CN107581655B - Compound sweet-taste-free electronic cigarette tobacco tar and preparation method thereof - Google Patents
Compound sweet-taste-free electronic cigarette tobacco tar and preparation method thereofDownload PDFInfo
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- CN107581655B CN107581655BCN201710756976.5ACN201710756976ACN107581655BCN 107581655 BCN107581655 BCN 107581655BCN 201710756976 ACN201710756976 ACN 201710756976ACN 107581655 BCN107581655 BCN 107581655B
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Abstract
Description
Technical Field
The invention relates to electronic cigarette tobacco tar, in particular to a preparation method of compound sweet-free electronic cigarette tobacco tar.
Background
Electronic cigarettes are cigarette substitutes based on mechanical devices, are generally similar to cigarette appearances, achieve the same sense of feel as cigarettes by simulating cigarette taste and smoking feel, and are generally realized by heating cigarette liquid.
However, the existing electronic cigarette tobacco tar has the following defects:
people have no substantial functional effect when various tastes meet the taste, but the glycerol serving as the main component of the cigarette has sweet taste, the taste of the traditional tobacco is sweet-free, and people always pursue to meet the real cigarette experience of traditional smokers.
Disclosure of Invention
In order to overcome the defects of the prior art, one of the purposes of the invention is to provide the compound type sweet-taste-free electronic cigarette tobacco tar, eleven types of essence absolute oil with fruit fragrance are added into the electronic cigarette tobacco tar, so that the electronic cigarette tobacco tar is cool and cool in taste, full in fruit taste and not greasy after being taken for a long time, has no sweet taste in the electronic cigarette tobacco tar, also has the functions of cooling, refreshing and restoring consciousness, is more similar to the taste of real cigarettes, and is a pure natural and pollution-free food-grade tobacco tar product without adding an industrial preservative in the formula.
The second purpose of the invention is to provide a preparation method of the compound sweet-free electronic cigarette tobacco tar, wherein the vitamin effervescent tablets are fully dissolved, impurities are filtered, and the rest components are added, so that the purity of the electronic cigarette tobacco tar is kept, the preparation steps are simple, and the preparation method is suitable for large-scale industrial production.
One of the purposes of the invention is realized by adopting the following technical scheme:
the compound sweet-free electronic cigarette tobacco tar is prepared from the following components in percentage by mass:
further, the compound sweet-free electronic cigarette tobacco tar is prepared from the following components in percentage by mass:
further, in the cooling agent essence absolute oil, the cooling agent is prepared from the following components in percentage by mass:
further, in the cooling agent essence absolute oil, the cooling agent is prepared from the following components in percentage by mass:
further, in the vitamin effervescent tablet, the vitamin is prepared from the following components in percentage by mass:
further, in the vitamin effervescent tablet, the vitamin is prepared from the following components in percentage by mass:
further, in the sweet taste improver absolute oil, the sweet taste improver is prepared from the following components in percentage by mass:
2- (4-methoxyphenoxy) -propionic acid sodium 30-50%
50 to 70 percent of distilled water.
Further, in the sweet taste improver absolute oil, the sweet taste improver is prepared from the following components in percentage by mass:
2- (4-Methoxyphenoxy) -propionic acid sodium 40%
60% of distilled water.
The second purpose of the invention can be achieved by adopting the following technical scheme:
a preparation method of compound sweet-free electronic cigarette tobacco tar comprises the following steps:
dissolving the effervescent tablets: dissolving the vitamin effervescent tablet in boiling water to obtain primary effervescent liquid; wherein the weight ratio of the vitamin effervescent tablets to the boiling water is 1: (8-20);
and (3) impurity filtering: filtering the effervescent solution by using a filter screen to remove impurities, adding the filtered effervescent solution into propylene glycol, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain an effervescent dissolved solution;
mixing: adding the snow pear essence absolute oil, the sweet grape essence absolute oil, the green grape essence absolute oil, the litchi essence absolute oil, the lemon soda water essence absolute oil, the mint essence absolute oil, the Hami melon essence absolute oil, the watermelon essence absolute oil, the red apple essence absolute oil, the melon essence absolute oil, the ice-cold agent essence absolute oil, the taurine essence absolute oil, the ice mint essence absolute oil, the sweet taste modifier absolute oil and the glycerol into the effervescent dissolving liquid according to the proportion, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain the electronic cigarette oil.
