技术领域technical field
本发明属于卷烟纸技术领域，具体涉及一种润香卷烟纸、其制备方法及用途。The invention belongs to the technical field of cigarette paper, and in particular relates to a fragrance-moisturizing cigarette paper, a preparation method and an application thereof.
背景技术Background technique
卷烟纸属于薄页纸，一般定量在26-34g/m2之间，卷烟纸作为卷烟产品的包装用纸，在烟草工业中占有较重要的地位。卷烟纸一般占卷烟烟支总重量的5％，由于它直接参与燃烧，因而卷烟纸可通过控制烟支的燃烧性和对烟气的稀释作用，来影响卷烟的燃烧性、香味、焦油产生量以及其他的烟气有害成分特别是一氧化碳的产生量。Cigarette paper belongs to thin paper, generally between 26-34g/m2 , cigarette paper, as the packaging paper of cigarette products, occupies an important position in the tobacco industry. Cigarette paper generally accounts for 5% of the total weight of cigarettes. Since it directly participates in combustion, cigarette paper can affect the flammability, flavor, and tar production of cigarettes by controlling the flammability of cigarettes and the dilution of smoke. And other harmful components of smoke, especially the production of carbon monoxide.
传统烟草中经常使用的保润剂大多为甘油、丙二醇、山梨糖醇等多元醇类，属于吸湿保温类物质，此类物质一般是通过吸入环境中的水分来保湿，由于此类物质可以大量的工业化制造，价格低廉，安全性高，所以在卷烟中应用规模较大。但此类保润剂保润效果容易受到环境湿度影响，在不同地域不同温湿度的环境下特别是南方高温高湿的环境下，卷烟容易吸湿，从而造成卷烟烟气谐调性、香气下降，长时间放置由于水分偏高，卷烟甚至会发霉。Moisturizers often used in traditional tobacco are mostly polyols such as glycerin, propylene glycol, and sorbitol, which are hygroscopic and heat-retaining substances. Industrialized manufacturing, low price and high safety, so it is widely used in cigarettes. However, the moisturizing effect of this kind of humectant is easily affected by the environmental humidity. Under the environment of different temperature and humidity in different regions, especially in the environment of high temperature and high humidity in the south, cigarettes are easy to absorb moisture, which will cause the smoke harmony and aroma of cigarettes to decrease, and the long-term Cigarettes may even become moldy due to high moisture content after being left for a long time.
目前卷烟保润主要通过在烟丝、烟用材料中添加保润剂来实现卷烟的保润功能。在烟丝中添加保润剂，虽然可以起到一定的润香作用，但由于不同产地的烟草香气千差万别，保润剂的比例偏大也容易对卷烟烟气感官质量产生一定的负面影响；在烟用材料中的添加目前都是统一添加，没有对烟用材料作针对性的提升，保润剂的施加方式也较单一，主要都是突出“润”而无法实现在“润”的同时修饰卷烟香气、润色烟草本香。At present, the moisturizing function of cigarettes is mainly realized by adding humectants to shredded tobacco and tobacco materials. Adding humectants to shredded tobacco can play a certain role in moisturizing the aroma, but because the aroma of tobacco from different origins varies greatly, a large proportion of humectants is likely to have a certain negative impact on the sensory quality of cigarette smoke; The addition of materials is currently added uniformly, there is no targeted improvement of tobacco materials, and the application method of humectant is relatively simple, mainly highlighting "moistening" and it is impossible to modify cigarettes while "moistening" Aroma, embellished tobacco aroma.
发明内容Contents of the invention
为解决上述问题，本发明在卷烟纸的内、外表面施加不同类型的保润剂，来达到在不同地域不同温湿度的环境下的最佳保润效果；同时在卷烟纸中加入优选复配的烟草提取物，所选的提取物的香气既能较好的协调卷烟香气，又能与卷烟纸的内、外表面施加不同类型的保润剂、以及卷烟纸内的助燃剂较好的匹配和协同，能够起到“润”的同时润饰卷烟香气、润色烟草本香。In order to solve the above problems, the present invention applies different types of humectants to the inner and outer surfaces of the cigarette paper to achieve the best moisturizing effect in different regions and different temperature and humidity environments; Tobacco extract, the aroma of the selected extract can not only better coordinate the aroma of cigarettes, but also better match the different types of humectants applied to the inner and outer surfaces of cigarette paper, and the combustion enhancer in cigarette paper And synergistically, it can "moisturize" and modify the aroma of cigarettes and the original fragrance of tobacco at the same time.
