技术领域technical field
本发明涉及烟草替代品制备领域，特别是涉及一种含化型无烟气烟草制品及其制备方法和用途。The invention relates to the field of preparation of tobacco substitutes, in particular to a chemical-containing smokeless tobacco product and its preparation method and application.
背景技术Background technique
卷烟燃烧生成的烟气中含有对人体有害的成分，吸烟有害健康已经成为公共卫生界的定论。中国是世界上最大的烟草生产国和消费国，随着《世界卫生组织烟草控制框架公约》中有关条款在我国的逐步实施，特别是人们对于健康和环保的日益关注，公共场所禁止吸烟逐渐成为一种社会共识，这对传统卷烟的发展造成越来越多的制约。无烟气烟草制品以非燃烧的形式向消费者提供类似于吸食传统卷烟的生理满足感，主要包括口含型(不咀嚼，有残渣)、含化型(不咀嚼，无残渣)、胶基型(咀嚼，有残渣)烟草制品等。无烟气烟草制品可以作为传统卷烟的补充替代产品，避免了人们在公共场所接触到烟草烟雾，对于促进公共健康和烟草行业的长远持续发展具有重要意义。The smoke generated by burning cigarettes contains components harmful to the human body. Smoking is harmful to health and has become the conclusion of the public health community. China is the world's largest tobacco producer and consumer. With the gradual implementation of the relevant provisions of the "World Health Organization Framework Convention on Tobacco Control" in our country, especially people's increasing concern for health and environmental protection, smoking bans in public places have gradually become A social consensus, which creates more and more constraints on the development of traditional cigarettes. Smokeless tobacco products provide consumers with the physiological satisfaction similar to smoking traditional cigarettes in a non-combustible form, mainly including buccal type (no chewing, residue), containing type (no chewing, no residue), gum base Type (chewing, residue) tobacco products, etc. Smokeless tobacco products can be used as supplementary alternatives to traditional cigarettes, avoiding people's exposure to tobacco smoke in public places, and are of great significance for promoting public health and the long-term sustainable development of the tobacco industry.
目前，无烟气烟草制品主要在欧洲、北美等地区以散装或袋装口含烟的形式进行销售。然而，国内消费者并无使用口含烟的传统，并且口含烟是直接以烟叶原料的形式在口腔中使用，烟碱释放不稳定，刺激性较大，舒适性较差，消费者的接受程度低。含化型无烟气烟草制品是将烟草细粉或者烟草提取物与其他添加剂混合后压制成一定形状，使用时在口腔唾液等作用下，发生崩解、溶解等作用，较平稳地释放烟碱、香味物质等有效成分，刺激性较小，无烟气产生，使用方便，国内消费者容易接受，是一种在国内市场有很好发展前景的新型无烟气烟草制品。At present, smokeless tobacco products are mainly sold in the form of snus in bulk or in pouches in Europe, North America and other regions. However, domestic consumers do not have the tradition of using snus, and snus is directly used in the oral cavity in the form of tobacco leaf raw materials. The release of nicotine is unstable, the irritation is large, and the comfort is poor. Consumer acceptance low level. Chemical-containing smokeless tobacco products are made by mixing tobacco fine powder or tobacco extracts with other additives and pressing them into a certain shape. When in use, they will disintegrate and dissolve under the action of oral saliva, etc., and release nicotine relatively smoothly. It is a new type of smokeless tobacco product with good development prospects in the domestic market.
发明内容Contents of the invention
鉴于以上所述现有技术的缺点，本发明的目的在于提供一种含化型无烟气烟草制品及其制备方法和用途，用于解决现有技术中的问题。In view of the above-mentioned shortcomings of the prior art, the purpose of the present invention is to provide a liquefied smokeless tobacco product and its preparation method and use, which are used to solve the problems in the prior art.
为实现上述目的及其他相关目的，本发明第一方面提供一种含化型无烟气烟草制品，其原料按重量份计，包括如下组分：In order to achieve the above purpose and other related purposes, the first aspect of the present invention provides a chemical-containing smokeless tobacco product, the raw materials of which include the following components in parts by weight:
优选的，所述含化型无烟气烟草制品，其原料按重量份计，包括如下组分：Preferably, the raw materials of the chemical-containing smokeless tobacco product include the following components in parts by weight:
优选的，所述含化型无烟气烟草制品中的烟碱含量为0.005-8mg/g。Preferably, the nicotine content in the chemical-containing smokeless tobacco product is 0.005-8 mg/g.
优选的，所述烟草选自烤烟、晾烟、晒烟、香料烟中的一种或多种的组合。Preferably, the tobacco is selected from one or more combinations of flue-cured tobacco, air-cured tobacco, sun-cured tobacco, and oriental tobacco.
更优选的，所述晾烟选自白肋烟、马里兰烟、雪茄烟、深色晾烟及其他晾烟中的一种或多种的组合，所述晒烟选自晒红烟和晒黄烟及其他晒烟中的一种或多种的组合。More preferably, the air-cured tobacco is selected from one or more combinations of Burley tobacco, Maryland tobacco, cigar tobacco, dark air-cured tobacco and other air-cured tobaccos, and the sun-cured tobacco is selected from sun-cured red tobacco and sun-cured yellow tobacco and One or more combinations of other sun-cured tobaccos.
进一步优选的，所述烟草为产自贵州地区的晾晒烟，或者该晾晒烟与其他烟草的组合。Further preferably, the tobacco is air-cured tobacco produced in Guizhou region, or a combination of the air-cured tobacco and other tobaccos.
优选的，所述烟草是常规烟叶和有机生态烟叶中的一种或多种的组合。Preferably, the tobacco is a combination of one or more of conventional tobacco leaves and organic ecological tobacco leaves.
优选的，所述烟草经自然发酵、陈化(在本发明一优选实施例中，陈化时间为一年)、抽梗、清洗、脱水后进行增香处理。Preferably, the tobacco is naturally fermented, aged (in a preferred embodiment of the present invention, the aging time is one year), stemmed, washed and dehydrated, followed by flavoring treatment.
增香处理是指用香料液浸泡或浸润烟草材料，或将香料液喷洒到烟草粉末或烟草提取物上。香料液可通过香料材料煎水或者香味剂配制而成。Flavoring treatment refers to soaking or infiltrating tobacco material with flavor liquid, or spraying flavor liquid onto tobacco powder or tobacco extract. The spice liquid can be prepared by decocting spice materials or flavoring agents.
更优选的，所述烟草粉末为烟草粉碎、筛分后获得的粒度大于100目的细粉、微粉、超微粉等中的一种或多种的组合。More preferably, the tobacco powder is a combination of one or more of fine powder, micropowder, ultrafine powder, etc. obtained after tobacco pulverization and sieving with a particle size greater than 100 mesh.
进一步优选的，所述烟草粉末的粒度为200-2000目。Further preferably, the particle size of the tobacco powder is 200-2000 mesh.
更优选的，所述烟草提取物为液态烟草提取物或者烟草提取物复合物细粉。More preferably, the tobacco extract is liquid tobacco extract or tobacco extract compound fine powder.
所述烟草提取物是指烟草经过干燥、粉碎、筛分后，经过提取得到的烟草提取物，烟草提取物复合物细粉为烟草提取物经过分子蒸馏、冷冻干燥、喷雾干燥等手段，在赋形剂的作用下制成的烟草提取物复合物细粉。The tobacco extract refers to the tobacco extract obtained after the tobacco is dried, pulverized, and sieved. Tobacco extract compound fine powder made under the action of excipient.
更优选的，所述提取方法选自超临界萃取、溶剂浸提、超声辅助萃取、微波辅助萃取、蒸馏萃取等中的一种或多种的组合。More preferably, the extraction method is selected from one or more combinations of supercritical extraction, solvent extraction, ultrasonic-assisted extraction, microwave-assisted extraction, and distillation extraction.
优选的，所述中药剂选自桑叶、薄荷、桔梗、枇杷、佛手柑、藏青果、蜂蜜、板蓝根、黄芩、布渣叶、鸡蛋花、杭白菊、金银花、款冬花、凉粉草、夏枯草、甘草、麦冬、牛蒡子、半夏、无花果、蒲公英、陈皮、紫苏子、蝉蜕、麻黄及其他清热润喉、止咳润肺中药材中的一种或多种的组合。Preferably, the Chinese medicine is selected from the group consisting of mulberry leaves, mint, platycodon grandiflorum, loquat, bergamot, Tibetan green fruit, honey, isatis root, scutellaria baicalensis, Buza leaves, frangipani, chrysanthemum, honeysuckle, coltsfoot, jelly grass, and prunella vulgaris , Licorice, Ophiopogon japonicus, Arctium, pinellia, fig, dandelion, tangerine peel, perilla seed, cicada slough, ephedra and other Chinese medicinal materials for clearing away heat and moistening throat, relieving cough and moistening lung.
更优选的，所述中药剂是指中药材粉末或者中药材提取物。More preferably, the traditional Chinese medicine refers to Chinese herbal medicine powder or Chinese herbal medicine extract.
优选的，所述矫味剂选自氯化钠、氯化钾、柠檬酸钠、柠檬酸钾、苹果酸钠、葡萄糖酸钠及其他食品用矫味剂中的一种或多种的组合。Preferably, the flavoring agent is selected from one or more combinations of sodium chloride, potassium chloride, sodium citrate, potassium citrate, sodium malate, sodium gluconate and other food flavoring agents.
优选的，所述甜味剂选自果糖、葡萄糖(浆)、蔗糖、饴糖、氢化淀粉水解物、玉米糖浆、枫树糖浆、蛋白糖、甘草粉、甘草酸盐、甜菊糖苷、罗汉果甜苷、非洲竹竽甜素、蜂蜜、甘露糖、D-甘露糖醇、乳糖、乳糖醇、木糖醇、安赛蜜、纽甜、阿斯巴甜、麦芽糖醇(浆)、山梨糖醇(浆)、糖精钠、甜蜜素、环己基氨基磺酸钙、三氯蔗糖、阿力甜、异麦芽酮糖、赤藓糖醇、异麦芽低聚糖、异麦芽酮糖醇、低聚半乳糖、乳酮糖、低聚果糖、棉子糖、大豆低聚糖、低聚乳果糖、低聚木糖、菊粉低聚糖、蔗糖素、甘草甜素、新橙皮苷二氢查尔酮、仙茅甜蛋白、神秘果甜蛋白、薯芋防己甜素、双甜、L-阿拉伯糖及其他食品用糖类和/或非糖甜味剂中的一种或多种的组合。Preferably, the sweetener is selected from fructose, glucose (syrup), sucrose, maltose, hydrogenated starch hydrolyzate, corn syrup, maple syrup, protein sugar, licorice powder, glycyrrhizinate, steviol glycoside, mogroside, African bamboo sweetin, honey, mannose, D-mannitol, lactose, lactitol, xylitol, acesulfame potassium, neotame, aspartame, maltitol (syrup), sorbitol (syrup) , sodium saccharin, cyclamate, calcium cyclamate, sucralose, alitame, isomaltulose, erythritol, isomalt-oligosaccharides, isomalt, galacto-oligosaccharides, milk Ketose, fructooligosaccharides, raffinose, soybean oligosaccharides, lactulose oligosaccharides, xylooligosaccharides, inulin oligosaccharides, sucralose, glycyrrhizin, neohesperidin dihydrochalcone, celery A combination of one or more of Maatin, Miracin, Tetretin, Double Sweet, L-Arabinose and other food sugars and/or non-sugar sweeteners.
