技术领域technical field
本发明涉及烟草制品，具体地说，涉及一种烟草含化片及其制备方法。The invention relates to tobacco products, in particular to a tobacco containing sheet and a preparation method thereof.
背景技术Background technique
可燃吸烟草制品产生的烟雾中含有危害人体健康的有害成分。中国是世界上最大的烟草生产国和消费国，我国吸烟人群超过3亿，另有约7.4亿不吸烟人群遭受二手烟的危害，吸烟的危害性已经成为一种严重的公共卫生问题。2006年1月，《世界卫生组织烟草控制框架公约》在我国正式生效，政府正全力推进公共场所全面禁止吸烟，传统卷烟在产销、消费等多个环节受到越来越多的管控。无烟气烟草制品以非燃烧的形式向消费者提供类似于吸食传统卷烟的生理满足感，主要包括口含型(不咀嚼，有残渣)、含化型(不咀嚼，无残渣)、胶基型(咀嚼，有残渣)烟草制品等。无烟气烟草制品不产生可燃吸烟草制品烟雾中的有害成分，避免了二手烟的危害，可以作为传统卷烟的补充替代产品，对于保护公众健康具有重要意义。The smoke produced by combustible smoking tobacco products contains harmful components that are harmful to human health. China is the world's largest tobacco producer and consumer. There are more than 300 million smokers in my country, and about 740 million non-smokers suffer from second-hand smoke. The harmfulness of smoking has become a serious public health problem. In January 2006, the "World Health Organization Framework Convention on Tobacco Control" came into effect in my country. The government is fully promoting the ban on smoking in public places. Traditional cigarettes are subject to more and more controls in production, sales, consumption and other links. Smokeless tobacco products provide consumers with the physiological satisfaction similar to smoking traditional cigarettes in a non-combustible form, mainly including buccal type (no chewing, residue), containing type (no chewing, no residue), gum base Type (chewing, residue) tobacco products, etc. Smokeless tobacco products do not produce harmful components in the smoke of combustible tobacco products and avoid the harm of second-hand smoke. They can be used as supplementary alternatives to traditional cigarettes and are of great significance for protecting public health.
含化型无烟气烟草制品是将烟草细粉或者烟草提取物与其他添加剂混合后压制成一定形状，使用时在口腔中发生崩解、溶解等过程，较平稳地释放烟碱、香味物质等有效成分而提供给消费者一定的生理满足感，无烟气产生，使用方便，国内消费者容易接受，是一种在国内市场有很好发展前景的新型无烟气烟草制品。国外含化型无烟气烟草制品主要通过单纯在产品中添加烟碱的方式提供生理满足感，起到一定的替代吸烟的效果，不能降低吸烟者对烟碱的依赖，并且游离态的烟碱释放快，产品无烟草香气。Chemical-containing smokeless tobacco products are made by mixing tobacco fine powder or tobacco extracts with other additives and pressing them into a certain shape. During use, they disintegrate and dissolve in the oral cavity, releasing nicotine and flavor substances more smoothly. It is a new type of smokeless tobacco product with good development prospects in the domestic market. Foreign chemical-containing smokeless tobacco products mainly provide physiological satisfaction by simply adding nicotine to the product, which can replace smoking to a certain extent, and cannot reduce smokers' dependence on nicotine, and the release of free nicotine Fast, the product has no tobacco aroma.
发明内容Contents of the invention
为了解决现有技术中存在的问题，本发明的目的是提供一种烟草含化片及其制备方法。In order to solve the problems existing in the prior art, the object of the present invention is to provide a tobacco containing sheet and a preparation method thereof.
为了实现本发明目的，本发明首先提供一种烟草含化片，其原料按重量份计，包括如下组分：In order to achieve the purpose of the present invention, the present invention firstly provides a tobacco-containing chemical sheet, the raw materials of which include the following components in parts by weight:
所述烟草含化片中的烟碱含量为0.005-6mg/g；The nicotine content in the tobacco-containing tablets is 0.005-6 mg/g;
所述烟草材料包括烟草粉末和/或烟草提取物。The tobacco material includes tobacco powder and/or tobacco extract.