Furthermore, in the impurity filtering step, the aperture of the filter screen is 1000-3000 meshes.
The invention has the beneficial effects that:
1. the electronic cigarette oil is added with eleven types of essence absolute oil with fruit fragrance, so that the electronic cigarette oil is fresh and cool in taste, full in fruit taste and not greasy after being taken for a long time, has no sweet taste, has the functions of cooling and refreshing, is more similar to the taste of a real cigarette, and is a pure natural pollution-free food-grade cigarette oil product without adding an industrial preservative in the formula;
2. according to the preparation method of the compound sweet-free electronic cigarette tobacco tar, the vitamin effervescent tablets are fully dissolved, impurities are filtered, and the rest components are added, so that the purity of the electronic cigarette tobacco tar is kept, the preparation steps are simple, and the preparation method is suitable for large-scale industrial production.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
The compound sweet-free electronic cigarette tobacco tar is prepared from the following components in percentage by mass:
the sum of the mass percentages of the components is 100 percent.
As a further implementation mode, the compound sweet-free electronic cigarette tobacco tar is prepared from the following components in percentage by mass:
the snow pear essence absolute oil is D671110 model produced by De Zhi (Shanghai) limited company.
The sweet grape essence absolute oil is the sweet grape essence absolute oil with the model number of D7635, which is produced by Dezhi (Shanghai) Limited company.
The grape essence absolute oil is the grape essence absolute oil with the model number ZW201636, produced by Shenzhen Palivor Biotech limited company.
The green extracted essential oil is the green extracted essence essential oil with the model of MW1529561 produced by Guangzhou City Huachen essence Co.
The litchi essence absolute oil is H160516, which is produced by Shenzhen Heyao Chuanyuan Biotech limited company.
The lemon essence absolute oil is the lemon essence absolute oil with the model D642212, which is produced by De Zhi (Shanghai) Co.
The lemon soda essence absolute oil is H160215, which is produced by Shenzhen, Hechun creative Biotech limited company.
The peppermint essence absolute oil is produced by Shenzhen Palivor Biotech limited company, and has a model number of ZW 201627.
The hami melon essence absolute oil is produced by Shenzhen pei liwa biotechnology limited company, and the model is the hami melon essence absolute oil of ZW 201614.
The watermelon essence absolute oil is the watermelon essence absolute oil with the model number of H160305 produced by Shenzhen, Hexinyuan Biotech limited company.
The red apple essence absolute oil is the red apple essence absolute oil which is produced by Shenzhen Paliwo biotechnology limited company and has the model number of ZW 201605.
The melon essence absolute oil is produced by Dezhi (Shanghai) Limited and has the model number of D165108.
The cool agent essence absolute oil is the cool agent essence absolute oil which is produced by Shenzhen Paliwo biotechnology limited company and has the model number of ZW 201602.
The taurine essence clean oil is the taurine fragrant essence clean oil with the model number of H170625, which is produced by Shenzhen Heyao Biotech limited company.
The Mentha haplocalyx essence absolute oil is prepared by Shenzhen Palimo Biotech limited company, and has model number ZW201604 Mentha haplocalyx essence absolute oil.
As a further implementation mode, in the cooling agent essence absolute oil, the cooling agent is prepared from the following components in percentage by mass:
the sum of the mass percentages of the components is 100 percent.
As a further implementation mode, in the cooling agent essence absolute oil, the cooling agent is prepared from the following components in percentage by mass:
in a further embodiment, the vitamin effervescent tablet is prepared from the following components in percentage by mass:
the sum of the mass percentages of the components is 100 percent.
In a further embodiment, the vitamin effervescent tablet is prepared from the following components in percentage by mass:
as a further embodiment, in the sweet taste improver absolute oil, the sweet taste improver is prepared from the following components in percentage by mass:
2- (4-methoxyphenoxy) -propionic acid sodium 30-50%
50% -70% of distilled water;
the sum of the mass percentages of the components is 100 percent.