优选的，所述香味剂选自咖啡油、罗勒油、万寿菊油、小豆蔻油、甜橙油、康酿克油、冬青油、白兰花油、杭白菊油、柠檬油、圆柚油、乌梅酊、红茶酊、绿茶酊、可可酊、山楂酊、枣子酊、芦荟提取物、金银花提取物、荷叶提取物、朗姆酒等；也可以是咖啡粉、梅子粉、红枣粉、可可粉、绿茶粉、果汁及其他食品用香味剂中的一种或多种的组合。Preferably, the flavoring agent is selected from the group consisting of coffee oil, basil oil, marigold oil, cardamom oil, sweet orange oil, Kang Nongke oil, wintergreen oil, white orchid oil, chrysanthemum oil, lemon oil, pomelo oil, Black plum tincture, black tea tincture, green tea tincture, cocoa tincture, hawthorn tincture, jujube tincture, aloe extract, honeysuckle extract, lotus leaf extract, rum, etc.; coffee powder, plum powder, jujube powder, cocoa powder , green tea powder, fruit juice and other food flavoring agents in one or more combination.
优选的，所述填充剂选自滑石粉、磷酸氢钙、碳酸钙、碳酸镁、磷酸钙、玉米淀粉、环糊精、麦芽糊精、D-甘露糖醇、乳糖、乳糖醇、木糖醇、麦芽糖醇、山梨糖醇及其他食品用填充剂中的一种或多种的组合。Preferably, the filler is selected from talcum powder, calcium hydrogen phosphate, calcium carbonate, magnesium carbonate, calcium phosphate, corn starch, cyclodextrin, maltodextrin, D-mannitol, lactose, lactitol, xylitol , maltitol, sorbitol and other food fillers in one or more combination.
优选的，所述粘合剂选自淀粉、磷酸化二淀粉磷酸酯、羧甲基淀粉钠、淀粉磷酸酯钠、麦芽糊精、环糊精、微晶纤维素、羧甲基纤维素钠、羟丙基纤维素、甲基纤维素、乙基纤维素、羟丙甲基纤维素、明胶、阿拉伯胶、酪蛋白、甲壳素、壳聚糖及其衍生物、壳寡糖及其衍生物、海藻酸钠、海藻酸铵、海藻酸丙二醇酯、刺云实胶、甘露糖醇、山梨糖醇、乳糖醇、瓜尔胶、果胶、海萝胶、葫芦巴胶、槐豆胶、黄蜀葵胶、黄原胶、桃胶、紫胶、决明胶、黄蓍胶、卡拉胶、可得然胶、可溶性大豆多糖、罗望子多糖胶、普鲁兰多糖、亚麻籽胶及其他食品用粘合剂中的一种或多种的组合。Preferably, the binder is selected from starch, phosphorylated distarch phosphate, sodium carboxymethyl starch, sodium starch phosphate, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethyl cellulose, Hydroxypropyl cellulose, methyl cellulose, ethyl cellulose, hydroxypropyl methyl cellulose, gelatin, gum arabic, casein, chitin, chitosan and its derivatives, chitosan oligosaccharide and its derivatives, Sodium Alginate, Ammonium Alginate, Propylene Glycol Alginate, Tara Gum, Mannitol, Sorbitol, Lactitol, Guar Gum, Pectin, Seaweed Gum, Fenugreek Gum, Locust Bean Gum, Marshmallow Gum , xanthan gum, peach gum, shellac, cassia gum, tragacanth gum, carrageenan, curdlan gum, soluble soybean polysaccharide, tamarind polysaccharide gum, pullulan polysaccharide, linseed gum and other food adhesives one or a combination of more.
优选的，所述乳化剂选自单、双、三脂肪酸甘油酯、卵磷脂、大豆磷脂、脱脂可可粉、乙酰化单双脂肪酸甘油酯、聚甘油脂肪酸酯、聚乙二醇、聚乙烯脱水山梨醇酯、泊洛沙姆、蔗糖脂肪酸酯及其他食品用乳化剂中的一种或多种的组合。Preferably, the emulsifier is selected from mono-, di-, and tri-fatty acid glycerides, lecithin, soybean lecithin, defatted cocoa powder, acetylated mono- and di-fatty acid glycerides, polyglycerin fatty acid esters, polyethylene glycol, polyethylene dehydrated A combination of one or more of sorbitol esters, poloxamers, sucrose fatty acid esters and other food emulsifiers.
更优选的，所述三脂肪酸甘油酯可以使用三乙酸甘油酯等。More preferably, triacetin and the like may be used as the triglyceride of fatty acid.
优选的，所述崩解助剂选自淀粉、预胶化淀粉、微晶纤维素、交联聚乙烯基吡咯烷酮、羧甲基淀粉钠、低取代羟丙基纤维素、交联羧甲基纤维素钠、结冷胶、黄原胶及其他食品用崩解助剂中的一种或多种的组合。Preferably, the disintegration aid is selected from starch, pregelatinized starch, microcrystalline cellulose, cross-linked polyvinylpyrrolidone, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, cross-linked carboxymethyl cellulose A combination of one or more of sodium sodium, gellan gum, xanthan gum and other food disintegration aids.
优选的，所述pH调节剂选自碳酸钠、碳酸氢钠、碳酸钾、碳酸氢钾、柠檬酸钠、柠檬酸钾、葡萄糖酸钠及其他食品用pH调节剂中的一种或多种的组合。Preferably, the pH regulator is selected from one or more of sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate, sodium gluconate and other food pH regulators combination.
优选的，所述清凉剂选自薄荷醇、椒样薄荷油、亚洲薄荷油、亚洲薄荷素油、胡薄荷油、天然薄荷脑、N-对苯乙腈基薄荷烷基甲酰胺、N-(2-(吡啶-2-基)乙基)薄荷烷基甲酰胺、薄荷内酯及其他薄荷提取物或衍生物等中的一种或多种的组合。Preferably, the cooling agent is selected from menthol, peppermint oil, peppermint oil, peppermint oil, peppermint oil, natural menthol, N-phenylacetonitrile menthyl formamide, N-(2- A combination of one or more of (pyridin-2-yl)ethyl)menthanyl formamide, mentholactone, and other mint extracts or derivatives.
优选的，所述着色剂选自二氧化钛、赤藓红、亮蓝、红曲黄色素、茶黄色素、茶绿色素、紫甘薯色素、β-阿朴-8’-胡萝卜素醛、叶绿素铜、靛蓝、多穗柯棕、番茄红素、柑桔黄、黑豆红、黑加仑红、红花黄、红米红、红曲红、姜黄、焦糖色、金樱子棕、菊花黄浸膏、可可壳色、辣椒橙、萝卜红、花生衣红、落葵红、玫瑰茄红、葡萄皮红、桑葚红、酸枣色、天然苋菜红、胭脂虫红、杨梅红、叶黄素、藻蓝、β-胡萝卜素及其他食品用着色剂中的一种或多种的组合。Preferably, the coloring agent is selected from titanium dioxide, erythrosine, brilliant blue, monascus yellow pigment, tea yellow pigment, tea green pigment, purple sweet potato pigment, β-apo-8'-carotene aldehyde, copper chlorophyll, Indigo, tachycarp, lycopene, citrus yellow, black bean red, blackcurrant red, safflower yellow, red rice red, monascus red, turmeric, caramel color, golden cherry brown, chrysanthemum yellow extract, cocoa Shell color, pepper orange, radish red, peanut red, sunflower red, roselle red, grape skin red, mulberry red, jujube color, natural amaranth red, cochineal red, bayberry red, lutein, algal blue, β - A combination of one or more of carotene and other food coloring agents.
优选的，所述抗氧化剂选自茶多酚、丁基羟基茴香醚、苯甲酸钠、二丁基羟基甲苯、没食子酸丙酯、山梨酸及其钾盐、dl-α-生育酚、d-α-生育酚、、维生素C、抗坏血酸钙、抗坏血酸棕榈酸酯、D-异抗坏血酸及其钠盐、鼠尾草酸、甘草抗氧化物、竹叶抗氧化物、银杏提取物、茶叶提取物和葡萄籽提取物及其他食品用抗氧化剂中的一种或多种的组合。Preferably, the antioxidant is selected from tea polyphenols, butyl hydroxyanisole, sodium benzoate, dibutyl hydroxytoluene, propyl gallate, sorbic acid and its potassium salt, dl-α-tocopherol, d-α -Tocopherol, vitamin C, calcium ascorbate, ascorbyl palmitate, D-erythorbic acid and its sodium salt, carnosic acid, licorice antioxidant, bamboo leaf antioxidant, ginkgo biloba extract, tea leaf extract and grape seed One or more combinations of extracts and other food antioxidants.
优选的，所述润滑剂选自硬脂酸、硬脂酸钙、硬脂酸镁、硬脂酸钠、硬脂酸钾、滑石粉、巴西棕榈蜡、蜂蜡、聚乙烯蜡、聚乙二醇、石蜡、石油石蜡、微晶石蜡、小烛树蜡、蔗糖脂肪酸酯、氢化植物油及其他食品用润滑剂中的一种或多种的组合。Preferably, the lubricant is selected from the group consisting of stearic acid, calcium stearate, magnesium stearate, sodium stearate, potassium stearate, talcum powder, carnauba wax, beeswax, polyethylene wax, polyethylene glycol , paraffin, petroleum paraffin, microcrystalline paraffin, candelilla wax, sucrose fatty acid ester, hydrogenated vegetable oil and other food lubricants in one or more combinations.