本发明第一方面提供一种润香卷烟纸，所述润香卷烟纸的pH值呈弱碱性，所述润香卷烟纸的内表面含有烟草提取物、第一助燃剂和第一保润剂，外表面含有第二助燃剂和第二保润剂；所述第一保润剂为线性多糖结构物质，所述第二保润剂为多元醇类物质。The first aspect of the present invention provides a flavoring cigarette paper, the pH value of the flavoring cigarette paper is weakly alkaline, and the inner surface of the flavoring cigarette paper contains tobacco extract, a first combustion enhancer and a first moisturizing agent, the outer surface contains a second combustion enhancer and a second humectant; the first humectant is a linear polysaccharide structure substance, and the second humectant is a polyhydric alcohol substance.
优选地，所述线性多糖结构物质为N-已酰氨基葡萄糖或D-葡萄糖醛酸，占所述润香卷烟纸的0.1～1.0wt％；所述多元醇类物质为甘油、丙二醇或山梨糠醇，占所述润香卷烟纸的0.1～1.0wt％。Preferably, the linear polysaccharide structure substance is N-hexanoylglucosamine or D-glucuronic acid, accounting for 0.1-1.0 wt% of the flavoring cigarette paper; the polyol substance is glycerin, propylene glycol or sorbitol , accounting for 0.1-1.0 wt% of the flavoring cigarette paper.
优选地，所述烟草提取物占所述润香卷烟纸的0.1～1.5wt％。Preferably, the tobacco extract accounts for 0.1-1.5 wt% of the flavoring cigarette paper.
优选地，所述烟草提取物为质量比为3:1～1:1的片烟C1F、C2F或C3F提取物和HTMOA、HTMOB或HTMOE烤烟提取物的混合物。Preferably, the tobacco extract is a mixture of leaf tobacco C1F, C2F or C3F extract and HTMOA, HTMOB or HTMOE flue-cured tobacco extract at a mass ratio of 3:1 to 1:1.
优选地，所述第一助燃剂为酒石酸钾钠，占所述润香卷烟纸的比0.1～1.0wt％；所述第二助燃剂为质量比为2:1～1:2柠檬酸钾和柠檬酸钠的混合物，占所述润香卷烟纸的比0.1～1.0wt％。Preferably, the first combustion enhancer is potassium sodium tartrate, accounting for 0.1 to 1.0 wt% of the flavoring cigarette paper; the second combustion enhancer is potassium citrate and potassium citrate with a mass ratio of 2:1 to 1:2 The mixture of sodium citrate accounts for 0.1-1.0 wt% of the flavoring cigarette paper.
优选地，所述润香卷烟纸的pH值为7.1～7.5。Preferably, the pH value of the flavor-moisturizing cigarette paper is 7.1-7.5.
