The preparation method of the electronic cigarette liquid of grape flavorTechnical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of electronic cigarette liquid and preparation method thereof, particularly relate to a kind of PortugalElectronic cigarette liquid of grape local flavor and preparation method thereof.
Background technology
Electronic cigarette has another name called electronic cigarette, has the outward appearance similar to Medicated cigarette and the taste of medicated cigarette approximation, the same also like Medicated cigaretteEnergy sucking-off cigarette, sucking-off taste and sensation are come.Electronic cigarette does not has other harmful components such as the tar in Medicated cigarette, suspended particulates, the most severalDo not produce second hand smoking.
The fragrance of electronic cigarette and mouthfeel derive from electronic cigarette liquid, and the composition of electronic cigarette liquid is mainly essence and flavoring agent, and Nicotiana tabacum L. carriesTake thing and propylene glycol, glycerol equal solvent.In order to cater to the consumption habit of consumer's diversification, during the electronic cigarette on market hasThe brand cigarette tastes such as China, Yuxi, also have the non-tobacco tastes such as Herba Menthae, cocoa, Rhizoma et radix valerianae.At present, the fruity without nicotineElectronic cigarette is quite welcome by consumer with its pure and fresh sweet mouthfeel.
Summary of the invention
Solve the technical problem that: fruity electronic cigarette mainly brings sense by its pure and fresh sweet mouthfeel to consumerPleasurable sensation on official, but the mouthfeel of fruity electronic cigarette in the market is universal sweet greasy, and pleasant impression is the cleanest, it is impossible to meets and disappearsThe requirement of sense of the person of expense.
Technical scheme: for above-mentioned technical problem, the invention discloses the electronic cigarette liquid of a kind of grape flavor, described PortugalThe electronic cigarette liquid of grape local flavor consists of the following composition: propylene glycol, glycerol, 1,3 butylene glycol, xylitol liquid, Sucus Vitis viniferae concentrated solution andTable grapes essence.
Preferably, in the electronic cigarette liquid of described a kind of grape flavor, the parts by weight of each component are: propylene glycol is 1-80Part, glycerol be 1-60 part, 1,3 butylene glycol be 1-50 part, xylitol liquid be 1-30 part, Sucus Vitis viniferae concentrated solution be 5-10 part, edibleGrape essence is 0.1-2 part.
Preferably, the electronic cigarette liquid of described a kind of grape flavor is sundown.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, described table grapes essence is composed of the following components:Methyl 2-aminobenzoate, N-methyl anthranilic acid methyl ester, ethyl acetate, ethyl n-butyrate., isoamyl acetate, 2-methyl fourthAcetoacetic ester, maltol, 2-methyl butanol, phenethanol, trans-2-hexenol, citral, Alcohols,fusel, white lemon oil, oranger terpene,Cognac green oil and propylene glycol.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, the weight of each component in described table grapes essenceNumber is: methyl 2-aminobenzoate be 3-6 part, N-methyl anthranilic acid methyl ester be 2-7 part, ethyl acetate be 1-5 part,Ethyl n-butyrate. be 0.1-1 part, isoamyl acetate be 0.1-1 part, ethyl 2-methylbutyrate be 0.1-1 part, maltol be 0.1-1Part, 2-methyl butanol be 1-5 part, phenethanol be 0.1-1 part, trans-2-hexenol be 0.01-1 part, citral be 0.01-1 part,Alcohols,fusel be 1-5 part, white lemon oil be 0.1-1 part, oranger terpene be 0.1-1 part, cognac green oil be 0.1-1 part, propylene glycolFor 70-90 part.
Preferably, the electronic cigarette liquid of described a kind of grape flavor, described Sucus Vitis viniferae concentrated solution is that Fructus Vitis viniferae squeezing is extractedAfter the Sucus Vitis viniferae concentrated solution that is concentrated to give.
Preferably, described Sucus Vitis viniferae concentrated solution preparation method comprises the following steps: (1) weighs clean Fructus Vitis viniferae, uses groupKnit bruisher to smash to pieces；(2) carry out squeezing with small-sized basket squeezer and obtain original grape juice；(3) original grape juice decompression is rotatedEvaporation and concentration becomes thick liquid, standby.
Preferably, the temperature that the rotary evaporation that reduces pressure in the preparation method of described Sucus Vitis viniferae concentrated solution concentrates is 50 DEG C, veryReciprocal of duty cycle is 0.095 Mpa, and the Baume degrees of final gained Sucus Vitis viniferae concentrated solution is at 50-55 ° of Bx.
The preparation method of the electronic cigarette liquid of a kind of grape flavor, comprises the steps: that (1) weighs clean Fructus Vitis viniferae, uses groupKnit bruisher to smash to pieces；(2) carry out squeezing with small-sized basket squeezer and obtain original grape juice；(3) original grape juice decompression is rotatedEvaporation and concentration becomes thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095 Mpa, is concentrated into Baume degrees and reaches 50-After 55 ° of Bx standby；(4) methyl 2-aminobenzoate 3-6 part, N-methyl anthranilic acid methyl ester 2-7 part, ethyl acetate 1-are taken5 parts, ethyl n-butyrate. 0.1-1 part, isoamyl acetate 0.1-1 part, ethyl 2-methylbutyrate 0.1-1 part, maltol 0.1-1 part, 2-Methyl butanol 1-5 part, phenethanol 0.1-1 part, trans-2-hexenol 0.01-1 part, citral 0.01-1 part, Alcohols,fusel 1-5 part, whiteFructus Citri Limoniae oil 0.1-1 part, oranger terpene 0.1-1 part, cognac green oil 0.1-1 part, propylene glycol 70-90 part, mix mentioned componentAfter obtain table grapes essence；(5) propylene glycol 1-80 part, glycerol 1-60 part, 1,3 butylene glycol 1-50 part, xylitol liquid 1-30 are takenPart, Sucus Vitis viniferae concentrated solution 5-10 part, Fructus Vitis viniferae edible essence 0.1-2 part, prepare grape flavor after being mixed by mentioned componentElectronic cigarette liquid.