本发明第二方面提供所述含化型无烟气烟草制品的制备方法，可以采取制粒压片法，包括如下步骤：The second aspect of the present invention provides the preparation method of the chemical-containing smokeless tobacco product, which can adopt the granulation and tabletting method, including the following steps:
(1)按配比将烟草粉末和/或烟草提取物、中药剂、矫味剂、甜味剂、香味剂、填充剂、粘合剂、乳化剂、pH调节剂、着色剂等混合均匀，用制粒机进行湿法制粒，得到14-50目颗粒；(1) Mix tobacco powder and/or tobacco extract, traditional Chinese medicine, flavoring agent, sweetener, flavoring agent, filler, binder, emulsifier, pH regulator, coloring agent, etc. uniformly according to the proportioning ratio, and use The granulator performs wet granulation to obtain 14-50 mesh granules;
(2)将步骤(1)制粒得到的组合物颗粒在烘箱中干燥0.5-2小时，然后用14-50目筛网进行整粒；(2) drying the composition granules obtained by granulating in step (1) in an oven for 0.5-2 hours, and then sizing with a 14-50 mesh screen;
(3)将整粒得到的组合物颗粒与抗氧化剂、清凉剂、崩解助剂、润滑剂等混合均匀，在压片机中压制成规格为0.5-2g/片粒的含化型无烟气烟草制品。(3) Mix the granules of the composition obtained by sizing with antioxidants, cooling agents, disintegration aids, lubricants, etc., and press them into a tablet machine to form a chemical-containing smoke-free product with a specification of 0.5-2g/tablet. gas tobacco products.
也可采取直接压片法，包括如下步骤：Also can adopt direct compression method, comprise the following steps:
(1)按配比将烟草粉末和/或烟草提取物、中药剂、矫味剂、甜味剂、香味剂、填充剂、粘合剂、乳化剂、pH调节剂、着色剂、抗氧化剂、清凉剂、崩解助剂、润滑剂等混合均匀，在压片机中压制得到规格为0.5-2g/片粒的含化型无烟气烟草制品；(1) Tobacco powder and/or tobacco extract, traditional Chinese medicine, flavoring agent, sweetener, flavoring agent, filler, binder, emulsifier, pH regulator, colorant, antioxidant, cooling agent, etc. Agents, disintegration aids, lubricants, etc. are mixed evenly, and compressed in a tablet machine to obtain a chemical-containing smokeless tobacco product with a specification of 0.5-2g/tablet;
(2)将步骤(1)得到的片粒在烘箱中干燥后即得含化型无烟气烟草制品。(2) drying the flakes obtained in the step (1) in an oven to obtain a chemical-containing smokeless tobacco product.
进一步的，可对上述所得的含化型无烟气烟草制品进行外包衣，即成包衣型含化型无烟气烟草制品。Further, the above-obtained chemical-containing smokeless tobacco product can be coated, that is, a coated chemical-containing smokeless tobacco product.
本发明第三方面提供所述含化型无烟气烟草制品在烟草补充替代品制备领域的用途。The third aspect of the present invention provides the use of the chemical-containing smokeless tobacco product in the field of preparation of tobacco supplementary substitutes.
本发明所述的含化型无烟气烟草制品，选用贵州地区的晾晒烟作为主要原料，香气浓郁，劲头足，并且对烟叶经过增香处理，控制烟碱含量，添加了清热润喉、止咳润肺的中药剂，平衡了产品的生理满足感和口感舒适度，对于无烟气烟草制品的市场推广具有促进作用。基于本发明的产品入口崩解，口感舒适，香味持久，不产生烟气，可以在公共场所使用，保质期长，方便携带，是一种口感舒适、安全环保的新型无烟气烟草制品。The chemical-containing smokeless tobacco product of the present invention uses air-dried tobacco in Guizhou as the main raw material, which has a rich aroma and strong energy, and the tobacco leaves are treated with aroma enhancement to control the content of nicotine, and add heat-clearing, throat-relieving and cough-relieving ingredients. The lung-nourishing traditional Chinese medicine balances the physiological satisfaction and taste comfort of the product, and has a promoting effect on the marketing of smokeless tobacco products. The product based on the invention disintegrates at the entrance, has a comfortable taste, long-lasting fragrance, does not produce smoke, can be used in public places, has a long shelf life, is convenient to carry, and is a new type of smokeless tobacco product with comfortable taste, safety and environmental protection.
附图说明Description of drawings
图1所示为本发明工艺流程图Fig. 1 shows that process flow chart of the present invention
具体实施方式detailed description
本发明的目的在于提供一种传统卷烟的补充替代产品，即一种含化型无烟气烟草制品。本发明发明人发现贵州地区的晾晒烟香味浓郁、吃味丰满、劲头足，将该晾晒烟通过烟草增香处理工艺，并进一步添加中药剂、矫味剂、甜味剂、香味剂、填充剂、粘合剂、清凉剂、崩解助剂等成分后，具有香气浓郁、劲头足等特点，从而提供一种口感舒适、安全环保的新型无烟气烟草制品，在此基础上完成了本发明。The purpose of the present invention is to provide a supplementary alternative to traditional cigarettes, that is, a chemical-containing smokeless tobacco product. The inventors of the present invention found that the air-cured tobacco in Guizhou area has a strong aroma, full taste, and strong energy. The air-cured tobacco was processed by tobacco flavoring treatment, and further added Chinese medicines, flavoring agents, sweeteners, flavoring agents, and fillers. , adhesives, cooling agents, disintegration aids and other components, it has the characteristics of rich aroma and strong strength, so as to provide a new type of smokeless tobacco product with comfortable taste, safety and environmental protection. On this basis, the present invention has been completed .
本发明提供一种含化型无烟气烟草制品，其原料按重量份计，包括如下组分：The invention provides a chemical-containing smokeless tobacco product, the raw materials of which include the following components in parts by weight:
优选的，所述含化型无烟气烟草制品中的烟碱含量为0.005-8mg/g。Preferably, the nicotine content in the chemical-containing smokeless tobacco product is 0.005-8 mg/g.
优选的，所述烟草粉末和/或烟草提取物中，烟草选自烤烟、晾烟、晒烟、香料烟中的一种或多种的组合。具体可使用烟草的叶、花、茎、种子等部位。Preferably, in the tobacco powder and/or tobacco extract, the tobacco is selected from one or more combinations of flue-cured tobacco, air-cured tobacco, sun-cured tobacco, and oriental tobacco. Specifically, leaves, flowers, stems, seeds and other parts of tobacco can be used.
更优选的，所述晾烟选自白肋烟、马里兰烟、雪茄烟、深色晾烟等中的一种或多种的组合，晒烟选自晒红烟和晒黄烟等中的一种或多种的组合。More preferably, the air-cured tobacco is selected from one or more combinations of Burley tobacco, Maryland tobacco, cigar tobacco, dark air-cured tobacco, etc., and the air-cured tobacco is selected from one or more of sun-cured red tobacco and sun-cured yellow tobacco. Various combinations.
在本发明优选实施例中，所述烟草为贵州地区的晾晒烟，或者该晾晒烟与其他烟草的组合，组合物中，该晾晒烟的重量百分比≥30％。In a preferred embodiment of the present invention, the tobacco is air-cured tobacco in Guizhou region, or a combination of the air-cured tobacco and other tobaccos, and in the composition, the weight percentage of the air-cured tobacco is ≥ 30%.
更优选的，所述烟草可以是常规烟叶，也可以是有机生态烟叶，或者有机生态烟叶与常规烟叶的组合。More preferably, the tobacco can be conventional tobacco leaves, organic ecological tobacco leaves, or a combination of organic ecological tobacco leaves and conventional tobacco leaves.
优选的，所述烟草经自然发酵、陈化(在本发明一优选实施例中，陈化时间为一年)、抽梗、清洗、脱水后进行增香处理。Preferably, the tobacco is naturally fermented, aged (in a preferred embodiment of the present invention, the aging time is one year), stemmed, washed and dehydrated, followed by flavoring treatment.
增香处理是指用香料液浸泡或浸润细粉化前的烟草，或将香料液喷洒到烟草粉末或烟草提取物复合物细粉上。香料液可通过香料材料煎水或者香味剂配制而成，具体可选择的香料材料或香味剂包括但不限于甘草、金银花、康酿克油、烟草提取物等中的一种或多种的选择。Flavoring treatment refers to soaking or infiltrating the tobacco before fine powdering with flavor liquid, or spraying flavor liquid onto tobacco powder or tobacco extract compound fine powder. The spice liquid can be prepared by decocting spice materials or flavoring agents, and the specific optional flavoring materials or flavoring agents include but are not limited to one or more of licorice, honeysuckle, Kang Nongke oil, tobacco extract, etc. .
更优选的，所述的香料液中可以加入附着剂，以提高增香效果，具体可供选择的附着剂包括但不限于蜂蜜、玉米糖浆、β-环糊精、阿拉伯胶、明胶等中的一种或多种的组合。More preferably, an adhering agent can be added to the flavor liquid to improve the flavoring effect, and specific optional adhering agents include but are not limited to honey, corn syrup, β-cyclodextrin, gum arabic, gelatin, etc. One or more combinations.
所述烟草粉末为烟草材料经过干燥、粉碎后过筛网形成粗粉，利用超微粉碎设备将粗粉粉碎后过筛网后形成烟草粉末。所述含化型无烟气烟草制品按重量份计，包括0.005-25份烟草粉末，优选包括1-20份烟草粉末。The tobacco powder is dried and pulverized tobacco material and passed through a sieve to form a coarse powder, and the coarse powder is pulverized by an ultrafine grinding device and passed through a sieve to form a tobacco powder. The chemical-containing smokeless tobacco product includes 0.005-25 parts of tobacco powder, preferably 1-20 parts of tobacco powder in parts by weight.
更优选的，所述烟草粉末为烟草粉碎、筛分后得到的粒度大于100目的细粉、微粉、超微粉等中的一种或多种的组合。More preferably, the tobacco powder is a combination of one or more of fine powder, micropowder, superfine powder, etc. obtained after tobacco pulverization and sieving with a particle size greater than 100 mesh.
进一步优选的，所述烟草粉末的粒度为200-2000目。Further preferably, the particle size of the tobacco powder is 200-2000 mesh.
在本发明一优选实施例中，所述烟草粉末为烟草经过干燥、粉碎后过80目筛网形成粗粉，利用超微粉碎设备将粗粉粉碎后过300目筛网后形成烟草粉末。In a preferred embodiment of the present invention, the tobacco powder is dried and pulverized and passed through an 80-mesh sieve to form a coarse powder, and the coarse powder is pulverized by an ultrafine grinding device and passed through a 300-mesh sieve to form tobacco powder.
更优选的，所述烟草提取物是指烟草材料经过干燥、粉碎、筛分后，利用一定提取手段得到的烟草提取物。More preferably, the tobacco extract refers to the tobacco extract obtained by using certain extraction means after the tobacco material is dried, pulverized and sieved.
更优选的，所述提取手段选自超临界萃取、溶剂浸提、超声辅助萃取、微波辅助萃取、同时蒸馏萃取等中的一种或多种的组合。More preferably, the extraction means is selected from one or more combinations of supercritical extraction, solvent extraction, ultrasonic-assisted extraction, microwave-assisted extraction, and simultaneous distillation extraction.