优选地，所述烟草含化片，其原料按重量份计，包括如下组分：Preferably, the raw materials of the tobacco-containing sheet include the following components in parts by weight:
进一步地，所述玛卡组合物包括玛卡粉或玛卡提取物；Further, the Maca composition includes Maca powder or Maca extract;
或者所述玛卡组合物包括玛卡粉或玛卡提取物与蜂花粉、辣木提取物、绞股蓝提取物、枸杞提取物、菊粉、阿萨依果提取物、卡姆果提取物、可乐果提取物、瓜拉纳提取物、释迦提取物、苜蓿提取物、诺丽果提取物、达米阿那提取物中一种或多种的组合；Or the Maca composition includes Maca powder or Maca extract and bee pollen, Moringa extract, Jiaogulan extract, wolfberry extract, inulin, Acai fruit extract, camu camu extract, A combination of one or more of Dimethoate Extract, Guarana Extract, Sakyamuni Extract, Alfalfa Extract, Noni Fruit Extract, Damiana Extract;
优选地，所述玛卡组合物的配方是：玛卡提取物30-60份、蜂花粉20-40份、辣木提取物10-30份、瓜拉纳提取物5-15份；Preferably, the formula of the Maca composition is: 30-60 parts of Maca extract, 20-40 parts of bee pollen, 10-30 parts of Moringa extract, and 5-15 parts of Guarana extract;
或：玛卡提取物20-40份、枸杞提取物20-40份、绞股蓝提取物10-30份、卡姆果提取物10-30份；Or: 20-40 parts of maca extract, 20-40 parts of wolfberry extract, 10-30 parts of Jiaogulan extract, 10-30 parts of camu camu extract;
或：玛卡提取物40-70份、菊粉10-30份、阿萨依果提取物5-20份、释迦提取物5-20份；Or: 40-70 parts of Maca extract, 10-30 parts of inulin, 5-20 parts of Acai fruit extract, 5-20 parts of Sakyamuni extract;
或：玛卡提取物40-60份、可乐果提取物10-30份、苜蓿提取物5-15份、诺丽果提取物5-15份、达米阿那提取物5-15份。Or: 40-60 parts of maca extract, 10-30 parts of kola nut extract, 5-15 parts of alfalfa extract, 5-15 parts of noni fruit extract, 5-15 parts of damiana extract.
玛卡是一种原产于南美洲安第斯山区的十字花科独行菜属植物，具有丰富的营养价值和保健功效。但是直接食用或者机械粉碎无法将植物细胞内的有效成分完全释放。为了提高有效成分的溶出率和人体吸收率，本发明技术方案中使用的玛卡组分为玛卡超微粉或玛卡提取物。Maca is a cruciferous plant native to the Andes in South America. It has rich nutritional value and health benefits. However, direct consumption or mechanical crushing cannot fully release the active ingredients in the plant cells. In order to improve the dissolution rate and human body absorption rate of active ingredients, the Maca component used in the technical solution of the present invention is Maca superfine powder or Maca extract.
玛卡本身带有较为强烈的辛辣、苦涩口感，本发明技术方案中将玛卡组分与优选的其他植物组分进行复配，有效改善玛卡的口感质量，并且提高玛卡组合物的使用效果。Maca itself has a relatively strong spicy and bitter taste. In the technical solution of the present invention, the Maca component is compounded with other preferred plant components to effectively improve the taste quality of Maca and increase the use of the Maca composition. Effect.