The described xylitol aqueous solution that xylitol liquid is 20wt% to 50wt%.
Beneficial effect: the electronic cigarette liquid of the grape flavor prepared by the preparation method of the present invention is sundown,Overcome fruity electronic cigarette mouthfeel universal sweet greasy, pleasant impression is the cleanest, it is impossible to the shortcoming meeting consumer sensory's demand, the present inventionElectronic cigarette liquid suction time be provided that fresh and sweet Fructus Vitis viniferae fragrance, mouthfeel is soft and moist and pleasant impression is the most comfortable, and described electronic cigaretteThe preparation method of liquid is easy, and constant product quality can be widely applied in electronic cigarette product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 4 parts, N-methyl anthranilic acid methyl ester 5 parts, ethyl acetate 2 parts, butanoic acid are taken by weightEthyl ester 0.4 part, isoamyl acetate 0.5 part, ethyl 2-methylbutyrate 0.5 part, maltol 0.6 part, 2-methyl butanol 1 part, benzene secondAlcohol 0.1 part, trans-2-hexenol 0.05 part, citral 0.01 part, Alcohols,fusel 1 part, white lemon oil 0.1 part, oranger terpene 0.1 part,Cognac green oil 0.1 part, propylene glycol 80 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 50 parts, glycerol 20 parts, 1,3 butylene glycol 10 parts, the xylitol liquid 5 parts of 20wt%, Sucus Vitis viniferae are taken by weight denseContracting liquid 9.5 parts, 0.5 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Embodiment 2
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 3 parts, N-methyl anthranilic acid methyl ester 7 parts, ethyl acetate 5 parts, butanoic acid are taken by weightEthyl ester 0.1 part, isoamyl acetate 0.1 part, ethyl 2-methylbutyrate 0.1 part, maltol 0.1 part, 2-methyl butanol 2.5 parts, benzeneEthanol 0.5 part, trans-2-hexenol 0.01 part, citral 0.03 part, Alcohols,fusel 2 parts, white lemon oil 0.4 part, oranger terpene 0.2Part, cognac green oil 0.5 part, propylene glycol 70 parts, obtain table grapes essence after being mixed by mentioned component；
(3) propylene glycol 80 parts, glycerol 1 part, 1,3 butylene glycol 1 part, the xylitol liquid 30 parts of 40wt%, Sucus Vitis viniferae are taken by weight denseContracting liquid 10 parts, 0.1 part of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
Embodiment 3
(1) weigh clean Fructus Vitis viniferae, smash to pieces with tissue mashing machine；Carry out squeezing with small-sized basket squeezer and obtain original grape juice；Original grape juice decompression rotary evaporation is condensed into thick liquid, and the temperature of evaporation and concentration is 50 DEG C, and vacuum is 0.095Mpa, is concentrated into after Baume degrees reaches 50-55 ° of Bx standby；
(2) methyl 2-aminobenzoate 6 parts, N-methyl anthranilic acid methyl ester 2 parts, ethyl acetate 1 part, butanoic acid are taken by weightEthyl ester 1 part, isoamyl acetate 1 part, ethyl 2-methylbutyrate 1 part, maltol 1 part, 2-methyl butanol 5 parts, phenethanol 1 part, trans-2-hexenol 1 part, citral 1 part, Alcohols,fusel 5 parts, white lemon oil 1 part, oranger terpene 1 part, cognac green oil 1 part, propylene glycol90 parts, after being mixed by mentioned component, obtain table grapes essence；
(3) propylene glycol 1 part, glycerol 60 parts, 1,3 butylene glycol 50 parts, the xylitol liquid 1 part of 50wt%, Sucus Vitis viniferae are taken by weight denseContracting liquid 5 parts, 2 parts of mix homogeneously of table grapes essence, obtain the electronic cigarette liquid of grape flavor.
The embodiment 1 prepared, embodiment 2, the grape flavor electronic cigarette liquid of embodiment 3 are taken 0.5mL and add to electricityIn sub-cigarette, and separately take after commercially available table grapes essence propylene glycol is diluted to 0.3wt%, take the commercially available edible Portugal of 0.3wt% of 0.5mLGrape essence diluent adds to electronic cigarette, as a comparison case, carries out integrated sensory's quality evaluation.Result is as follows:
Embodiment 1: flue gas is full, Fructus Vitis viniferae gives off a strong fragrance, mouthfeel is soft, pleasant impression is comfortable.
Embodiment 2: exquisiteness that flue gas is strong, Fructus Vitis viniferae fragrance is soft and moist, mouthfeel is fresh and sweet, pleasant impression are clean.
Embodiment 3: flue gas is strong, Fructus Vitis viniferae soft aroma and, delicate mouthfeel, pleasant impression clean.
Comparative example: flue gas is strong, Fructus Vitis viniferae fragrance coordinate, mouthfeel sweet greasy, pleasant impression is not good enough.
Can be seen that from result, the electronic cigarette liquid of the grape flavor prepared by the preparation method of the present invention is had clearlySweet Fructus Vitis viniferae fragrance, mouthfeel is soft and moist and pleasant impression is the most comfortable, and the preparation method of described electronic cigarette liquid is easy, and product quality is steadyFixed, can be widely applied in electronic cigarette product.