本发明第二方面提供所述的润香卷烟纸的制备方法，包括如下任何顺序或同时进行的步骤：The second aspect of the present invention provides the method for preparing the flavoring cigarette paper, comprising the following steps in any order or simultaneously:
(1)烟草提取物的制备及喷淋：分别将片烟C1F、C2F或C3F和HTMOA、HTMOB或HTMOE烤烟粉碎后，经过超声波提取，再经过醚提取和醇提取，在温度为－30℃～－40℃、真空度为2～8Pa下干燥后即得到所述的烟草提取物；按片烟C1F、C2F或C3F提取物和HTMOA、HTMOB或HTMOE烤烟提取物质量比为3:1～1:1进行复配混合，然后将混合物加入到水中混合均匀，在0℃～40℃下均匀喷淋到卷烟纸内表面；(1) Preparation and spraying of tobacco extract: After crushing sheet tobacco C1F, C2F or C3F and HTMOA, HTMOB or HTMOE flue-cured tobacco, they are subjected to ultrasonic extraction, ether extraction and alcohol extraction, at a temperature of -30 ° C ~ After drying at -40°C and a vacuum degree of 2-8 Pa, the tobacco extract can be obtained; the mass ratio of the tobacco extract C1F, C2F or C3F and the extract of HTMOA, HTMOB or HTMOE flue-cured tobacco is 3:1-1: 1 Carry out compound mixing, then add the mixture into water and mix evenly, and spray evenly on the inner surface of the cigarette paper at 0°C to 40°C;
(2)将第一助燃剂溶解后，加入第一保润剂搅拌均匀，用第一涂布辊涂布在卷烟纸内表面；(2) After dissolving the first combustion enhancer, add the first humectant and stir evenly, and coat the inner surface of the cigarette paper with the first coating roller;
(3)将第二助燃剂溶解后，加入第二保润剂搅拌均匀，用第二涂布辊涂布在卷烟纸外表面。(3) After dissolving the second combustion enhancer, add the second humectant and stir evenly, and coat the outer surface of the cigarette paper with the second coating roller.
本发明第三方面提供所述的的润香卷烟纸用于润饰卷烟香气、润色烟草本香的用途。The third aspect of the present invention provides the use of the flavor-moisturizing cigarette paper for embellishing the aroma of cigarettes and the aroma of tobacco.
相对于现有技术，本发明取得了以下有益效果：Compared with the prior art, the present invention has achieved the following beneficial effects:
(1)本发明利用保润剂的不同作用机理，将第一保润剂和第二保润剂分别施加在润香卷烟纸内表面和外表面，可以更加有效的利用不同的保润机理，使润香卷烟纸内表面保润剂可以锁住烟丝中所含的水分来保持烟丝中水分的稳定，润香卷烟纸外表面的保润剂可以保持润香卷烟纸外表面水分的稳定；从而达到在不同地域、不同温湿度的环境下的卷烟的最佳保润效果。(1) The present invention utilizes different mechanisms of action of humectants to apply the first humectant and the second humectant to the inner surface and outer surface of the flavoring cigarette paper respectively, so that different moisturizing mechanisms can be more effectively utilized, The humectant on the inner surface of the flavoring cigarette paper can lock the moisture contained in the shredded tobacco to keep the moisture in the shredded tobacco stable, and the humectant on the outer surface of the flavoring cigarette paper can keep the moisture on the outer surface of the flavoring cigarette paper stable; thus To achieve the best moisturizing effect of cigarettes in different regions and different temperature and humidity environments.
(2)本发明采用超声波提取方法提取烟草提取物，可以使液体微小气泡爆裂，产生极大的压力，使植物细胞壁及整个生物体的破裂在瞬间完成，缩短了破碎时间；同时超声波产生的振动作用加强了胞内物质的释放、扩散和溶解，从而显著提高提取效率；并且由于采用低温冷冻干燥处理，浓缩时间短、浓缩效率高；另外由于采用低温干燥，避免高温对烟草提取物中有效成分的破坏。另一方面，通过将烟草原料干燥加工为粉末后，既可以最大化保存烟草原料中的香料成分，又可以制备成溶于水的粉末状，方便运输与使用。由于烟草提取物在提取、干燥、溶解、喷淋全过程中温度均较低，对烟草提取物中致香物质的破坏小，从而尽可能地减小了加工过程对烟草提取物中致香成分的影响。(2) The present invention adopts the ultrasonic extraction method to extract the tobacco extract, which can make the micro-bubbles of the liquid burst and generate great pressure, so that the rupture of the plant cell wall and the whole organism is completed in an instant, shortening the crushing time; The effect strengthens the release, diffusion and dissolution of intracellular substances, thereby significantly improving the extraction efficiency; and due to the low-temperature freeze-drying treatment, the concentration time is short and the concentration efficiency is high; in addition, due to the low-temperature drying, high temperature is avoided. destruction. On the other hand, by drying and processing the tobacco raw material into powder, the flavor components in the tobacco raw material can be preserved to the greatest extent, and it can also be prepared into a water-soluble powder, which is convenient for transportation and use. Since the temperature of the tobacco extract is low during the whole process of extraction, drying, dissolution and spraying, the damage to the aromatizing substances in the tobacco extract is small, thereby reducing the processing of the aromatizing components in the tobacco extract as much as possible. Impact.