优选地，所述玛卡粉的制备方法是：Preferably, the preparation method of described Maca powder is:
(1)将新鲜玛卡清洗后，切成厚度1-5mm的片状，然后利用冷冻干燥或低温干燥技术将玛卡水分干燥至低于5％。冷冻干燥的温度为-20--45℃，真空度为10-30Pa。低温干燥的温度为30-60℃，真空度为100-200Pa。(1) After cleaning the fresh Maca, cut it into slices with a thickness of 1-5 mm, and then use freeze-drying or low-temperature drying technology to dry the Maca moisture to less than 5%. The freeze-drying temperature is -20--45°C, and the vacuum degree is 10-30Pa. The temperature of low-temperature drying is 30-60°C, and the degree of vacuum is 100-200Pa.
(2)将干燥后的玛卡切片粉碎、筛分，得到20-100目的粗粉。(2) Grinding and sieving the dried Maca slices to obtain coarse powder of 20-100 mesh.
(3)利用低温气流超微粉碎机将玛卡粗粉进行二次粉碎，筛分得到玛卡超微粉。(3) Using a low-temperature airflow ultrafine pulverizer to pulverize the Maca coarse powder for a second time, and sieve to obtain the Maca superfine powder.
更优选地，所述玛卡粉的粒度大于200目。More preferably, the particle size of the maca powder is greater than 200 mesh.
进一步优选地，所述玛卡粉的粒度为大于2000目。Further preferably, the particle size of the maca powder is greater than 2000 mesh.
优选地，所述玛卡提取物的制备方法是：Preferably, the preparation method of the Maca extract is:
(1)将新鲜玛卡清洗后，切成厚度1-5mm的片状，然后利用冷冻干燥或低温干燥技术将玛卡水分干燥至低于5％。将干燥后的玛卡切片粉碎、筛分，得到20-100目的粗粉。(1) After cleaning the fresh Maca, cut it into slices with a thickness of 1-5 mm, and then use freeze-drying or low-temperature drying technology to dry the Maca moisture to less than 5%. The dried Maca slices are pulverized and sieved to obtain a coarse powder of 20-100 mesh.
(2)利用95％乙醇作为提取剂，提取剂与玛卡粉的比例为10：1-30：1，在50-80℃下萃取1-5小时，分离、真空浓缩得到玛卡醇提物。(2) Use 95% ethanol as the extractant, the ratio of the extractant to Maca powder is 10:1-30:1, extract at 50-80°C for 1-5 hours, separate and concentrate in vacuo to obtain Maca ethanol extract .
(3)将(2)中提取后的滤渣加入10-20倍水，在80-100℃下萃取0.5-3小时，分离、真空浓缩得到玛卡水提物。(3) Add 10-20 times of water to the filter residue extracted in (2), extract at 80-100° C. for 0.5-3 hours, separate and concentrate in vacuo to obtain Maca water extract.
(4)将玛卡醇提物和水提物按照1：1-5：1比例混合后即得玛卡提取物。经进一步冷冻干燥、喷雾干燥可制备粉状玛卡提取物。(4) Maca ethanol extract and water extract are mixed according to the ratio of 1:1-5:1 to obtain Maca extract. After further freeze-drying and spray-drying, the powdered maca extract can be prepared.
更优选地，醇提工艺和水提工艺的次序可以互换，或者在任一工序前、后加入其他处理工序。More preferably, the sequence of the alcohol extraction process and the water extraction process can be interchanged, or other treatment processes can be added before or after any process.
进一步优选地，所述提取方法包括溶剂浸提、超声辅助萃取、微波辅助萃取、蒸馏萃取等中的一种或多种的组合。Further preferably, the extraction method includes a combination of one or more of solvent extraction, ultrasonic-assisted extraction, microwave-assisted extraction, and distillation extraction.
优选地，所述玛卡组合物中的其他提取物组分是经过干燥、粉碎、提取、浓缩得到的膏状或粉状提取物。Preferably, other extract components in the Maca composition are paste or powder extracts obtained through drying, crushing, extraction, and concentration.