As a further embodiment, in the sweet taste improver absolute oil, the sweet taste improver is prepared from the following components in percentage by mass:
2- (4-Methoxyphenoxy) -propionic acid sodium 40%
60% of distilled water.
The preparation method of the compound sweet-free electronic cigarette tobacco tar comprises the following steps:
dissolving the effervescent tablets: dissolving the vitamin effervescent tablet in boiling water to obtain primary effervescent liquid; wherein the weight ratio of the vitamin effervescent tablets to the boiling water is 1: (8-20);
and (3) impurity filtering: filtering the effervescent solution by using a filter screen to remove impurities, adding the filtered effervescent solution into propylene glycol, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain an effervescent dissolved solution;
mixing: adding the snow pear essence absolute oil, the sweet grape essence absolute oil, the green grape essence absolute oil, the litchi essence absolute oil, the lemon soda water essence absolute oil, the mint essence absolute oil, the Hami melon essence absolute oil, the watermelon essence absolute oil, the red apple essence absolute oil, the melon essence absolute oil, the ice-cold agent essence absolute oil, the taurine essence absolute oil, the ice mint essence absolute oil, the sweet taste modifier absolute oil and the glycerol into the effervescent dissolving liquid according to the proportion, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain the electronic cigarette oil.
In a further embodiment, in the impurity filtering step, the aperture of the filter screen is 1000-3000 mesh.
The following are specific examples of the present invention, and raw materials, equipments and the like used in the following examples can be obtained by purchasing them unless otherwise specified.
Examples 1 to 7:
the compound sweet-free electronic cigarette tobacco tar of the embodiments 1 to 7 is prepared from the following components in percentage by mass (%):
TABLE 1 Components and proportions of examples 1-7
In the cooling agent essence absolute oil of the embodiments 1 to 7, the cooling agent is prepared from the following components in percentage by mass:
in the vitamin effervescent tablets of examples 1 to 7, the vitamins are prepared from the following components in percentage by mass:
in the sweet taste improver absolute oil of examples 1 to 7, the sweet taste improver is prepared from the following components in percentage by mass:
2- (4-Methoxyphenoxy) -propionic acid sodium 40%
60% of distilled water.
The preparation methods of the compound sweet-free electronic cigarette tobacco tar of examples 1 to 7 are all carried out according to the following steps:
dissolving the effervescent tablets: dissolving the vitamin effervescent tablet in boiling water to obtain primary effervescent liquid; wherein the weight ratio of the vitamin effervescent tablets to the boiling water is 1: (8-20);
and (3) impurity filtering: filtering the effervescent solution by using a filter screen to remove impurities, adding the filter screen with the aperture of 1000-3000 meshes into propylene glycol, uniformly stirring at the stirring speed of 280-320r/min for 15-20min to obtain an effervescent solution;
mixing: adding the snow pear essence absolute oil, the sweet grape essence absolute oil, the green grape essence absolute oil, the litchi essence absolute oil, the lemon soda water essence absolute oil, the mint essence absolute oil, the Hami melon essence absolute oil, the watermelon essence absolute oil, the red apple essence absolute oil, the melon essence absolute oil, the ice-cold agent essence absolute oil, the taurine essence absolute oil, the ice mint essence absolute oil, the sweet taste modifier absolute oil and the glycerol into the effervescent dissolving liquid according to the proportion, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain the electronic cigarette oil.
Effect evaluation and Performance detection
Subject: the e-cigarette plumes of examples 1-7 were used as test samples.
