于495g水中，然后加入1000g山东烤烟烟粉，混合均匀后在20℃条件下密封存放7天，然后于170℃的鼓风干燥箱中进行鼓风干燥2h，制得改性烟草G。Dissolve 5g of sodium bicarbonate in 495g of water, then add 1000g of Shandong flue-cured tobacco powder, mix evenly, store in a sealed container at 20°C for 7 days, and then carry out blast drying in a blast drying oven at 170°C for 2 hours to obtain the modified Sexual Tobacco G.
将500g改性烟草、20g果胶、10g碳酸氢钠和50g香兰素和50g烤烟提取物粉混合均匀后，加入150g甘油均匀混合制得固液混合物。将固液混合物放置于18℃、相对湿度70％环境中24h。将吸湿处理后的物料加入模具中，挤成直径7mm、长16mm的圆柱体。最后将圆柱体放置于150℃的鼓风干燥箱中鼓风干燥30分钟。最终制得发烟制品GG。After 500g of modified tobacco, 20g of pectin, 10g of sodium bicarbonate, 50g of vanillin and 50g of flue-cured tobacco extract powder were mixed evenly, 150g of glycerin was added and evenly mixed to prepare a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 18° C. and a relative humidity of 70% for 24 hours. Add the moisture-absorbing material into the mold and extrude it into a cylinder with a diameter of 7 mm and a length of 16 mm. Finally, the cylinder was placed in a blast drying oven at 150° C. for 30 minutes by blast drying. Finally, the smoking product GG is obtained.
本实施例制得的发烟制品为直径为7mm，长度为16mm的圆柱形发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至300℃，即可抽吸烟气。The smoking product prepared in this example is a cylindrical smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, the heating tank is sealed, and the heating function is activated , heated to 300 ° C, you can smoke the gas.
抽吸烟气有明显的烟草本香，香气浓郁，烟雾量充足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has obvious tobacco aroma, strong aroma, and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be produced, and it will not cause pollution to the device.
实施例8Example 8
将60g碳酸氢钠溶解于440g水中，然后加入1000g晒烟烟粉，混合均匀后在35℃条件下密封存放2h，然后于200℃的鼓风干燥箱中进行鼓风干燥10min，制得改性烟草H。Dissolve 60g of sodium bicarbonate in 440g of water, then add 1000g of sun-cured tobacco powder, mix well, store in a sealed container at 35°C for 2 hours, then dry in a blast drying oven at 200°C for 10min to obtain the modified Tobacco H.
将600g改性烟草、200g果胶、100g碳酸铵和100g香兰素、50g烤烟提取物粉和50g可可粉混合均匀后，加入200g甘油和100g丙二醇均匀混合制得固液混合物。将固液混合物放置于35℃、相对湿度90％环境中2h。将吸湿处理后的物料加入模具(模具上设有20个孔)中，挤成长宽高分别为10mm*10mm*1mm的长方体，其中长方体高度方向开20个0.5mm的孔。最后将长方体放置于170℃的鼓风干燥箱中鼓风干燥30分钟。最终制得发烟制品HH。After mixing 600g of modified tobacco, 200g of pectin, 100g of ammonium carbonate, 100g of vanillin, 50g of flue-cured tobacco extract powder and 50g of cocoa powder, add 200g of glycerin and 100g of propylene glycol and mix evenly to prepare a solid-liquid mixture. The solid-liquid mixture was placed in an environment of 35° C. and a relative humidity of 90% for 2 hours. Add the moisture-absorbing material into a mold (20 holes are provided on the mold), and extrude a cuboid whose length, width and height are 10mm*10mm*1mm respectively, wherein 20 holes of 0.5mm are opened in the height direction of the cuboid. Finally, the cuboid was placed in a blast drying oven at 170° C. for 30 minutes by blast drying. The smoking article HH is finally produced.
本实施例制得的发烟制品为直径为7mm，长度为16mm的长方体发烟体，将其用作芯棒置于加热不燃烧香烟的加热腔体中，封盖加热槽，启动加热功能，加热至250℃，即可抽吸烟气。The smoking product prepared in this example is a cuboid smoking body with a diameter of 7 mm and a length of 16 mm, which is used as a mandrel and placed in the heating chamber of a heat-not-burn cigarette, and the heating tank is sealed to start the heating function. Heating to 250 ° C, you can smoke the gas.