所述烟草粉末由烟草材料经清洗、干燥后，进行机械粉碎、筛分得到20-100目的粗粉；利用低温气流超微粉碎机将烟草粗粉进行二次粉碎，筛分得到烟草粉末。The tobacco powder is cleaned and dried from the tobacco material, then mechanically pulverized and sieved to obtain a coarse powder of 20-100 mesh; the tobacco coarse powder is pulverized a second time by a low-temperature airflow ultrafine pulverizer, and then sieved to obtain tobacco powder.
优选地，所述烟草粉末的目粒度大于200目；Preferably, the mesh particle size of the tobacco powder is greater than 200 mesh;
更有选的，所述烟草粉末的目粒度大于500目；More preferably, the mesh particle size of the tobacco powder is greater than 500 mesh;
进一步优选地，所述烟草粉末的目粒度大于2000目。Further preferably, the mesh particle size of the tobacco powder is greater than 2000 mesh.
所述烟草提取物为液态烟草提取物或者烟草提取物复合物细粉。The tobacco extract is liquid tobacco extract or fine powder of tobacco extract compound.
所述液态烟草提取物是指烟草经过干燥、粉碎、筛分后，经过提取得到的烟草提取物，所述烟草提取物复合物细粉为烟草提取物经过分子蒸馏、冷冻干燥、喷雾干燥等手段，在赋形剂的作用下制成的烟草提取物复合物细粉。所述提取方法选自超临界萃取、溶剂浸提、超声辅助萃取、微波辅助萃取、蒸馏萃取等中的一种或多种。The liquid tobacco extract refers to the tobacco extract obtained by extracting tobacco after drying, pulverizing and sieving, and the fine powder of the tobacco extract compound is obtained by means of molecular distillation, freeze-drying, spray-drying and other means of tobacco extract. , the tobacco extract compound fine powder prepared under the action of excipients. The extraction method is selected from one or more of supercritical extraction, solvent extraction, ultrasonic-assisted extraction, microwave-assisted extraction, and distillation extraction.
所述烟草选自烤烟、晒烟、晾烟、白肋烟、香料烟、黄花烟中的一种或多种。The tobacco is selected from one or more of flue-cured tobacco, sun-cured tobacco, air-cured tobacco, burley tobacco, oriental tobacco and yellow flower tobacco.
更优选地，所述晒烟选自晒红烟和晒黄烟及其他地方性晒烟中的一种或多种，所述晾烟选自马里兰烟、雪茄烟及其他地方性晾烟中的一种或多种。More preferably, the sun-cured tobacco is selected from one or more of sun-cured red tobacco, yellow sun-cured tobacco and other local sun-cured tobaccos, and the sun-cured tobacco is selected from one of Maryland tobacco, cigar tobacco and other local sun-cured tobaccos. one or more species.
进一步优选地，所述烟草为产自贵州地区的晾晒烟，或者该晾晒烟与其他烟草的组合。Further preferably, the tobacco is air-cured tobacco produced in Guizhou region, or a combination of the air-cured tobacco and other tobaccos.
优选地，所述烟草是常规烟叶和有机生态烟叶中的一种或多种。Preferably, the tobacco is one or more of conventional tobacco leaves and organic ecological tobacco leaves.
优选地，所述烟草经自然发酵、陈化(在本发明的一个实施方式中，陈化时间为一年)、抽梗、清洗、脱水后进行增香处理。Preferably, the tobacco is naturally fermented, aged (in one embodiment of the present invention, the aging time is one year), stemmed, washed and dehydrated, followed by aroma-enhancing treatment.
所述增香处理是指用香料液浸泡或浸润烟草材料，或将香料液喷洒到烟草粉末或烟草提取物上。香料液可通过香料材料煎水或者香味剂配制而成。The flavoring treatment refers to soaking or infiltrating the tobacco material with flavor liquid, or spraying the flavor liquid onto tobacco powder or tobacco extract. The spice liquid can be prepared by decocting spice materials or flavoring agents.