The experimental contents are as follows: randomly selecting 100 volunteers of smokers, randomly dividing the volunteers into 10 groups, wherein each group comprises 10 persons, the same test sample is used in each group, the use mode is twice a day, and the volunteers are subjected to use evaluation record after ten days; the sensory evaluation comprises ten items, each item is 10 points, the total point is 100 points, and the ten items are respectively the fragrance of fruits, the taste is comfortable, the refreshing and refreshing effects are realized, the refreshing and consciousness restoring effects are realized, the lasting and non-greasy smoking effect is realized, the physical strength is supplemented, the aftertaste is fresh, the stimulation effect is comfortable, the feeling of the real smoke is similar to the feeling of the mouth, and the impact effect of the steam and water is realized; the average scores for examples 1-7 were as follows:
TABLE 2 sensory scores for examples 1-7
As can be seen from Table 2, the effects of examples 1 to 3 are better than those of examples 4 to 7 in the case of examples 1 to 7, wherein example 1 is the most preferable example, while in the case of examples 4 to 7, example 4 is inferior to examples 1 to 3 in terms of mouthfeel, greasy taste and refreshing aftertaste, particularly, too low in similarity to the mouthfeel of real cigarettes, because no sweetness modifier neat oil, taurine flavor neat oil and ice mint flavor neat oil are added, while example 5 is inferior to examples 1 to 3 in the effects of refreshing, greasy taste, stimulating, refreshing aftertaste and feeling upon impact of soda water because no coolness agent flavor neat oil, taurine flavor neat oil and ice mint flavor neat oil are added, and the mixture ratio of examples 6 to 7 is out of the range of the mixture ratio of the present invention, thus each effect is inferior to that of examples 1 to 3, which indicates that eleven fruit flavor neat oils are added to the electronic cigarette oil of the present invention, the electronic cigarette oil has fresh and cool taste, the fruit taste is full and the electronic cigarette oil is not greasy after being taken for a long time, and the electronic cigarette oil has no sweet taste, also has the functions of cooling, refreshing and restoring consciousness, is more similar to the taste of real cigarettes, and is a pure natural pollution-free food-grade cigarette oil product without adding industrial preservatives in the formula.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (3)
1. The compound sweet-free electronic cigarette tobacco tar is characterized by being prepared from the following components in percentage by mass:
in the cooling agent essence absolute oil, a cooling agent is prepared from the following components in percentage by mass:
in the vitamin effervescent tablet, vitamins are prepared from the following components in percentage by mass:
in the sweet improver absolute oil, the sweet improver is prepared from the following components in percentage by mass:
2- (4-Methoxyphenoxy) -propionic acid sodium 40%
60% of distilled water.
2. The preparation method of the compound sweet-free electronic cigarette tobacco tar according to claim 1, characterized by comprising the following steps:
dissolving the effervescent tablets: dissolving the vitamin effervescent tablet in boiling water to obtain primary effervescent liquid; wherein the weight ratio of the vitamin effervescent tablets to the boiling water is 1: (8-20);
and (3) impurity filtering: filtering the effervescent solution by using a filter screen to remove impurities, adding the filtered effervescent solution into propylene glycol, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain an effervescent dissolved solution;
mixing: adding the snow pear essence absolute oil, the sweet grape essence absolute oil, the green grape essence absolute oil, the litchi essence absolute oil, the lemon soda water essence absolute oil, the mint essence absolute oil, the Hami melon essence absolute oil, the watermelon essence absolute oil, the red apple essence absolute oil, the melon essence absolute oil, the ice-cold agent essence absolute oil, the taurine essence absolute oil, the ice mint essence absolute oil, the sweet taste modifier absolute oil and the glycerol into the effervescent dissolving liquid according to the proportion, and uniformly stirring at the stirring speed of 280 plus 320r/min for 15-20min to obtain the electronic cigarette oil.
3. The method for preparing the compound sweet-free electronic cigarette tobacco tar according to claim 2, wherein the compound sweet-free electronic cigarette tobacco tar is prepared by the following steps: in the impurity filtering step, the aperture of the filter screen is 1000-3000 meshes.
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110295087B (en)* | 2019-07-30 | 2022-08-02 | 福建中烟工业有限责任公司 | Hami melon essence and application thereof |
| CN110859316A (en)* | 2019-09-12 | 2020-03-06 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| CN110522070A (en)* | 2019-09-12 | 2019-12-03 | 深圳雾芯科技有限公司 | Flavour compositions and electronic cigarette liquid comprising the flavour compositions |
| CN110558603A (en)* | 2019-09-12 | 2019-12-13 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| CN110959903A (en)* | 2019-09-12 | 2020-04-07 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| CN110638086A (en)* | 2019-09-12 | 2020-01-03 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| CN113615860B (en)* | 2021-08-16 | 2023-09-12 | 深圳市真味生物科技有限公司 | Cool agent for cigarettes and electronic atomized liquid with cool mouthfeel |
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