进一步优选的，烟草提取物可经过分子蒸馏、冷冻干燥、喷雾干燥等手段，在赋形剂的作用下制成烟草提取物复合物细粉。所述含化型无烟气烟草制品按重量份计，包括0.005-25份烟草提取物，优选包括0.1-20份烟草提取物。Further preferably, the tobacco extract can be made into a tobacco extract compound fine powder under the action of excipients through molecular distillation, freeze drying, spray drying and other means. The chemical-containing smokeless tobacco product includes 0.005-25 parts of tobacco extract, preferably 0.1-20 part of tobacco extract, in parts by weight.
本发明所提供的含化型无烟气烟草制品中，所述中药剂可使用各种具有清热润喉、止咳润肺功效的中药材及组合。具体可选用的中药剂包括但不限于桑叶、薄荷、桔梗、枇杷、佛手柑、藏青果、蜂蜜、板蓝根、黄芩、布渣叶、鸡蛋花、杭白菊、金银花、款冬花、凉粉草、夏枯草、甘草、麦冬、牛蒡子、半夏、无花果、蒲公英、陈皮、紫苏子、蝉蜕、麻黄等中的一种或多种的组合。所述中药剂是指中药材粉末或者中药材提取物。所述含化型无烟气烟草制品按重量份计，包括0-5份中药剂，优选包括0.5-5份中药剂。In the chemical-containing smokeless tobacco product provided by the present invention, the traditional Chinese medicine can use various Chinese medicinal materials and combinations that have the functions of clearing away heat and moistening throat, relieving cough and moistening lung. Specific Chinese medicines that can be used include but are not limited to mulberry leaves, mint, bellflower, loquat, bergamot, Tibetan green fruit, honey, isatis root, scutellaria baicalensis, cloth dregs leaves, frangipani, chrysanthemum, honeysuckle, coltsfoot, jelly, summer One or more combinations of dry grass, licorice, Ophiopogon japonicus, burdock, pinellia, fig, dandelion, tangerine peel, perilla seed, cicada slough, ephedra, etc. The traditional Chinese medicine refers to Chinese medicinal material powder or Chinese medicinal material extract. The chemical-containing smokeless tobacco product includes 0-5 parts of traditional Chinese medicine, preferably 0.5-5 parts of traditional Chinese medicine, in parts by weight.
本发明所提供的含化型无烟气烟草制品中，所述矫味剂可使用各种食品中许可使用的矫味剂，只要不对本发明的发明目的产生限制即可。具体可选用的矫味剂包括但不限于氯化钠、氯化钾、柠檬酸钠、柠檬酸钾、苹果酸钠、葡萄糖酸钠等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-2份矫味剂，优选包括0.5-1份矫味剂。In the chemical-containing smokeless tobacco product provided by the present invention, the flavoring agent approved for use in various foods can be used as the flavoring agent, as long as it does not limit the purpose of the invention. Specific optional flavoring agents include, but are not limited to, one or more combinations of sodium chloride, potassium chloride, sodium citrate, potassium citrate, sodium malate, sodium gluconate, and the like. The chemical-containing smokeless tobacco product includes 0-2 parts of flavoring agent in parts by weight, preferably 0.5-1 part of flavoring agent.
本发明所提供的含化型无烟气烟草制品中，所述甜味剂可使用各种食品中许可使用的甜味剂，包括天然或合成甜味剂，只要不对本发明的发明目的产生限制即可。具体可选用的甜味剂包括但不限于果糖、葡萄糖(浆)、蔗糖、饴糖、氢化淀粉水解物、玉米糖浆、枫树糖浆、蛋白糖、甘草粉、甘草酸盐、甜菊糖苷、罗汉果甜苷、非洲竹竽甜素、蜂蜜、甘露糖、D-甘露糖醇、乳糖、乳糖醇、木糖醇、安赛蜜、纽甜、阿斯巴甜、麦芽糖醇(浆)、山梨糖醇(浆)、糖精钠、甜蜜素、环己基氨基磺酸钙、三氯蔗糖、阿力甜、异麦芽酮糖、赤藓糖醇、异麦芽低聚糖、异麦芽酮糖醇、低聚半乳糖、乳酮糖、低聚果糖、棉子糖、大豆低聚糖、低聚乳果糖、低聚木糖、菊粉低聚糖、蔗糖素、甘草甜素、新橙皮苷二氢查尔酮、仙茅甜蛋白、神秘果甜蛋白、薯芋防己甜素、双甜、L-阿拉伯糖等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0.05-50份甜味剂，优选包括35-45份甜味剂。In the chemical-containing smokeless tobacco product provided by the present invention, the sweetener can be a sweetener approved for use in various foods, including natural or synthetic sweeteners, as long as it does not limit the purpose of the present invention That's it. Specific optional sweeteners include but are not limited to fructose, glucose (syrup), sucrose, maltose, hydrogenated starch hydrolyzate, corn syrup, maple syrup, protein sugar, licorice powder, glycyrrhizinate, steviol glycoside, mogroside , African bamboo sweetin, honey, mannose, D-mannitol, lactose, lactitol, xylitol, acesulfame potassium, neotame, aspartame, maltitol (syrup), sorbitol (syrup) ), sodium saccharin, cyclamate, calcium cyclamate, sucralose, alitame, isomaltulose, erythritol, isomalt oligosaccharides, isomalt, galactooligosaccharides, Lactulose, fructooligosaccharide, raffinose, soybean oligosaccharide, lactulose oligosaccharide, xylooligosaccharide, inulin oligosaccharide, sucralose, glycyrrhizin, neohesperidin dihydrochalcone, One or a combination of curcululin, miraculin, yam-tetradine, double sweet, L-arabinose, etc. The chemical-containing smokeless tobacco product includes 0.05-50 parts of sweetener, preferably 35-45 parts of sweetener, by weight.
本发明所提供的含化型无烟气烟草制品中，所述香味剂可使用各种食品中许可使用的香味剂，只要不对本发明的发明目的产生限制即可。具体可选用的香味剂包括但不限于咖啡油、罗勒油、万寿菊油、小豆蔻油、甜橙油、康酿克油、冬青油、白兰花油、杭白菊油、柠檬油、圆柚油、乌梅酊、红茶酊、绿茶酊、可可酊、山楂酊、枣子酊、芦荟提取物、金银花提取物、荷叶提取物、朗姆酒、咖啡粉、梅子粉、红枣粉、可可粉、绿茶粉、果汁等中的一种或多种的组合；所述果汁可以是苹果、杏、香蕉、黑莓、樱桃、枣、无花果、甜橙、桃子、梨子、李子、梅子、葡萄等水果的浓缩果汁中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0.05-15份香味剂，优选包括1.5-10份香味剂。In the chemical-containing smokeless tobacco product provided by the present invention, the flavoring agent can be a flavoring agent approved for use in various foods, as long as it does not limit the purpose of the present invention. Specific optional flavoring agents include, but are not limited to, coffee oil, basil oil, marigold oil, cardamom oil, sweet orange oil, konjac oil, wintergreen oil, white orchid oil, chrysanthemum oil, lemon oil, pomelo oil , ebony tincture, black tea tincture, green tea tincture, cocoa tincture, hawthorn tincture, date tincture, aloe extract, honeysuckle extract, lotus leaf extract, rum, coffee powder, plum powder, red date powder, cocoa powder, green tea powder , fruit juice, etc.; the fruit juice can be concentrated fruit juices such as apples, apricots, bananas, blackberries, cherries, dates, figs, sweet oranges, peaches, pears, plums, plums, grapes, etc. one or a combination of more. The chemical-containing smokeless tobacco product includes 0.05-15 parts of flavoring agent in parts by weight, preferably 1.5-10 parts of flavoring agent.
本发明所提供的含化型无烟气烟草制品中，所述填充剂可使用各种食品中许可使用的填充剂，只要不对本发明的发明目的产生限制即可。具体可选用的填充剂包括但不限于滑石粉、磷酸氢钙、碳酸钙、碳酸镁、磷酸钙、玉米淀粉、环糊精、麦芽糊精、D-甘露糖醇、乳糖、乳糖醇、木糖醇、麦芽糖醇、山梨糖醇等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括1-50份填充剂，优选包括25-45份填充剂。In the liquefied smokeless tobacco product provided by the present invention, the fillers approved for use in various foods can be used as the filler, as long as there is no limitation to the purpose of the invention. Specific optional fillers include, but are not limited to, talc, calcium hydrogen phosphate, calcium carbonate, magnesium carbonate, calcium phosphate, corn starch, cyclodextrin, maltodextrin, D-mannitol, lactose, lactitol, xylose One or more combinations of alcohol, maltitol, sorbitol, etc. The chemical-containing smokeless tobacco product includes 1-50 parts of filler, preferably 25-45 parts of filler, by weight.
本发明所提供的含化型无烟气烟草制品中，所述粘合剂可使用各种食品中许可使用的粘合剂，只要不对本发明的发明目的产生限制即可。具体可选用的粘合剂包括但不限于淀粉、磷酸化二淀粉磷酸酯、羧甲基淀粉钠、淀粉磷酸酯钠、麦芽糊精、环糊精、微晶纤维素、羧甲基纤维素钠、羟丙基纤维素、甲基纤维素、乙基纤维素、羟丙甲基纤维素、明胶、阿拉伯胶、酪蛋白、甲壳素、壳聚糖及其衍生物、壳寡糖及其衍生物、海藻酸钠、海藻酸铵、海藻酸丙二醇酯、刺云实胶、甘露糖醇、山梨糖醇、乳糖醇、瓜尔胶、果胶、海萝胶、葫芦巴胶、槐豆胶、黄蜀葵胶、黄原胶、桃胶、紫胶、决明胶、黄蓍胶、卡拉胶、可得然胶、可溶性大豆多糖、罗望子多糖胶、普鲁兰多糖、亚麻籽胶等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0.5-10份粘合剂，优选包括1-6份粘合剂。In the liquefied smokeless tobacco product provided by the present invention, the adhesives that are approved for use in various foods can be used as the adhesive, as long as the purpose of the present invention is not limited. Specific optional binders include but are not limited to starch, phosphorylated distarch phosphate, sodium carboxymethyl starch, sodium starch phosphate, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethyl cellulose , hydroxypropyl cellulose, methyl cellulose, ethyl cellulose, hydroxypropyl methyl cellulose, gelatin, gum arabic, casein, chitin, chitosan and its derivatives, chitosan oligosaccharide and its derivatives , sodium alginate, ammonium alginate, propylene glycol alginate, tara gum, mannitol, sorbitol, lactitol, guar gum, pectin, seaweed gum, fenugreek gum, locust bean gum, marshmallow Gum, xanthan gum, peach gum, shellac, cassia gum, tragacanth gum, carrageenan, curdlan gum, soluble soybean polysaccharide, tamarind polysaccharide gum, pullulan polysaccharide, linseed gum, etc. or Various combinations. The chemical-containing smokeless tobacco product includes 0.5-10 parts of binder, preferably 1-6 parts of binder, by weight.