进一步地，所述糖基选自果糖、葡萄糖、蔗糖、饴糖、氢化淀粉水解物、玉米糖浆、枫树糖浆、蛋白糖、甘草粉、甘草酸盐、甜菊糖苷、罗汉果甜苷、非洲竹竽甜素、蜂蜜、甘露糖、D-甘露糖醇、乳糖、乳糖醇、木糖醇、安赛蜜、纽甜、阿斯巴甜、麦芽糖醇、山梨糖醇、糖精钠、甜蜜素、环己基氨基磺酸钙、三氯蔗糖、阿力甜、异麦芽酮糖、赤藓糖醇、异麦芽低聚糖、异麦芽酮糖醇、低聚半乳糖、乳酮糖、低聚果糖、棉子糖、大豆低聚糖、低聚乳果糖、低聚木糖、菊粉低聚糖、蔗糖素、甘草甜素、新橙皮苷二氢查尔酮、仙茅甜蛋白、神秘果甜蛋白、薯芋防己甜素、双甜、L-阿拉伯糖中的一种或多种；Further, the sugar group is selected from fructose, glucose, sucrose, maltose, hydrogenated starch hydrolyzate, corn syrup, maple syrup, protein sugar, licorice powder, glycyrrhizinate, steviol glycoside, mogroside, African bamboo Vegetarian, honey, mannose, D-mannitol, lactose, lactitol, xylitol, acesulfame potassium, neotame, aspartame, maltitol, sorbitol, sodium saccharin, cyclamate, cyclohexylamino Calcium sulfonate, sucralose, alitame, isomaltulose, erythritol, isomalt-oligosaccharide, isomalt, galacto-oligosaccharide, lactulose, fructo-oligosaccharide, raffinose , soybean oligosaccharides, lactulose oligosaccharides, xylooligosaccharides, inulin oligosaccharides, sucralose, glycyrrhizin, neohesperidin dihydrochalcone, curculinin, mysterious fruit sweetin, potato One or more of taro tetradtame, double sweet, L-arabinose;
所述香味剂选自水果提取物、芦荟提取物、金银花提取物、罗汉果酊、山楂酊、枣子酊、佛手油、葫芦巴酊、酒花酊、可可酊、乌梅酊、红茶酊、绿茶酊、柠檬油、咖啡油、布枯叶油、丁香叶油、罗勒油、甜橙油、天然康酿克油、白兰花油、圆柚油、杭白菊油、咖啡粉、梅子粉、红枣粉、可可粉、绿茶粉、朗姆酒中的一种或多种；The fragrance agent is selected from fruit extract, aloe vera extract, honeysuckle extract, mangosteen tincture, hawthorn tincture, jujube tincture, bergamot oil, fenugreek tincture, hop tincture, cocoa tincture, ebony tincture, black tea tincture, green tea tincture, lemon oil, coffee oil, buku leaf oil, clove leaf oil, basil oil, sweet orange oil, natural konjac oil, white orchid oil, pomelo oil, chrysanthemum oil, coffee powder, plum powder, red date powder, cocoa powder One or more of , green tea powder, and rum;
所述填充剂选自滑石粉、磷酸氢钙、碳酸钙、碳酸镁、磷酸钙、玉米淀粉、环糊精、麦芽糊精、D-甘露糖醇、乳糖、乳糖醇、木糖醇、麦芽糖醇、山梨糖醇中的一种或多种；The filler is selected from talcum powder, calcium hydrogen phosphate, calcium carbonate, magnesium carbonate, calcium phosphate, corn starch, cyclodextrin, maltodextrin, D-mannitol, lactose, lactitol, xylitol, maltitol , one or more of sorbitol;
所述粘合剂选自淀粉、磷酸化二淀粉磷酸酯、羧甲基淀粉钠、淀粉磷酸酯钠、麦芽糊精、环糊精、微晶纤维素、羧甲基纤维素钠、羟丙基纤维素、甲基纤维素、乙基纤维素、羟丙甲基纤维素、明胶、阿拉伯胶、酪蛋白、甲壳素、壳聚糖及其衍生物、壳寡糖及其衍生物、海藻酸钠、海藻酸铵、海藻酸丙二醇酯、刺云实胶、甘露糖醇、山梨糖醇、乳糖醇、瓜尔胶、果胶、海萝胶、葫芦巴胶、槐豆胶、黄蜀葵胶、黄原胶、桃胶、紫胶、决明胶、黄蓍胶、卡拉胶、可得然胶、可溶性大豆多糖、罗望子多糖胶、普鲁兰多糖、亚麻籽胶中的一种或多种；The binder is selected from starch, phosphorylated distarch phosphate, sodium carboxymethyl starch, sodium starch phosphate, maltodextrin, cyclodextrin, microcrystalline cellulose, sodium carboxymethyl cellulose, hydroxypropyl Cellulose, methylcellulose, ethylcellulose, hydroxypropylmethylcellulose, gelatin, gum