抽吸烟气有明显的烟草本香，香气浓郁，烟雾量充足，抽吸结束后，发烟制品取出加热不燃烧装置时，不会产生粉末或颗粒，不会造成对装置的污染。Smoking smoke has obvious tobacco aroma, strong aroma, and sufficient smoke volume. After smoking, when the smoking product is taken out of the heat-not-burn device, no powder or particles will be produced, and it will not cause pollution to the device.
对比例1Comparative example 1
制备方法同实施例1，与实施例1不同的是，对比例1中加入烟草500g、25gCMC(羧甲基纤维素)、50g碳酸氢钠、100g香兰素和200g甘油。The preparation method is the same as in Example 1, except that in Comparative Example 1, 500 g of tobacco, 25 g of CMC (carboxymethylcellulose), 50 g of sodium bicarbonate, 100 g of vanillin and 200 g of glycerin were added.
对比例1制得发烟制品加入加热不燃烧装置抽吸时，与实施例1相比，对比例1的烟雾量不足，烟草本香也稍有欠缺，且出现明显的难闻气味(类似塑料烧烤味)。When the smoking article prepared in Comparative Example 1 was added to the heat-not-burn device for smoking, compared with Example 1, the amount of smoke in Comparative Example 1 was insufficient, and the original fragrance of tobacco was also slightly lacking, and an obvious unpleasant smell (similar to plastic BBQ smell).
对比例2Comparative example 2
制备方法同实施例1，与实施例1不同的是，对比例2中加入烟草500g、25g果胶、100g香兰素和200g甘油。The preparation method is the same as that of Example 1, and the difference from Example 1 is that 500 g of tobacco, 25 g of pectin, 100 g of vanillin and 200 g of glycerin are added in Comparative Example 2.
对比例2制得发烟制品加入加热不燃烧装置抽吸时，与实施例1相比，对比例2的烟雾量不足。When the smoking article prepared in Comparative Example 2 is added to a heat-not-burn device for smoking, compared with Example 1, the amount of smoke in Comparative Example 2 is insufficient.
对比例3Comparative example 3
制备方法同实施例1，与实施例1不同的是，对比例3中直接加入的烟丝。The preparation method is the same as that of Example 1, and the difference from Example 1 is that the shredded tobacco is directly added in Comparative Example 3.
对比例3制得发烟制品加入加热不燃烧装置抽吸时，与实施例1相比，对比例3的烟雾量不足。When the smoking article prepared in Comparative Example 3 was added to a heat-not-burn device for smoking, compared with Example 1, the amount of smoke in Comparative Example 3 was insufficient.
对比例4Comparative example 4
制备方法同实施例1，与实施例1不同的是，对比例4中直接加入的烟草碎片。The preparation method is the same as that of Example 1, and the difference from Example 1 is that in Comparative Example 4, tobacco chips are added directly.
对比例4制得发烟制品加入加热不燃烧装置抽吸时，与实施例1相比，对比例4的烟雾量不足。When the smoking article prepared in Comparative Example 4 was added to a heat-not-burn device for smoking, compared with Example 1, the amount of smoke in Comparative Example 4 was insufficient.
对比例5Comparative example 5
制备方法同实施例1，与实施例1不同的是，对比例5中直接加入的烟草颗粒。The preparation method is the same as that of Example 1, except that the tobacco particles added directly in Comparative Example 5 are different from Example 1.
对比例5制得发烟制品加入加热不燃烧装置抽吸时，与实施例1相比，对比例5的烟雾量不足。When the smoking article prepared in Comparative Example 5 was added to a heat-not-burn device for smoking, compared with Example 1, the amount of smoke in Comparative Example 5 was insufficient.
对比例6Comparative example 6
制备方法同实施例1，与实施例1不同的是，对比例6中直接加入的烟末。The preparation method is the same as that of Example 1, and the difference from Example 1 is that the tobacco powder directly added in Comparative Example 6.
对比例6制得发烟制品加入加热不燃烧装置抽吸时，与实施例1相比，对比例6的烟雾量不足。When the smoking article prepared in Comparative Example 6 was added to a heat-not-burn device for smoking, compared with Example 1, the amount of smoke in Comparative Example 6 was insufficient.
感官评价试验Sensory Evaluation Test
进一步地，对实施例1-8、对比例1-2中制得的发烟制品加入到加热不燃烧装置中，抽吸进行感官效果评价。Further, the smoking articles prepared in Examples 1-8 and Comparative Examples 1-2 were put into a heat-not-burn device and smoked for sensory evaluation.