本发明所提供的含化型无烟气烟草制品中，所述乳化剂可使用各种食品中许可使用的乳化剂，只要不对本发明的发明目的产生限制即可。具体可选用的乳化剂包括但不限于单、双、三脂肪酸甘油酯、卵磷脂、大豆磷脂、脱脂可可粉、乙酰化单双脂肪酸甘油酯、聚甘油脂肪酸酯、聚乙二醇、聚乙烯脱水山梨醇酯、泊洛沙姆、蔗糖脂肪酸酯等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-2份乳化剂，优选包括0.5-2份乳化剂。In the liquefied smokeless tobacco product provided by the present invention, the emulsifiers approved for use in various foods can be used as the emulsifier, as long as the purpose of the present invention is not limited. Specific optional emulsifiers include but are not limited to mono-, di-, and tri-fatty acid glycerides, lecithin, soybean lecithin, defatted cocoa powder, acetylated mono- and di-fatty acid glycerides, polyglycerin fatty acid esters, polyethylene glycol, polyethylene A combination of one or more of sorbitan esters, poloxamers, sucrose fatty acid esters, etc. The liquefied smokeless tobacco product includes 0-2 parts of emulsifier, preferably 0.5-2 part of emulsifier, by weight.
更优选的，所述三脂肪酸甘油酯可以使用三乙酸甘油酯等。More preferably, triacetin and the like may be used as the triglyceride of fatty acid.
本发明所提供的含化型无烟气烟草制品中，所述崩解助剂可使用各种食品中许可使用的崩解助剂，只要不对本发明的发明目的产生限制即可。具体可选用的崩解助剂包括但不限于淀粉、预胶化淀粉、微晶纤维素、交联聚乙烯基吡咯烷酮、羧甲基淀粉钠、低取代羟丙基纤维素、交联羧甲基纤维素钠、结冷胶、黄原胶等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-10份崩解助剂，优选包括0.5-5份崩解助剂。In the chemical-containing smokeless tobacco product provided by the present invention, the disintegration aids approved for use in various foods can be used as the disintegration aids, as long as the object of the invention is not limited. Specific optional disintegration aids include but are not limited to starch, pregelatinized starch, microcrystalline cellulose, cross-linked polyvinylpyrrolidone, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, cross-linked carboxymethyl A combination of one or more of sodium cellulose, gellan gum, xanthan gum, etc. The chemical-containing smokeless tobacco product includes 0-10 parts of disintegration aids in parts by weight, preferably 0.5-5 parts of disintegration aids.
本发明所提供的含化型无烟气烟草制品中，所述pH调节剂可使用各种食品中许可使用的pH调节剂，只要不对本发明的发明目的产生限制即可。具体可选用的pH调节剂包括但不限于碳酸钠、碳酸氢钠、碳酸钾、碳酸氢钾、柠檬酸钠、柠檬酸钾、葡萄糖酸钠等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-2份pH调节剂。In the chemical-containing smokeless tobacco product provided by the present invention, the pH regulator can be a pH regulator approved for use in various foods, as long as it does not limit the purpose of the present invention. Specific optional pH regulators include, but are not limited to, one or more combinations of sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate, sodium gluconate, and the like. The chemical-containing smokeless tobacco product includes 0-2 parts by weight of a pH regulator.
本发明所提供的含化型无烟气烟草制品中，所述清凉剂可使用各种食品中许可使用的清凉剂，只要不对本发明的发明目的产生限制即可。具体可选用的清凉剂包括但不限于薄荷醇、椒样薄荷油、亚洲薄荷油、亚洲薄荷素油、胡薄荷油、天然薄荷脑、N-对苯乙腈基薄荷烷基甲酰胺、N-(2-(吡啶-2-基)乙基)薄荷烷基甲酰胺、薄荷内酯等薄荷提取物或衍生物等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-1份清凉剂。In the chemical-containing smokeless tobacco product provided by the present invention, the cooling agent can be the cooling agent approved for use in various foods, as long as it does not limit the purpose of the invention. Specific optional cooling agents include but are not limited to menthol, peppermint oil, peppermint oil, peppermint oil, peppermint oil, natural menthol, N-phenylacetonitrile menthyl formamide, N-(2 - a combination of one or more of mint extracts or derivatives such as (pyridin-2-yl)ethyl)menthanyl formamide, mentholactone, etc. The chemical-containing smokeless tobacco product includes 0-1 part of cooling agent in parts by weight.
本发明所提供的含化型无烟气烟草制品中，所述着色剂可使用各种食品中许可使用的着色剂，只要不对本发明的发明目的产生限制即可。具体可选用的着色剂包括但不限于二氧化钛、赤藓红、亮蓝、红曲黄色素、茶黄色素、茶绿色素、紫甘薯色素、β-阿朴-8’-胡萝卜素醛、叶绿素铜、靛蓝、多穗柯棕、番茄红素、柑桔黄、黑豆红、黑加仑红、红花黄、红米红、红曲红、姜黄、焦糖色、金樱子棕、菊花黄浸膏、可可壳色、辣椒橙、萝卜红、花生衣红、落葵红、玫瑰茄红、葡萄皮红、桑葚红、酸枣色、天然苋菜红、胭脂虫红、杨梅红、叶黄素、藻蓝、β-胡萝卜素等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-0.5份着色剂，优选包括0-0.1份着色剂。In the chemical-containing smokeless tobacco product provided by the present invention, the colorant may be colorants approved for use in various foods, as long as the object of the present invention is not limited. Specific optional coloring agents include but are not limited to titanium dioxide, erythrosine, brilliant blue, monascus yellow pigment, tea yellow pigment, tea green pigment, purple sweet potato pigment, β-apo-8'-carotene aldehyde, copper chlorophyllin , indigo, multi-spike brown, lycopene, citrus yellow, black bean red, black currant red, safflower yellow, red rice red, monascus red, turmeric, caramel color, golden cherry brown, chrysanthemum yellow extract, Cocoa shell color, pepper orange, radish red, peanut red, sunflower red, roselle red, grape skin red, mulberry red, jujube color, natural amaranth red, cochineal red, bayberry red, lutein, algal blue, One or more combinations of β-carotene and the like. The chemical-containing smokeless tobacco product includes 0-0.5 part of coloring agent, preferably 0-0.1 part of coloring agent, by weight.
本发明所提供的含化型无烟气烟草制品中，所述抗氧化剂可使用各种食品中许可使用的抗氧化剂，只要不对本发明的发明目的产生限制即可。具体可选用的抗氧化剂包括但不限于茶多酚、丁基羟基茴香醚、苯甲酸钠、二丁基羟基甲苯、没食子酸丙酯、山梨酸及其钾盐、dl-α-生育酚、d-α-生育酚、维生素C、抗坏血酸钙、抗坏血酸棕榈酸酯、D-异抗坏血酸及其钠盐、鼠尾草酸、甘草抗氧化物、竹叶抗氧化物、银杏提取物、茶叶提取物和葡萄籽提取物等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0-1份抗氧化剂，优选包括0-0.05份抗氧化剂。In the chemical-containing smokeless tobacco product provided by the present invention, the antioxidants approved for use in various foods can be used, as long as the purpose of the present invention is not limited. Specific optional antioxidants include but are not limited to tea polyphenols, butylated hydroxyanisole, sodium benzoate, dibutyl hydroxytoluene, propyl gallate, sorbic acid and its potassium salt, dl-α-tocopherol, d- Alpha-tocopherol, vitamin C, calcium ascorbate, ascorbyl palmitate, D-erythorbic acid and its sodium salt, carnosic acid, licorice antioxidant, bamboo leaf antioxidant, ginkgo biloba extract, tea leaf extract and grape seed One or more combinations of extracts and the like. The chemical-containing smokeless tobacco product includes 0-1 part of antioxidant, preferably 0-0.05 part of antioxidant in parts by weight.
本发明所提供的含化型无烟气烟草制品中，所述润滑剂可使用各种食品中许可使用的润滑剂，只要不对本发明的发明目的产生限制即可。具体可选用的润滑剂包括但不限于硬脂酸、硬脂酸钙、硬脂酸镁、硬脂酸钠、硬脂酸钾、滑石粉、巴西棕榈蜡、蜂蜡、聚乙烯蜡、聚乙二醇、石蜡、石油石蜡、微晶石蜡、小烛树蜡、蔗糖脂肪酸酯、氢化植物油等中的一种或多种的组合。所述含化型无烟气烟草制品按重量份计，包括0.05-3份润滑剂，优选包括0.05-2份润滑剂。In the liquefied smokeless tobacco product provided by the present invention, the lubricants approved for use in various foods can be used as the lubricant, as long as the purpose of the present invention is not limited. Specific optional lubricants include, but are not limited to, stearic acid, calcium stearate, magnesium stearate, sodium stearate, potassium stearate, talcum powder, carnauba wax, beeswax, polyethylene wax, polyethylene glycol One or more combinations of alcohol, paraffin, petroleum paraffin, microcrystalline paraffin, candelilla wax, sucrose fatty acid ester, hydrogenated vegetable oil, etc. The chemical-containing smokeless tobacco product includes 0.05-3 parts of lubricant, preferably 0.05-2 parts of lubricant in parts by weight.
本发明还提供所述含化型无烟气烟草制品的制备方法，可以采取制粒压片法，包括如下步骤：The present invention also provides a method for preparing the chemical-containing smokeless tobacco product, which may adopt a granulation and tabletting method, including the following steps:
(1)按配比将烟草粉末和/或烟草提取物、中药剂、矫味剂、甜味剂、香味剂、填充剂、粘合剂、乳化剂、pH调节剂、着色剂混合均匀，用制粒机进行湿法制粒，得到14-50目颗粒；(1) Mix tobacco powder and/or tobacco extract, traditional Chinese medicine, flavoring agent, sweetener, flavoring agent, filler, binder, emulsifier, pH regulator, coloring agent uniformly according to the proportion, and use the preparation Granulator for wet granulation to obtain 14-50 mesh granules;
(2)将步骤(1)制粒得到的组合物颗粒在烘箱中干燥0.5-2小时，然后用14-50目筛网进行整粒；(2) drying the composition granules obtained by granulating in step (1) in an oven for 0.5-2 hours, and then sizing with a 14-50 mesh screen;
(3)将整粒得到的组合物颗粒与抗氧化剂、清凉剂、崩解助剂、润滑剂等混合均匀，在压片机中压制成规格为0.5-2g/片粒的含化型无烟气烟草制品。(3) Mix the granules of the composition obtained by sizing with antioxidants, cooling agents, disintegration aids, lubricants, etc., and press them into a tablet machine to form a chemical-containing smoke-free product with a specification of 0.5-2g/tablet. gas tobacco products.