arabic, casein, chitin, chitosan and its derivatives, chitosan oligosaccharide and its derivatives, sodium alginate , Ammonium Alginate, Propylene Glycol Alginate, Tara Gum, Mannitol, Sorbitol, Lactitol, Guar Gum, Pectin, Seaweed Gum, Fenugreek Gum, Locust Bean Gum, Melaholth Gum, Xanthan Gum One or more of gum, peach gum, shellac, cassia gum, tragacanth gum, carrageenan, curdlan gum, soluble soybean polysaccharide, tamarind polysaccharide gum, pullulan polysaccharide, linseed gum;
所述乳化剂选自单、双、三脂肪酸甘油酯、卵磷脂、大豆磷脂、脱脂可可粉、乙酰化单双脂肪酸甘油酯、聚甘油脂肪酸酯、聚乙二醇、聚乙烯脱水山梨醇酯、泊洛沙姆、蔗糖脂肪酸酯中的一种或多种；The emulsifier is selected from mono-, di-, and tri-fatty acid glycerides, lecithin, soybean lecithin, defatted cocoa powder, acetylated mono- and di-fatty acid glycerides, polyglycerin fatty acid esters, polyethylene glycol, polyethylene sorbitan ester One or more of poloxamer, sucrose fatty acid ester;
所述崩解剂选自淀粉、预胶化淀粉、微晶纤维素、交联聚乙烯基吡咯烷酮、羧甲基淀粉钠、低取代羟丙基纤维素、交联羧甲基纤维素钠、结冷胶、黄原胶中的一种或多种；The disintegrant is selected from starch, pregelatinized starch, microcrystalline cellulose, cross-linked polyvinylpyrrolidone, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, cross-linked sodium carboxymethyl cellulose, starch One or more of cold gum and xanthan gum;
所述清凉剂选自薄荷醇、椒样薄荷油、亚洲薄荷油、亚洲薄荷素油、胡薄荷油、天然薄荷脑、N-对苯乙腈基薄荷烷基甲酰胺、N-(2-(吡啶-2-基)乙基)薄荷烷基甲酰胺、薄荷内酯中的一种或多种；Described cooling agent is selected from menthol, peppermint oil, peppermint oil, peppermint oil, peppermint oil, natural menthol, N-p-phenylacetonitrile menthyl formamide, N-(2-(pyridine- 2-yl) ethyl) one or more of menthyl formamide, mentholactone;
所述抗氧化剂选自茶多酚、丁基羟基茴香醚、苯甲酸钠、二丁基羟基甲苯、没食子酸丙酯、山梨酸及其钾盐、dl-α-生育酚、d-α-生育酚、维生素C、抗坏血酸钙、抗坏血酸棕榈酸酯、D-异抗坏血酸及其钠盐、鼠尾草酸、甘草抗氧化物、竹叶抗氧化物、银杏提取物、茶叶提取物和葡萄籽提取物中的一种或多种；The antioxidant is selected from tea polyphenols, butyl hydroxyanisole, sodium benzoate, dibutyl hydroxytoluene, propyl gallate, sorbic acid and its potassium salt, dl-alpha-tocopherol, d-alpha-tocopherol , vitamin C, calcium ascorbate, ascorbyl palmitate, D-erythorbic acid and its sodium salt, carnosic acid, licorice antioxidant, bamboo leaf antioxidant, ginkgo biloba extract, tea extract and grape seed extract one or more;
所述润滑剂选自硬脂酸、硬脂酸钙、硬脂酸镁、硬脂酸钠、硬脂酸钾、滑石粉、巴西棕榈蜡、蜂蜡、聚乙烯蜡、聚乙二醇、石蜡、石油石蜡、微晶石蜡、小烛树蜡、蔗糖脂肪酸酯、氢化植物油中的一种或多种。Described lubricant is selected from stearic acid, calcium stearate, magnesium stearate, sodium stearate, potassium stearate, talcum powder, carnauba wax, beeswax, polyethylene wax, polyethylene glycol, paraffin, One or more of petroleum paraffin, microcrystalline paraffin, candelilla wax, sucrose fatty acid ester, hydrogenated vegetable oil.