(3)本发明的烟草提取物的原料采用片烟C1F、C2F或C3F(云南玉溪烟草原料)和HTMOA、HTMOB或HTMOE烤烟(巴西烟草原料)，本发明人意外发现两种原料能够很好的匹配谐调，特别是将两种烟草提取物粉末按质量3:1～1:1进行复配混合添加后，卷烟有较好的吸味，烟草丰富性、协调性有较好的提升，具有有较好的增香、协香功效，能与清香型卷烟风格相匹配且能够更好的谐调卷烟的本香。(3) The raw material of tobacco extract of the present invention adopts sheet tobacco C1F, C2F or C3F (Yunnan Yuxi tobacco raw material) and HTMOA, HTMOB or HTMOE flue-cured tobacco (Brazilian tobacco raw material), and the inventor unexpectedly finds that two kinds of raw materials can be well Matching and harmonizing, especially after the two kinds of tobacco extract powders are compounded and added according to the mass ratio of 3:1 to 1:1, the cigarette has a better smoking taste, and the richness and coordination of tobacco are better improved. It has better flavor-increasing and flavor-associated effects, can match the style of fresh-flavor cigarettes and can better harmonize the original fragrance of cigarettes.
(4)本发明在润香卷烟纸的内、外表面施加不同类型的保润剂，同时在卷烟纸中加入优选复配的烟草提取物，所选的烟草提取物能与卷烟纸的内、外表面施加不同类型的保润剂、以及卷烟纸内的助燃剂较好的匹配和协同，能够起到“润”的同时润饰卷烟香气、润色烟草本香。(4) The present invention applies different types of humectants on the inner and outer surfaces of the fragrant cigarette paper, and simultaneously adds a preferred compound tobacco extract in the cigarette paper, and the selected tobacco extract can be combined with the inside and outside of the cigarette paper. Applying different types of humectant on the outer surface and the better matching and synergy of the combustion enhancer in the cigarette paper can "moisturize" and modify the aroma of cigarettes and the original aroma of tobacco at the same time.
(5)本发明在润香卷烟纸的内、外表面施加不同类型的助燃剂，都是弱的有机酸强碱盐，呈弱碱性，能分别与卷烟纸的内、外表面施加不同类型的保润剂较好的匹配和协同，能够起到“润”的同时润饰卷烟香气、润色烟草本香。(5) The present invention applies different types of combustion accelerants on the inner and outer surfaces of moistening cigarette paper, all of which are weak organic acid strong alkali salts, which are weakly alkaline, and can be applied with different types on the inner and outer surfaces of cigarette paper respectively. The better matching and synergism of the moisturizing agent can "moisturize" and modify the aroma of cigarettes and the original aroma of tobacco at the same time.
(6)本发明的润香卷烟纸可以满足卷烟纸纸张的各项指标，且本发明的润香卷烟纸保润效果好，对卷烟香气具有较好润饰作用，取得了较好的效果。(6) The fragrance-moisturizing cigarette paper of the present invention can meet various indicators of cigarette paper, and the fragrance-moisturizing cigarette paper of the present invention has a good moisture-retaining effect, and has a good embellishment effect on the aroma of cigarettes, and has achieved good results.
(7)本发明的润香卷烟纸制备方法简单，只需对常用的卷烟纸的内外表面进行简单的处理和加工，制备方法工艺简单，成本较低。适宜大规模工业生产应用。(7) The preparation method of the incense-enhancing cigarette paper of the present invention is simple, and only needs to carry out simple treatment and processing on the inner and outer surfaces of commonly used cigarette paper. The preparation method is simple in process and low in cost. Suitable for large-scale industrial production applications.