感官效果评价方法包括以下步骤：The sensory effect evaluation method includes the following steps:
(1)主要评价指标，包括刺激性、浓度、舒适度、香气风格、香气量和发烟量，并根据各项评价指标对发烟制品感官质量的不同影响程度赋予不同分值。(1) The main evaluation indicators include irritation, concentration, comfort, aroma style, aroma volume and smoke volume, and assign different scores according to the different influence degrees of each evaluation index on the sensory quality of smoking products.
(2)设置9人的评吸员，每人1g发烟制品和一份发烟制品感官质量评价表，采用暗评的评分方式，采用整体循环评吸法，对发烟制品进行抽吸，依据表1中感官质量评价指标评分值的含义，采用百分制评分法对发烟制品的感官质量进行综合评分，各项评价指标按五分、十分制或十五分制评分。发烟制品评价指标的评分值的具体含义见下表1：(2) Set up 9 smoking testers, each with 1g of smoking products and a sensory quality evaluation form of smoking products, adopt the scoring method of dark evaluation, and use the overall cycle evaluation method to smoke smoking products, According to the meanings of the sensory quality evaluation index scores in Table 1, the sensory quality of smoking products is comprehensively scored using the 100-point scoring method, and each evaluation index is scored on a five-point, ten-point or fifteen-point system. The specific meanings of the scoring values of the evaluation indicators of smoking products are shown in Table 1 below:
表1发烟制品感官质量评价指标的评分值含义表Table 1 Score value meaning table of sensory quality evaluation index of smoking products
(3)评价方法：根据表1中的评价指标和评分值，评吸员应对各评价指标进行感官质量评价，并记录其评价结果，评分值的最小计分单位为0.5。(3) Evaluation method: According to the evaluation indicators and scoring values in Table 1, the appraisers should evaluate the sensory quality of each evaluation index and record the evaluation results. The minimum scoring unit of the scoring value is 0.5.
(4)结果统计：所有评吸员的感官质量评价结果中去掉一个最低分和一个最高分，计算剩下有效的单项评价指标评分的算术平均值。(4) Statistics of the results: Remove the lowest score and the highest score from the sensory quality evaluation results of all appraisers, and calculate the arithmetic mean of the remaining effective individual evaluation index scores.
分别对实施例1-8和对比例1制得的发烟制品加入装置中抽吸，进行感官质量评价。具体评价结果见表2，各项指标评价的分值结果为9位评吸员打分的平均值。The smoking articles prepared in Examples 1-8 and Comparative Example 1 were put into the device for smoking, and sensory quality evaluation was performed. The specific evaluation results are shown in Table 2. The score results of each index evaluation are the average of the scores of 9 evaluators.
表2发烟制品的感官效果评价结果Table 2 Evaluation results of sensory effects of smoking products
从表2可以看出，本发明实施例1-8所制备的发烟制品用于加热不燃烧装置中抽吸时，发烟量充足，没有杂味，刺激性小，保持了烟草原味，香气浓郁；发泡剂的加入，更易于雾化剂和烟草香味成分的加热逸出。It can be seen from Table 2 that when the smoking products prepared in Examples 1-8 of the present invention are used for smoking in a heat-not-burn device, the amount of smoke generated is sufficient, there is no miscellaneous smell, the irritation is small, and the original flavor of tobacco is maintained. Full-bodied; the addition of foaming agent makes it easier for the atomizer and tobacco flavor components to escape when heated.
表3发烟制品使用之后器具中残留Table 3 Residues in appliances after use of smoking products
表3可以看出，本发明实施例中所制得的发烟制品为一体化结构，用于加热不燃烧型装置中较方便，抽吸结束后将发烟制品取出后装置内不会有残留。It can be seen from Table 3 that the smoking articles prepared in the examples of the present invention have an integrated structure, which is more convenient for use in heat-not-burn devices, and there will be no residue in the device after the smoking articles are taken out. .