本发明还提供了所述烟草含化片的制备方法，所述方法为制粒压片法，具体为：The present invention also provides a preparation method of the tobacco-containing chemical tablet, the method is a granulation and tabletting method, specifically:
(1)将烟草粉末和/或烟草提取物、玛卡组合物、糖基、香味剂、填充剂、粘合剂、乳化剂混合均匀，调节pH为6-8，用制粒机进行湿法制粒，得到14-50目颗粒；(1) Mix tobacco powder and/or tobacco extract, Maca composition, sugar base, flavoring agent, filler, binder, emulsifier uniformly, adjust pH to 6-8, and carry out wet process with granulator granules to obtain 14-50 mesh granules;
(2)将步骤(1)制粒得到的组合物颗粒在烘箱中干燥0.5-2小时，过14-50目筛网进行整粒；(2) drying the composition granules obtained by granulating in step (1) in an oven for 0.5-2 hours, passing through a 14-50 mesh screen for sizing;
(3)将整粒得到的组合物颗粒与抗氧化剂、清凉剂、崩解剂、润滑剂混合均匀，在压片机中压制即得；(3) mix uniformly the composition granules obtained by granulation with antioxidant, cooling agent, disintegrating agent and lubricant, and compress in a tablet machine;
或，所述方法为直接压片法，包括如下步骤：Or, the method is a direct compression method, comprising the steps of:
(1)将烟草粉末和/或烟草提取物、玛卡组合物、糖基、香味剂、填充剂、粘合剂、乳化剂、抗氧化剂、清凉剂、崩解剂、润滑剂混合均匀，调节pH为6-8，在压片机中压制成片粒，(1) Mix tobacco powder and/or tobacco extract, Maca composition, sugar base, flavoring agent, filler, binder, emulsifier, antioxidant, cooling agent, disintegrant, lubricant, adjust pH 6-8, compressed into tablets in a tablet machine,
(2)将步骤(1)得到的片粒在烘箱中干燥后即得；(2) drying the tablets obtained in step (1) in an oven;
其中，pH调节剂选自碳酸钠、碳酸氢钠、碳酸钾、碳酸氢钾、柠檬酸钠、柠檬酸钾、葡萄糖酸钠中的一种或多种。Wherein, the pH regulator is selected from one or more of sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, sodium citrate, potassium citrate, and sodium gluconate.
本发明还提供了所述的烟草含化片在作为烟草补充替代品方面的应用。The present invention also provides the application of the tobacco-containing sheet as a supplementary tobacco substitute.