也可采取直接压片法，包括如下步骤：Also can adopt direct compression method, comprise the following steps:
(1)按配比将烟草粉末和/或烟草提取物、中药剂、矫味剂、甜味剂、香味剂、填充剂、粘合剂、乳化剂、pH调节剂、着色剂、抗氧化剂、清凉剂、崩解助剂、润滑剂混合均匀，在压片机中压制得到规格为0.5-2g/片粒的含化型无烟气烟草制品；(1) Tobacco powder and/or tobacco extract, traditional Chinese medicine, flavoring agent, sweetener, flavoring agent, filler, binder, emulsifier, pH regulator, colorant, antioxidant, cooling agent, etc. agent, disintegration aid, and lubricant are mixed evenly, and compressed in a tablet machine to obtain a chemical-containing smokeless tobacco product with a specification of 0.5-2g/tablet;
(2)将步骤(1)得到的片粒在烘箱中干燥后即得含化型无烟气烟草制品。(2) drying the flakes obtained in the step (1) in an oven to obtain a chemical-containing smokeless tobacco product.
进一步的，可对上述步骤所得的含化型无烟气烟草制品进行外包衣，即成包衣型含化型无烟气烟草制品。Further, the chemical-containing smokeless tobacco product obtained in the above steps can be coated, that is, a coated chemical-containing smokeless tobacco product.
本发明还提供了所述含化型无烟气烟草制品在烟草替代品制备领域的用途。The invention also provides the use of the chemical-containing smokeless tobacco product in the field of tobacco substitute preparation.
本发明所提供的含化型无烟气烟草制品是一种可在公共场所使用的传统卷烟的新型补充替代产品。本发明的产品可在唾液作用下发生崩解、溶解，稳定释放烟碱及烟草香提供给消费者适当的生理感受；不产生烟气，可以在公共场所使用，避免造成环境烟气污染；烟草原料中含有贵州产晾晒烟，并且通过烟草增香处理，劲头足，烟香浓郁，香味剂为食品许可使用的天然香味物质，且加入了清热润喉的中药剂，口感舒适，刺激性低。含化片含水量低，保质期长，方便携带，并且使用后无残渣，环保卫生，因此本产品是一种口感舒适、安全环保的新型无烟气烟草制品。The chemical-containing smokeless tobacco product provided by the invention is a new type of complementary and substitute product for traditional cigarettes that can be used in public places. The product of the present invention can disintegrate and dissolve under the action of saliva, and stably release nicotine and tobacco fragrance to provide consumers with appropriate physiological experience; it does not produce smoke and can be used in public places to avoid environmental smoke pollution; The raw material contains air-cured tobacco produced in Guizhou, and it has been processed by tobacco flavoring. It has a strong flavor and a strong smoke aroma. Succulent tablets have low water content, long shelf life, easy to carry, and no residue after use, which is environmentally friendly and hygienic. Therefore, this product is a new type of smokeless tobacco product with comfortable taste, safety and environmental protection.
以下通过特定的具体实例说明本发明的实施方式，本领域技术人员可由本说明书所揭露的内容轻易地了解本发明的其他优点与功效。本发明还可以通过另外不同的具体实施方式加以实施或应用，本说明书中的各项细节也可以基于不同观点与应用，在没有背离本发明的精神下进行各种修饰或改变。Embodiments of the present invention are described below through specific examples, and those skilled in the art can easily understand other advantages and effects of the present invention from the content disclosed in this specification. The present invention can also be implemented or applied through other different specific implementation modes, and various modifications or changes can be made to the details in this specification based on different viewpoints and applications without departing from the spirit of the present invention.
须知，下列实施例中未具体注明的工艺设备或装置均采用本领域内的常规设备或装置。It should be noted that the process equipment or devices not specifically indicated in the following examples all adopt conventional equipment or devices in the art.
此外应理解，本发明中提到的一个或多个方法步骤并不排斥在所述组合步骤前后还可以存在其他方法步骤或在这些明确提到的步骤之间还可以插入其他方法步骤，除非另有说明；还应理解，本发明中提到的一个或多个设备/装置之间的组合连接关系并不排斥在所述组合设备/装置前后还可以存在其他设备/装置或在这些明确提到的两个设备/装置之间还可以插入其他设备/装置，除非另有说明。而且，除非另有说明，各方法步骤的编号仅为鉴别各方法步骤的便利工具，而非为限制各方法步骤的排列次序或限定本发明可实施的范围，其相对关系的改变或调整，在无实质变更技术内容的情况下，当亦视为本发明可实施的范畴。In addition, it should be understood that one or more method steps mentioned in the present invention do not exclude that there may be other method steps before and after the combined steps or other method steps may be inserted between these explicitly mentioned steps, unless otherwise There are descriptions; it should also be understood that the combined connection relationship between one or more devices/devices mentioned in the present invention does not exclude that there may be other devices/devices before and after the combined devices/devices or those explicitly mentioned Other devices/apparatus can also be interposed between the two devices/apparatus, unless otherwise stated. Moreover, unless otherwise stated, the numbering of each method step is only a convenient tool for identifying each method step, and is not intended to limit the sequence of each method step or limit the scope of the present invention. The change or adjustment of its relative relationship is in In the case of no substantive change in the technical content, it shall also be regarded as the applicable scope of the present invention.
实施例1：Example 1:
各组分所占的重量比如下：晾晒烟(产自贵州，下同)粉末8份、中药剂4份、精盐细粉0.5份(矫味剂)、蔗糖粉39份(甜味剂)、咖啡油1.5份(香味剂)、麦芽糊精40份(填充剂)、阿拉伯胶1.5份(粘合剂)、卵磷脂0.5份(乳化剂)、微晶纤维素3.94份(崩解助剂)、金樱子棕0.05份(着色剂)、山梨酸钾0.01份(抗氧化剂)、硬脂酸镁1份(润滑剂)。其中，中药剂配方中各组分的重量比如下：布渣叶19.6份、凉粉草19.6份、鸡蛋花19.6份、杭白菊13.7份、金银花11.8份、夏枯草11.8份、甘草3.9份。The weight ratio of each component is as follows: 8 parts of air-cured tobacco (produced in Guizhou, the same below) powder, 4 parts of traditional Chinese medicine, 0.5 part of fine salt powder (flavoring agent), 39 parts of sucrose powder (sweetener), 1.5 parts of coffee oil (flavoring agent), 40 parts of maltodextrin (filler), 1.5 parts of gum arabic (binder), 0.5 parts of lecithin (emulsifier), 3.94 parts of microcrystalline cellulose (disintegration aid) , 0.05 part of golden cherry brown (colorant), 0.01 part of potassium sorbate (antioxidant), 1 part of magnesium stearate (lubricant). Among them, the weight ratio of each component in the traditional Chinese medicine formula is as follows: 19.6 parts of Buza Ye, 19.6 parts of Jelly, 19.6 parts of Frangipani, 13.7 parts of Hangbai Chrysanthemum, 11.8 parts of Honeysuckle, 11.8 parts of Prunella vulgaris, and 3.9 parts of Licorice.
制备步骤如下：The preparation steps are as follows:
a、将晾晒烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理。按照甘草：水＝1：10的比例将甘草在90-100℃下时间煎制1小时，降温、过滤后，在滤液中加入重量比为5％的蜂蜜配制成香料液，用香料液将晾晒烟浸润24-72小时，进行增香处理。a. The air-dried tobacco is naturally fermented and aged for one year, followed by stem extraction, cleaning and dehydration. According to the ratio of licorice: water = 1:10, decoct licorice at 90-100°C for 1 hour, cool down and filter, add honey with a weight ratio of 5% to the filtrate to prepare a spice liquid, and use the spice liquid to dry The smoke is infiltrated for 24-72 hours, and the flavoring treatment is carried out.
b、晾晒烟取出后，在120-140℃进行烘干至水分小于3wt％。将干燥后的烟草材料粉碎，过80目筛得到烟草粗粉。然后进行二次超微粉碎，过筛得到目粒度大于200目的晾晒烟粉末。b. After the air-dried tobacco is taken out, it is dried at 120-140°C until the moisture is less than 3wt%. The dried tobacco material is pulverized and passed through an 80-mesh sieve to obtain coarse tobacco powder. Then perform secondary ultrafine pulverization, and sieve to obtain air-dried tobacco powder with a mesh particle size greater than 200 mesh.
c、按配方称取中药材，干燥后，粉碎、筛分得到200-300目的中药材细粉。c. Weigh the Chinese medicinal materials according to the formula, and after drying, pulverize and sieve to obtain 200-300 mesh Chinese medicinal materials fine powder.
d、将阿拉伯胶、卵磷脂、咖啡油等分散在去离子水中，制备粘结剂溶液，备用；将原辅料过100目筛后，按配方称取晾晒烟粉末、中药材细粉、精盐细粉、蔗糖粉、麦芽糊精、微晶纤维素、金樱子棕，充分混合，然后利用粘结剂溶液在制粒机上用20目筛进行湿法制粒。将湿料放入厢式干燥器中，在50-80℃下干燥至物料含水量小于3wt％。然后将干料用18目筛整粒后储存备用。d. Disperse gum arabic, lecithin, coffee oil, etc. in deionized water to prepare a binder solution for later use; pass the raw and auxiliary materials through a 100-mesh sieve, weigh air-dried tobacco powder, fine powder of Chinese herbal medicines, and fine salt according to the formula powder, sucrose powder, maltodextrin, microcrystalline cellulose, and rosa japonica palm, mix thoroughly, and then use the binder solution to carry out wet granulation on a granulator with a 20-mesh sieve. Put the wet material into a box dryer and dry it at 50-80°C until the water content of the material is less than 3wt%. Then the dry material is sized with a 18-mesh sieve and stored for later use.
e、在干料中加入山梨酸钾和硬脂酸镁，搅拌均匀后喂入压片机，按照每片1.0g的规格进行压片，得到含化型无烟气烟草制品素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。e. Potassium sorbate and magnesium stearate were added to the dry material, stirred evenly, and then fed into a tablet press, and pressed according to the specification of 1.0 g per tablet, to obtain plain tablets of chemical-containing smokeless tobacco products. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
f、利用虫胶乙醇溶液、糖浆、阿拉伯胶、滑石粉、金樱子棕等原料为素片制作糖包衣，利用食用级巴西棕榈蜡进行表面抛光处理后，包装即成具有咖啡风味的含化型无烟气烟草制品。f. Use raw materials such as shellac ethanol solution, syrup, gum arabic, talcum powder, and rosa japonica to make sugar coating for plain tablets, and use food-grade carnauba wax to polish the surface, and then pack it into a coffee-flavored product. Smokeless tobacco products.