上述实施例仅例示性说明本发明的原理及其功效，而非用于限制本发明。任何熟悉此技术的人士皆可在不违背本发明的精神及范畴下，对上述实施例进行修饰或改变。因此，举凡所属技术领域中具有通常知识者在未脱离本发明所揭示的精神与技术思想下所完成的一切等效修饰或改变，仍应由本发明的权利要求所涵盖。The above-mentioned embodiments only illustrate the principles and effects of the present invention, but are not intended to limit the present invention. Anyone skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Therefore, all equivalent modifications or changes made by those skilled in the art without departing from the spirit and technical ideas disclosed in the present invention should still be covered by the claims of the present invention.
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710954491.7ACN107616541A (en) | 2017-10-13 | 2017-10-13 | A kind of smoking article and its production and use |
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710954491.7ACN107616541A (en) | 2017-10-13 | 2017-10-13 | A kind of smoking article and its production and use |
| Publication Number | Publication Date |
|---|---|
| CN107616541Atrue CN107616541A (en) | 2018-01-23 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710954491.7APendingCN107616541A (en) | 2017-10-13 | 2017-10-13 | A kind of smoking article and its production and use |
| Country | Link |
|---|---|
| CN (1) | CN107616541A (en) |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108477668A (en)* | 2018-03-28 | 2018-09-04 | 湖北中烟工业有限责任公司 | A kind of low temperature cigarette processing method and its application |
| CN108576910A (en)* | 2018-05-09 | 2018-09-28 | 四川三联新材料有限公司 | One kind is for mode of heating smoke gel filter stick and preparation method thereof |
| CN108685154A (en)* | 2018-05-14 | 2018-10-23 | 四川三联新材料有限公司 | Smoking material and preparation method thereof |
| WO2019015339A1 (en)* | 2017-07-21 | 2019-01-24 | 上海新型烟草制品研究院有限公司 | Tobacco material smoke generator for non-burning tobacco, and preparation method and use thereof |
| CN110150763A (en)* | 2019-06-12 | 2019-08-23 | 云南中烟工业有限责任公司 | A pyrolysis porous smoke-generating section, its preparation method and a cigarette containing it |
| CN110150716A (en)* | 2019-05-09 | 2019-08-23 | 安徽中烟工业有限责任公司 | An atomizer for heat-not-burn cigarettes and its application |
| CN110169606A (en)* | 2019-05-31 | 2019-08-27 | 广州市澳键丰泽生物科技股份有限公司 | It is a kind of to heat smoker particles inside and its preparation method and application of not burning |
| CN111838739A (en)* | 2019-04-30 | 2020-10-30 | 贵州中烟工业有限责任公司 | Method for manufacturing heating non-combustion smoke body |
| CN112656024A (en)* | 2020-12-02 | 2021-04-16 | 云南养瑞科技集团有限公司 | Preparation method of cooling and aroma-enhancing particles for HNB (household Natural gas) cigarettes and cooling and aroma-enhancing particles for HNB cigarettes |
| WO2021094453A1 (en)* | 2019-11-14 | 2021-05-20 | Jt International Sa | A method of forming a foam for an aerosol-generating article and a foam thereof |
| WO2022003125A1 (en)* | 2020-07-01 | 2022-01-06 | Jt International Sa | Aerosol-generating substrate comprising granulated flavoured particles |
| CN114668166A (en)* | 2020-12-24 | 2022-06-28 | 湖南中烟工业有限责任公司 | Preparation method of smoking material for heating cigarette and heating cigarette |
| US11712059B2 (en) | 2020-02-24 | 2023-08-01 | Nicoventures Trading Limited | Beaded tobacco material and related method of manufacture |
| US12016369B2 (en) | 2020-04-14 | 2024-06-25 | Nicoventures Trading Limited | Regenerated cellulose substrate for aerosol delivery device |
| CN118805935A (en)* | 2024-08-21 | 2024-10-22 | 湖北中烟工业有限责任公司 | Reconstituted tobacco leaves for heated cigarettes and preparation method thereof |
| US12310394B2 (en) | 2021-07-30 | 2025-05-27 | Nicoventures Trading Limited | Aerosol-generating substrate comprising microcrystalline cellulose |
| US12349719B2 (en) | 2021-03-19 | 2025-07-08 | Nicoventures Trading Limited | Beaded substrates for aerosol delivery devices |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1040134A (en)* | 1988-07-22 | 1990-03-07 | 菲利普莫里斯生产公司 | The thermally releasable flavor source that is used for fume extracting device |