具体实施方式Detailed ways
实施例1：润香卷烟纸的制备，包括如下3个步骤，该3个步骤可以任何顺序进行或同时进行。Example 1: The preparation of flavoring cigarette paper includes the following three steps, which can be carried out in any order or simultaneously.
(1)分别将片烟C2F(云南玉溪烟草原料)和HTMOA烤烟(巴西烟草原料),经过粉碎研磨，将粉碎后粉末通过超声波提取，然后再经过醚提醇提，经过低温(－30℃～－40℃)真空(2～8帕)冷冻干燥后，即可得到粉末状烟草提取物。按C2F(云南玉溪烟草原料)和HTMOA烤烟(巴西烟草原料)提取物质量比为0.8kg:0.4kg的比例进行复配，然后将烟草提取物加入到水中混合均匀，在0℃～40℃下均匀喷淋到1t卷烟纸内表面。(1) C2F sheet tobacco (Yunnan Yuxi tobacco raw material) and HTMOA flue-cured tobacco (Brazilian tobacco raw material) were crushed and ground respectively, and the pulverized powder was extracted by ultrasonic waves, and then extracted with ether and alcohol, and then subjected to low temperature (-30 ° C ~ -40°C) vacuum (2-8 Pa) and freeze-dried to obtain powdered tobacco extract. According to the mass ratio of C2F (Yuxi tobacco raw material in Yunnan) and HTMOA flue-cured tobacco (Brazilian tobacco raw material) extract mass ratio is 0.8kg:0.4kg, then add the tobacco extract into the water and mix evenly, at 0℃～40℃ Spray evenly onto the inner surface of 1t of cigarette paper.
(2)将助燃剂1kg酒石酸钾钠溶解后，加入1kg的N-已酰氨基葡萄糖搅拌均匀，用第一涂布辊涂布在1t卷烟纸内表面(2) After dissolving 1 kg of potassium sodium tartrate as a combustion aid, add 1 kg of N-caproylglucosamine and stir evenly, and coat the inner surface of 1 ton of cigarette paper with the first coating roller
(3)将助燃剂0.5kg柠檬酸钾和0.5kg柠檬酸钠溶解后，加入1kg的甘油搅拌均匀，用第二涂布辊涂布在1t卷烟纸外表面。(3) After dissolving 0.5 kg of potassium citrate and 0.5 kg of sodium citrate as combustion accelerants, add 1 kg of glycerin and stir evenly, and coat the outer surface of 1 ton of cigarette paper with a second coating roller.
实施例2：润香卷烟纸的制备，包括如下3个步骤，该3个步骤可以任何顺序进行或同时进行。Example 2: The preparation of flavoring cigarette paper includes the following three steps, which can be carried out in any order or simultaneously.
(1)分别将片烟C1F(云南玉溪烟草原料)和HTMOB烤烟(巴西烟草原料),经过粉碎研磨，将粉碎后粉末通过超声波提取，然后再经过醚提醇提，经过低温(－30℃～－40℃)真空(2～8帕)冷冻干燥后，即可得到粉末状烟草提取物。按C1F(云南玉溪烟草原料)和HTMOB烤烟(巴西烟草原料)提取物质量比为0.6kg:0.3kg的比例进行复配，然后将烟草提取物加入到水中混合均匀，在0℃～40℃下均匀喷淋到1t普通卷烟纸内表面。(1) The sheet tobacco C1F (Yunnan Yuxi tobacco raw material) and HTMOB flue-cured tobacco (Brazilian tobacco raw material) were pulverized and ground respectively, and the pulverized powder was extracted by ultrasonic waves, and then extracted with ether and alcohol, and then subjected to low temperature (-30 ° C ~ -40°C) vacuum (2-8 Pa) and freeze-dried to obtain powdered tobacco extract. Compound according to the mass ratio of C1F (Yunnan Yuxi tobacco raw material) and HTMOB flue-cured tobacco (Brazilian tobacco raw material) extract at a ratio of 0.6kg:0.3kg, then add the tobacco extract to water and mix evenly, at 0℃～40℃ Spray evenly onto the inner surface of 1t of ordinary cigarette paper.