实施例2：Example 2:
各组分所占的重量比如下：烤烟粉末3.75份、晾晒烟粉末1.25份、中药剂3份、木糖醇28份(甜味剂)、山梨糖醇15份(甜味剂)、绿茶粉4份(香味剂)、玉米淀粉36份(填充剂)、黄原胶3份(粘合剂)、羧甲基淀粉钠3份(崩解助剂)、碳酸钠1份(pH调节剂)、D-异抗坏血酸钠0.05份(抗氧化剂)、巴西棕榈蜡1.95份(润滑剂)。其中，中药剂的配方中各组分的重量比如下：夏枯草47.6份、桑叶28.5份、杭白菊19.1份、甘草4.8份。The weight ratio of each component is as follows: 3.75 parts of flue-cured tobacco powder, 1.25 parts of air-cured tobacco powder, 3 parts of Chinese medicine, 28 parts of xylitol (sweetener), 15 parts of sorbitol (sweetener), green tea powder 4 parts (flavoring agent), 36 parts of corn starch (filler), 3 parts of xanthan gum (binder), 3 parts of sodium carboxymethyl starch (disintegration aid), 1 part of sodium carbonate (pH regulator) , 0.05 parts of D-sodium erythorbate (antioxidant), 1.95 parts of carnauba wax (lubricant). Wherein, the weight ratio of each component in the formula of the traditional Chinese medicine is as follows: 47.6 parts of Prunella vulgaris, 28.5 parts of mulberry leaves, 19.1 parts of Chrysanthemum chrysanthemum, and 4.8 parts of licorice.
制备步骤如下：The preparation steps are as follows:
a、将晾晒烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理，将烤烟进行烤制、陈化一年，进行抽梗、清洗、脱水处理。按照金银花：水＝1：15的比例在80-90℃下煎制1-3小时，过滤后，在滤液中加入重量比为10％的玉米糖浆配制成香料液，冷却备用。按照烤烟：晾晒烟＝3：1的比例混合，浸入香料液中，在30-60℃下浸泡24小时，进行增香处理。a. The air-dried tobacco is naturally fermented and aged for one year, followed by stem extraction, cleaning and dehydration, and the flue-cured tobacco is cured and aged for one year, followed by stem extraction, cleaning and dehydration. Fry at 80-90°C for 1-3 hours according to the ratio of honeysuckle: water = 1:15. After filtering, add corn syrup with a weight ratio of 10% to the filtrate to prepare a spice liquid, and cool it for later use. Mix according to the ratio of flue-cured tobacco: air-cured tobacco = 3:1, soak in the spice liquid, soak at 30-60°C for 24 hours, and carry out aroma-enhancing treatment.
b、从香料液中取出烟草材料，转笼脱除水分，在50-60℃下进行烘干至水分小于3wt％。将干燥后的烟草材料进行粉碎，过80目筛得到烟草粗粉。然后进行二次超微粉碎，过筛得到目粒度大于300目的混合烟草粉末。b. Take out the tobacco material from the spice liquid, remove the water by turning it in a cage, and dry it at 50-60°C until the water content is less than 3wt%. The dried tobacco material is pulverized and passed through an 80-mesh sieve to obtain coarse tobacco powder. Then perform secondary ultrafine pulverization, and sieve to obtain mixed tobacco powder with a mesh particle size greater than 300 mesh.
c、按配方称取中药材,干燥后，粉碎得到中药材颗粒。按照中药材：水＝1：10-20的重量比，将中药材颗粒浸泡30分钟，然后煎制30分钟，加水二次煎制，过滤、浓缩得到中药材水煎剂。c. Weighing the Chinese herbal medicine according to the formula, and after drying, pulverize to obtain the Chinese herbal medicine granules. According to the weight ratio of Chinese medicinal materials: water = 1:10-20, soak the Chinese medicinal material granules for 30 minutes, then decoct for 30 minutes, add water for second decoction, filter and concentrate to obtain the Chinese medicinal material water decoction.
d、将黄原胶等分散在去离子水中，制成粘结剂溶液，备用；将原辅料过100目筛后，按配方称取混合烟草粉末、中药材水煎剂、木糖醇、山梨糖醇、绿茶粉、玉米淀粉、碳酸钠、羧甲基淀粉钠、D-异抗坏血酸钠和巴西棕榈蜡，搅拌均匀后喂入压片机，按照每片1.0g的规格进行压片，得到含化型无烟气烟草制品素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。d. Disperse xanthan gum in deionized water to make a binder solution for later use; after passing the raw and auxiliary materials through a 100-mesh sieve, weigh mixed tobacco powder, Chinese herbal medicine water decoction, xylitol, and sorbic acid according to the formula Sugar alcohol, green tea powder, cornstarch, sodium carbonate, sodium carboxymethyl starch, D-sodium erythorbate and carnauba wax are fed into the tablet machine after being stirred evenly, and are pressed into tablets according to the specification of 1.0g per tablet to obtain Plain flakes of smokeless tobacco products. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
e、将片粒在烘箱中干燥后即得含化型无烟气烟草制品素片。e. After the tablets are dried in an oven, the plain sheets of chemical-containing smokeless tobacco products are obtained.
f、利用明胶、糖浆、滑石粉、绿茶酊等原料为素片制作糖包衣，利用川蜡进行表面抛光处理后，包装即成具有绿茶风味的含化型无烟气烟草制品。f. Use gelatin, syrup, talcum powder, green tea tincture and other raw materials as raw materials to make sugar-coated plain tablets, use Sichuan wax to polish the surface, and pack them into chemical-containing smokeless tobacco products with green tea flavor.
实施例3：Example 3:
各组分所占的重量比如下：晾晒烟粉末16份、香料烟粉末4份、柠檬酸钾0.999份(pH调节剂)、木糖醇35份(甜味剂)、甜菊糖苷0.001份(甜味剂)、乌梅酊1.8份(香味剂)、环糊精30份(填充剂)、磷酸钙1份(填充剂)、海藻酸钠5份(粘合剂)、大豆磷脂0.94份(乳化剂)、结冷胶4.5份(崩解助剂)、薄荷油0.2份(清凉剂)、黑加仑红0.05份(着色剂)、鼠尾草酸0.01份(抗氧化剂)、氢化植物油0.5份(润滑剂)。The weight ratio of each component is as follows: 16 parts of air-cured tobacco powder, 4 parts of oriental tobacco powder, 0.999 parts of potassium citrate (pH regulator), 35 parts of xylitol (sweetener), 0.001 part of steviol glycoside (sweetener) Flavor), 1.8 parts of ebony tincture (flavor), 30 parts of cyclodextrin (filler), 1 part of calcium phosphate (filler), 5 parts of sodium alginate (binder), 0.94 parts of soybean lecithin (emulsifier ), 4.5 parts of gellan gum (disintegration aid), 0.2 parts of peppermint oil (cooling agent), 0.05 parts of blackcurrant red (colorant), 0.01 part of carnosic acid (antioxidant), 0.5 parts of hydrogenated vegetable oil (lubricant ).
制备步骤如下：The preparation steps are as follows:
a、将晾晒烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理，然后在80-90℃水中热处理1-2小时，取出后转笼脱除水分，在40-60℃下进行烘干。按照晾晒烟：香料烟＝4：1的重量比混合、粉碎，过80目筛得到烟草粗粉。然后进行二次超微粉碎，过筛得到目粒度大于400目的混合烟草粉末。a. Naturally ferment and age the air-dried tobacco for one year, then remove the stems, wash and dehydrate, then heat-treat in water at 80-90°C for 1-2 hours, take it out and turn it in a cage to remove water, and carry out at 40-60°C drying. According to the weight ratio of air-dried tobacco: oriental tobacco = 4:1, mix and pulverize, and pass through an 80-mesh sieve to obtain coarse tobacco powder. Then perform secondary ultrafine pulverization, and sieve to obtain mixed tobacco powder with a mesh size greater than 400 mesh.
b、将重量比为1％康酿克油、5％β-环糊精分散在乙醇中，强力搅拌、混合均匀制成香料液，均匀喷洒在烟草细粉中，以不结块为准，平衡水分后即得增香混合烟草粉末。b. Disperse 1% konjac oil and 5% beta-cyclodextrin in ethanol in a weight ratio, vigorously stir and mix evenly to make a spice liquid, and evenly spray it in the tobacco fine powder, subject to no agglomeration, After balancing the moisture, the flavored mixed tobacco powder is obtained.
c、将海藻酸钠、结冷胶、乌梅酊、大豆磷脂等分散在去离子水中，制成粘结剂溶液，备用；将原辅料过100目筛后，按配方称取混合烟草粉末、柠檬酸钾、木糖醇、甜菊糖苷、环糊精、磷酸钙、黑加仑红等，充分混合，利用粘结剂溶液在制粒机上用18目筛进行湿法制粒。将湿料放入厢式干燥器中，在50-60℃下干燥至物料含水量小于3wt％。然后将干料用16目筛整粒后储存备用。c. Disperse sodium alginate, gellan gum, ebony tincture, soybean lecithin, etc. in deionized water to make a binder solution for later use; after passing the raw and auxiliary materials through a 100-mesh sieve, weigh the mixed tobacco powder, lemon Potassium phosphate, xylitol, steviol glycoside, cyclodextrin, calcium phosphate, blackcurrant red, etc., fully mixed, using the binder solution to carry out wet granulation on a granulator with an 18-mesh sieve. Put the wet material into a box dryer and dry it at 50-60°C until the water content of the material is less than 3wt%. Then the dry material is sized with a 16-mesh sieve and stored for later use.
d、在干料中加入鼠尾草酸、薄荷油、氢化植物油等，搅拌均匀后喂入压片机，按照每片0.5g的规格进行压片，得到含化型无烟气烟草制品素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。d. Add carnosic acid, peppermint oil, hydrogenated vegetable oil, etc. to the dry material, stir evenly, and then feed it into a tablet machine, and perform tableting according to the specification of 0.5g per tablet, to obtain plain tablets of chemical-containing smokeless tobacco products. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
e、利用麦芽糖醇、明胶、黑加仑红、乌梅酊等原料为素片制作糖包衣，利用小烛树蜡和巴西棕榈蜡进行表面抛光处理后，包装即成具有梅子风味的含化型无烟气烟草制品。e. Use maltitol, gelatin, blackcurrant red, ebony tincture and other raw materials to make sugar coating for plain tablets, use candelilla wax and carnauba wax to polish the surface, and pack it into a plum-flavored non-chemical Smoke from tobacco products.