| US5060676A (en)* | 1982-12-16 | 1991-10-29 | Philip Morris Incorporated | Process for making a carbon heat source and smoking article including the heat source and a flavor generator |
| CN1218372A (en)* | 1996-03-07 | 1999-06-02 | 英美烟草(投资)有限公司 | Smokable filler material for smoking articles |
| CN1870913A (en)* | 2003-10-21 | 2006-11-29 | 英美烟草(投资)有限公司 | Smoking articles and smokable filler material therefor |
| CN105249518A (en)* | 2015-09-25 | 2016-01-20 | 安徽中烟工业有限责任公司 | Porous tobacco material for heating non-combustion type cigarettes and preparation method of porous tobacco material |
| CN106136305A (en)* | 2016-07-26 | 2016-11-23 | 上海烟草集团有限责任公司 | A kind of heating tobacco product and preparation method thereof |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5060676A (en)* | 1982-12-16 | 1991-10-29 | Philip Morris Incorporated | Process for making a carbon heat source and smoking article including the heat source and a flavor generator |
| CN1040134A (en)* | 1988-07-22 | 1990-03-07 | 菲利普莫里斯生产公司 | The thermally releasable flavor source that is used for fume extracting device |
| CN1218372A (en)* | 1996-03-07 | 1999-06-02 | 英美烟草(投资)有限公司 | Smokable filler material for smoking articles |
| CN1870913A (en)* | 2003-10-21 | 2006-11-29 | 英美烟草(投资)有限公司 | Smoking articles and smokable filler material therefor |
| CN105249518A (en)* | 2015-09-25 | 2016-01-20 | 安徽中烟工业有限责任公司 | Porous tobacco material for heating non-combustion type cigarettes and preparation method of porous tobacco material |
| CN106136305A (en)* | 2016-07-26 | 2016-11-23 | 上海烟草集团有限责任公司 | A kind of heating tobacco product and preparation method thereof |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019015339A1 (en)* | 2017-07-21 | 2019-01-24 | 上海新型烟草制品研究院有限公司 | Tobacco material smoke generator for non-burning tobacco, and preparation method and use thereof |
| CN108477668A (en)* | 2018-03-28 | 2018-09-04 | 湖北中烟工业有限责任公司 | A kind of low temperature cigarette processing method and its application |
| CN108576910A (en)* | 2018-05-09 | 2018-09-28 | 四川三联新材料有限公司 | One kind is for mode of heating smoke gel filter stick and preparation method thereof |
| CN108685154A (en)* | 2018-05-14 | 2018-10-23 | 四川三联新材料有限公司 | Smoking material and preparation method thereof |
| CN108685154B (en)* | 2018-05-14 | 2021-02-19 | 四川三联新材料有限公司 | Smoking material and method of making same |
| CN111838739A (en)* | 2019-04-30 | 2020-10-30 | 贵州中烟工业有限责任公司 | Method for manufacturing heating non-combustion smoke body |
| CN110150716A (en)* | 2019-05-09 | 2019-08-23 | 安徽中烟工业有限责任公司 | An atomizer for heat-not-burn cigarettes and its application |
| CN110169606A (en)* | 2019-05-31 | 2019-08-27 | 广州市澳键丰泽生物科技股份有限公司 | It is a kind of to heat smoker particles inside and its preparation method and application of not burning |
| CN110169606B (en)* | 2019-05-31 | 2022-05-06 | 广州市澳键丰泽生物科技股份有限公司 | Heating non-combustible fuming particle and preparation method and application thereof |
| CN110150763A (en)* | 2019-06-12 | 2019-08-23 | 云南中烟工业有限责任公司 | A pyrolysis porous smoke-generating section, its preparation method and a cigarette containing it |
| WO2021094453A1 (en)* | 2019-11-14 | 2021-05-20 | Jt International Sa | A method of forming a foam for an aerosol-generating article and a foam thereof |
| US20220386682A1 (en)* | 2019-11-14 | 2022-12-08 | Jt International Sa | A Method of Forming a Foam for an Aerosol-Generating Article and a Foam Thereof |
| US11712059B2 (en) | 2020-02-24 | 2023-08-01 | Nicoventures Trading Limited | Beaded tobacco material and related method of manufacture |
| US12185748B2 (en) | 2020-02-24 | 2025-01-07 | Nicoventures Trading Limited | Beaded tobacco material and related method of manufacture |
| US12016369B2 (en) | 2020-04-14 | 2024-06-25 | Nicoventures Trading Limited | Regenerated cellulose substrate for aerosol delivery device |
| WO2022003125A1 (en)* | 2020-07-01 | 2022-01-06 | Jt International Sa | Aerosol-generating substrate comprising granulated flavoured particles |