(2)将助燃剂0.5kg酒石酸钾钠溶解后，加入0.5kg的D-葡萄糖醛酸搅拌均匀，用第一涂布辊涂布在1t普通卷烟纸内表面(2) After dissolving 0.5 kg of potassium sodium tartrate as a combustion enhancer, add 0.5 kg of D-glucuronic acid and stir evenly, and coat the inner surface of 1 ton of ordinary cigarette paper with the first coating roller
(3)将助燃剂0.6kg柠檬酸钾和0.4kg柠檬酸钠溶解后，加入0.5kg的山梨糠醇搅拌均匀，用第二涂布辊涂布在1t卷烟纸外表面。(3) After 0.6 kg of potassium citrate and 0.4 kg of sodium citrate were dissolved, 0.5 kg of sorbitol was added and stirred evenly, and coated on the outer surface of 1 ton of cigarette paper with a second coating roller.
实施例3：卷烟样品进行对比评吸Embodiment 3: Cigarette samples are compared and evaluated for smoking
用实施例1和实施例2中制备的润香卷烟纸在卷烟机上卷制，制得卷烟样品。同时将常规卷烟纸(对照样1)和现有技术中的保润卷烟纸(对照样2)分别在相同的卷烟机上卷制，分别制得卷烟样品。将卷烟样品进行对比评吸，评吸结果如表1所示：The flavoring cigarette papers prepared in Examples 1 and 2 were rolled on a cigarette machine to prepare cigarette samples. Simultaneously, conventional cigarette paper (control sample 1) and moisturizing cigarette paper (control sample 2) in the prior art were respectively rolled on the same cigarette machine to prepare cigarette samples respectively. The cigarette samples were compared and smoked, and the smoking results are shown in Table 1:
表1：感官质量评吸结果Table 1: Smoking results of sensory quality evaluation
对比评吸结果表明，由本发明方法制备的润香卷烟纸制得的卷烟样品，在抽吸过程中的感官质量明显提升(总分较高)，特别是在香气、刺激性、润感等方面都有较大的改善。The comparative smoking results show that the sensory quality of the cigarette samples made from the fragrant cigarette paper prepared by the method of the present invention is obviously improved (the total score is higher) during the smoking process, especially in aspects such as aroma, pungency, moist feeling, etc. All have been greatly improved.
实施例4Example 4
分别实施例3中制备的卷烟样品进行抽吸，并检测各卷烟样品抽吸后的烟气成分。各种烟气成分含量如下表2所示：The cigarette samples prepared in Example 3 were respectively smoked, and the smoke components of each cigarette sample after smoking were detected. The contents of various smoke components are shown in Table 2 below:
表2：烟气常规检测结果Table 2: Routine detection results of flue gas
通过对本发明的润香卷烟纸制备的卷烟样品与对照样的烟气成分进行测定，结果表明，本发明的润香卷烟纸能够有效提高烟气中水分、降低卷烟产品抽吸过程产生的烟气中的C0。By measuring the smoke components of the cigarette samples prepared with the flavor-moistening cigarette paper of the present invention and the control sample, the results show that the flavor-moistening cigarette paper of the present invention can effectively increase the moisture in the smoke and reduce the smoke generated during the smoking process of cigarette products C0 in.
本发明的润香卷烟纸能够增加卷烟烟气润感，降低卷烟烟气中的有害成分，增强香气的丰富性。因此，本发明的润香卷烟纸具有广阔的应用前景。The fragrance-moistening cigarette paper of the invention can increase the moist feeling of cigarette smoke, reduce harmful components in cigarette smoke, and enhance the richness of aroma. Therefore, the flavor-moisturizing cigarette paper of the present invention has broad application prospects.
| Application Number | Priority Date | Filing Date | Title |
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| CN2016110390402 | 2016-11-21 | ||
| CN201611039040 | 2016-11-21 |
| Publication Number | Publication Date |
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| CN106948222A CN106948222A (en) | 2017-07-14 |
| CN106948222Btrue CN106948222B (en) | 2018-05-04 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710196299.6AActiveCN106948222B (en) | 2016-11-21 | 2017-03-29 | The fragrant cigarette paper of one kind profit, preparation method and the usage |
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