实施例4：Example 4:
各组分所占的重量比如下：烟草提取物复合物20份、异麦芽酮糖30份(甜味剂)、玉米糖浆10份(甜味剂)、水果提取物9份(香味剂)、康酿克油1份(香味剂)、D-甘露糖醇25份(填充剂)、羧甲基纤维素钠1.4份(粘合剂)、三乙酸甘油酯0.5份(乳化剂)、交联聚乙烯基吡咯烷酮1.994份(崩解助剂)、薄荷醇0.1份(清凉剂)、叶黄素0.001份(着色剂)、竹叶抗氧化物0.005份(抗氧化剂)、微晶石蜡1份(润滑剂)。The weight ratio of each component is as follows: 20 parts of tobacco extract compound, 30 parts of isomaltulose (sweetener), 10 parts of corn syrup (sweetener), 9 parts of fruit extract (flavoring agent), 1 part of konjac oil (flavor agent), 25 parts of D-mannitol (filler), 1.4 parts of sodium carboxymethylcellulose (binder), 0.5 part of glyceryl triacetate (emulsifier), cross-linking 1.994 parts of polyvinylpyrrolidone (disintegration aid), 0.1 part of menthol (cooling agent), 0.001 part of lutein (colorant), 0.005 part of bamboo leaf antioxidant (antioxidant), 1 part of microcrystalline paraffin ( lubricant).
制备步骤如下：The preparation steps are as follows:
a、将晾晒烟自然发酵、陈化一年，烤烟烤制、陈化一年，进行抽梗、清洗、脱水处理，在40-60℃下进行烘干。将香料烟在40-60℃下进行烘干。在按照烤烟：晾晒烟：香料烟＝5：3：2的重量比混合、粉碎，利用溶剂浸提法或者超临界萃取法制得混合烟草提取物。a. The air-dried tobacco is naturally fermented and aged for one year, and the flue-cured tobacco is cured and aged for one year, followed by stem extraction, cleaning, dehydration, and drying at 40-60°C. The oriental tobacco is dried at 40-60°C. The mixed tobacco extract is obtained by mixing and pulverizing flue-cured tobacco: air-dried tobacco: oriental tobacco in a weight ratio of 5:3:2, and using a solvent extraction method or a supercritical extraction method.
b、将重量比为5％烟草提取物、15％β-环糊精、5％明胶、5％阿拉伯胶分散在去离子水中，强力搅拌成均匀乳状液，喷雾干燥形成烟草提取物复合物。b. Disperse 5% tobacco extract, 15% β-cyclodextrin, 5% gelatin, and 5% gum arabic in deionized water by weight, stir vigorously to form a uniform emulsion, and spray dry to form a tobacco extract compound.
c、将羧甲基纤维素钠、水果提取物、康酿克油、三乙酸甘油酯和一半重量的交联聚乙烯基吡咯烷酮等分散在去离子水中，制成粘结剂溶液，备用；将原辅料过100目筛后，按配方称取有烟草提取物复合物、异麦芽酮糖、玉米糖浆、D-甘露糖醇、叶黄素等，充分混合，利用粘结剂溶液在制粒机上用20目筛进行湿法制粒。将湿料放入厢式干燥器中，在50-60℃下干燥至物料含水量小于3wt％。然后将干料用20目筛整粒后储存备用。c. Disperse sodium carboxymethyl cellulose, fruit extracts, Kang Nong Ke oil, glycerol triacetate and half of the weight of cross-linked polyvinylpyrrolidone in deionized water to make a binder solution for subsequent use; After the raw and auxiliary materials pass through a 100-mesh sieve, weigh tobacco extract compound, isomaltulose, corn syrup, D-mannitol, lutein, etc. according to the formula, mix them thoroughly, and use the binder solution on the granulator Wet granulation was carried out with a 20-mesh sieve. Put the wet material into a box dryer and dry it at 50-60°C until the water content of the material is less than 3wt%. Then the dry material is sized with a 20-mesh sieve and stored for later use.
d、在干料中加入竹叶抗氧化物、薄荷醇、另一半重量的交联聚乙烯基吡咯烷酮、微晶石蜡等，搅拌均匀后喂入压片机，按照每片0.5g的规格进行压片，得到含化型无烟气烟草制品素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。d. Add bamboo leaf antioxidants, menthol, the other half of the weight of cross-linked polyvinylpyrrolidone, microcrystalline paraffin, etc. to the dry material, stir well and feed it into the tablet press, and press it according to the specification of 0.5g per tablet Tablets to obtain chemical-containing smokeless tobacco product plain sheets. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
e、利用异麦芽酮糖、玉米糖浆、薄荷醇、普鲁兰多糖等原料为素片制作糖包衣，利用聚乙二醇、蜂蜡进行表面抛光处理后，包装即成具有水果风味的含化型无烟气烟草制品。e. Use isomaltulose, corn syrup, menthol, pullulan and other raw materials to make sugar coating for plain tablets, use polyethylene glycol and beeswax to polish the surface, and pack it into a fruit-flavored containing chemical type smokeless tobacco products.
对比例：Comparative example:
将烤烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理。在120-140℃烘干至水分小于3wt％。将干燥后的烟草材料粉碎，筛分得到目粒度大于300目的烤烟粉末。其他制备步骤、工艺参数、配方组成和实施例1相同，仅将烟草粉末的种类变更为烤烟，且未进行增香处理，白砂糖粉变更为40份，麦芽糊精变更为42份，微晶纤维素变更为4.94份，对比例中未添加中药剂。The flue-cured tobacco is naturally fermented and aged for one year, followed by stem extraction, cleaning and dehydration. Dry at 120-140°C until the moisture is less than 3wt%. The dried tobacco material is pulverized and sieved to obtain flue-cured tobacco powder with a mesh particle size greater than 300 mesh. Other preparation steps, process parameters, and formula composition are the same as in Example 1, only the type of tobacco powder is changed to flue-cured tobacco, and no flavoring treatment is performed, white sugar powder is changed to 40 parts, maltodextrin is changed to 42 parts, microcrystalline The cellulose was changed to 4.94 parts, and no traditional Chinese medicine was added in the comparative example.
将实施例1-4以及对比例所制备的含化型无烟气烟草制品进行感官评价测试，各指标评价等级分为6级，分别为0分＝几乎感受不到，1分＝很低，2分＝较低，3分＝一般，4分＝较强，5分＝很强，最小计分单位为0.5分。入口口感是指含化型无烟气烟草制品放入口腔后，使用者的初始综合感受。生理强度是指在使用过程中，使用者所感受到的生理满足感，即劲头。香料香是指在使用过程中，使用者所感受到的香味剂的量和质。烟草香是指在使用过程中，使用者所感受到的烟草香的量和质。刺激感是指在使用过程中，使用者口腔、咽喉、食道等部位所感受到辛辣、不适等刺激性感受。舒适感是指在使用过程中，使用者所感受到香味协调性、舒适性、无残渣异物感等愉悦性感受。释放均匀性是指在使用过程中，使用者所感受到香味、生理强度等随时间的释放稳定性。释放持久性是指在使用过程中，使用者所感受到香味、生理强度等持续时间长短。口腔余味是指在使用过程后，使用者口腔所残余的味觉感受。刺激感越强，得分越低；口腔余味感受越好，得分越高；其他项目是感受越强，得分越高；最后得分由各分项得分的算术加和得到。具体结果如表1所示：The chemical-containing smokeless tobacco products prepared in Examples 1-4 and Comparative Examples were subjected to sensory evaluation tests, and the evaluation grades of each index were divided into 6 grades, respectively 0 points = hardly felt, 1 point = very low, 2 points = low, 3 points = average, 4 points = strong, 5 points = very strong, the minimum scoring unit is 0.5 points. The mouthfeel refers to the initial comprehensive feeling of the user after the chemical-containing smokeless tobacco product is put into the mouth. Physiological strength refers to the physiological satisfaction felt by the user during use, that is, energy. Fragrance fragrance refers to the quantity and quality of the fragrance agent felt by the user during use. Tobacco aroma refers to the quantity and quality of tobacco aroma experienced by users during use. Stimulation refers to the irritating sensations such as pungentness and discomfort felt by users in the mouth, throat, esophagus and other parts during use. Comfort refers to pleasant feelings such as fragrance coordination, comfort, and no residue foreign body sensation that users feel during use. The release uniformity refers to the release stability over time of the user's perception of fragrance, physiological strength, etc. during use. Release duration refers to the duration of fragrance and physiological intensity felt by users during use. Oral aftertaste refers to the remaining taste sensation in the user's mouth after use. The stronger the stimulation, the lower the score; the better the mouth aftertaste, the higher the score; the stronger the other items, the higher the score; the final score is obtained by the arithmetic sum of the scores of each sub-item. The specific results are shown in Table 1:
表1含化型无烟气烟草制品的烟碱释放量和感官评价指标对比结果Table 1 Comparison results of nicotine release and sensory evaluation indicators of chemical-containing smokeless tobacco products
由表1可见，基于贵州产晾晒烟制备的含化型无烟气烟草制品具有烟香浓郁、口感舒适、刺激性小的特点，综合指标评价优于基于常规烤烟所制备的含化型无烟气烟草制品。It can be seen from Table 1 that the chemical-containing smokeless tobacco products prepared based on air-cured tobacco produced in Guizhou have the characteristics of rich aroma, comfortable taste and low irritation, and the comprehensive index evaluation is better than the chemical-containing smokeless tobacco products based on conventional flue-cured tobacco. gas tobacco products.
综上所述，本发明有效克服了现有技术中的种种缺点而具高度产业利用价值。To sum up, the present invention effectively overcomes various shortcomings in the prior art and has high industrial application value.
上述实施例仅例示性说明本发明的原理及其功效，而非用于限制本发明。任何熟悉此技术的人士皆可在不违背本发明的精神及范畴下，对上述实施例进行修饰或改变。因此，举凡所属技术领域中具有通常知识者在未脱离本发明所揭示的精神与技术思想下所完成的一切等效修饰或改变，仍应由本发明的权利要求所涵盖。The above-mentioned embodiments only illustrate the principles and effects of the present invention, but are not intended to limit the present invention. Anyone skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Therefore, all equivalent modifications or changes made by those skilled in the art without departing from the spirit and technical ideas disclosed in the present invention should still be covered by the claims of the present invention.
| Application Number | Priority Date | Filing Date | Title |
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| CN201410788564.6ACN105747267A (en) | 2014-12-17 | 2014-12-17 | Dissolvable smoke-free tobacco product and preparation method thereof |
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| CN201410788564.6ACN105747267A (en) | 2014-12-17 | 2014-12-17 | Dissolvable smoke-free tobacco product and preparation method thereof |
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| CN105747267Atrue CN105747267A (en) | 2016-07-13 |
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| CN201410788564.6APendingCN105747267A (en) | 2014-12-17 | 2014-12-17 | Dissolvable smoke-free tobacco product and preparation method thereof |
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