| JP2023530605A (en)* | 2020-07-01 | 2023-07-19 | ジェイティー インターナショナル エス．エイ． | Aerosol-generating substrate comprising particulate flavoring particles |
| CN112656024A (en)* | 2020-12-02 | 2021-04-16 | 云南养瑞科技集团有限公司 | Preparation method of cooling and aroma-enhancing particles for HNB (household Natural gas) cigarettes and cooling and aroma-enhancing particles for HNB cigarettes |
| CN112656024B (en)* | 2020-12-02 | 2023-03-14 | 云南养瑞科技集团有限公司 | Preparation method of cooling and aroma-enhancing particles for HNB (household Natural gas) cigarettes and cooling and aroma-enhancing particles for HNB cigarettes |
| CN114668166A (en)* | 2020-12-24 | 2022-06-28 | 湖南中烟工业有限责任公司 | Preparation method of smoking material for heating cigarette and heating cigarette |
| US12349719B2 (en) | 2021-03-19 | 2025-07-08 | Nicoventures Trading Limited | Beaded substrates for aerosol delivery devices |
| US12310394B2 (en) | 2021-07-30 | 2025-05-27 | Nicoventures Trading Limited | Aerosol-generating substrate comprising microcrystalline cellulose |
| CN118805935A (en)* | 2024-08-21 | 2024-10-22 | 湖北中烟工业有限责任公司 | Reconstituted tobacco leaves for heated cigarettes and preparation method thereof |
| Publication | Publication Date | Title |
|---|---|---|
| CN107616541A (en) | A kind of smoking article and its production and use | |
| CN107616540A (en) | A kind of smoking article and its production and use | |
| CN110506977B (en) | Low-temperature non-combustion tobacco particles for cigarettes and preparation method thereof, and smoke body and preparation method thereof | |
| WO2019100545A1 (en) | Low-temperature cigarette and preparation method therefor | |
| CN103750535B (en) | Preparation method of heating non-combustion type cigarette block | |
| WO2019119874A1 (en) | Sucking particle for heat-not-burn cigarette and manufacturing method | |
| CN105249524A (en) | Fragrance type heating nonflammable tobacco product and preparation method thereof | |
| CN105105317A (en) | Strong-flavor type tobacco product being nonflammable while heating and preparation method thereof | |
| CN108713788A (en) | The reconstituted tobacoo and production technology of a kind of high porosity applied to low temperature cigarette | |
| CN107536097B (en) | A kind of preparation method of natural flavor-enhancing cigarette | |
| CN112438424B (en) | Dual-purpose tobacco particles, smoking articles and preparation method thereof | |
| CN108013502B (en) | Chinese flue-cured tobacco efficient atomizing agent and application method thereof | |
| WO2020220502A1 (en) | Cigarette suitable for heat-not-burn device | |
| CN108576912A (en) | The reconstituted tobacoo and its production technology of a kind of metal-containing powders applied to low temperature cigarette | |
| CN111227298A (en) | A kind of preparation method of high-smoke heat-not-burn tobacco smoke bomb | |
| CN110771936A (en) | Tobacco shred and preparation method and application thereof | |
| WO2021063258A1 (en) | Tea-flavored cigarette and electronic cigarette | |
| CN105707980B (en) | Preparation method of cellulose acetate open-cell microporous foam material filter tip spice rod | |
| CN116491684A (en) | Heating non-combustion fuming material | |
| WO2019153885A1 (en) | Cigarette smoke generating carrier for electric heating without burning and preparation method therefor | |
| CN108991591A (en) | The low temperature cigarette and preparation method thereof of micropore tobacco segment with high thermal conductivity | |
| CN210382606U (en) | A thermally decomposed porous smoking section and a cigarette containing the same | |
| CN108741206A (en) | The low temperature cigarette and preparation method of loose integrated tobacco segment with high thermal conductivity | |
| WO2025001518A1 (en) | Reconstituted tobacco leaf, preparation process therefor and heat-not-burn tobacco product | |
| CN103892437B (en) | A kind of production method of novel tobacco goods |
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | Application publication date:20180123 | |
| RJ01 | Rejection of invention patent application after publication |