本发明的有益效果在于：The beneficial effects of the present invention are:
本发明所述的烟草含化片，选用贵州地区的特有晾晒烟作为主要烟草原料，并经过增香和/降低烟碱处理，香气浓郁，劲头适中，平衡了产品的生理满足感和口感舒适度，对于提升含化型无烟气烟草制品的口感质量和市场适应性有重要意义；玛卡经过超微粉碎或复合提取技术制备玛卡提取物，并与其他植物组分进行优化复配，降低了玛卡的辛辣口感，并且提高了有效成分的利用效率，与烟草材料协同作用，可以抗疲劳，提高人体精神状态，减少吸烟者对烟碱的依赖感；基于本发明的产品，口感舒适，香味持久，不产生烟气，可以在公共场所使用，方便携带，是一种口感舒适、安全环保的新型含化型无烟气烟草制品。The tobacco-containing slices of the present invention use the unique air-cured tobacco in Guizhou as the main tobacco raw material, and have been processed to increase flavor and/or reduce nicotine. The aroma is rich and the strength is moderate, which balances the physiological satisfaction and mouthfeel comfort of the product. , which is of great significance for improving the taste quality and market adaptability of chemical-containing smokeless tobacco products; The spicy taste of maca is improved, and the utilization efficiency of active ingredients is improved, and the synergistic effect with tobacco materials can resist fatigue, improve the mental state of the human body, and reduce the smoker's dependence on nicotine; the product based on the invention has a comfortable taste, It has a long-lasting fragrance and does not produce smoke. It can be used in public places and is easy to carry. It is a new chemical-containing smokeless tobacco product with a comfortable taste, safety and environmental protection.
具体实施方式detailed description
以下实施例用于说明本发明，但不用来限制本发明的范围。The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention.
实施例1Example 1
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
其中，玛卡组合物配方中各组分的重量比如下：玛卡提取物40份、破壁蜂花粉30份、辣木提取物20份、瓜拉纳提取物10份。Wherein, the weight ratio of each component in the Maca composition formula is as follows: 40 parts of Maca extract, 30 parts of broken bee pollen, 20 parts of Moringa oleifera extract, and 10 parts of Guarana extract.
制备步骤如下：The preparation steps are as follows:
(1)、原料处理(1), raw material processing
将贵州地区晾晒烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理。按照甘草：水＝1：10的比例将甘草在90-100℃下时间煎制1小时，降温、过滤后，在滤液中加入重量比为5％的蜂蜜配制成香料液，用香料液浸润晾晒烟24-72小时，进行增香处理。将晾晒烟取出后，在120-140℃进行烘干至水分小于3wt％。将干燥后的烟草材料粉碎，过80目筛得到烟草粗粉。然后进行二次超微粉碎，过筛得到粒度500-4000目的晾晒烟粉末。The air-cured tobacco in Guizhou is naturally fermented and aged for one year, followed by stem extraction, cleaning and dehydration. According to the ratio of licorice: water = 1:10, decoct licorice at 90-100°C for 1 hour, cool down and filter, add honey with a weight ratio of 5% to the filtrate to prepare a spice liquid, and soak it in the spice liquid to dry Smoke for 24-72 hours, and carry out aroma-enhancing treatment. After the air-cured tobacco is taken out, it is dried at 120-140°C until the moisture is less than 3wt%. The dried tobacco material is pulverized and passed through an 80-mesh sieve to obtain coarse tobacco powder. Then perform secondary ultrafine pulverization, and sieve to obtain air-dried tobacco powder with a particle size of 500-4000 mesh.
将玛卡提取物与破壁蜂花粉、辣木提取物、瓜拉纳提取物等按比例复配后得到玛卡组合物。The maca composition is obtained by compounding maca extract with broken bee pollen, moringa extract, guarana extract and the like in proportion.
(2)、制粒(2), granulation
将黄原胶、玛卡组合物、罗汉果酊、蓝莓提取物、薄荷醇、泊洛沙姆等分散在去离子水中，制备粘结剂溶液，备用；将原辅料过100目筛后，按配方称取晾晒烟粉末、木糖醇、山梨糖醇、麦芽糊精、微晶纤维素、碳酸钠，充分混合，然后利用粘结剂溶液在制粒机上用20目筛进行湿法制粒。将湿料放入厢式干燥器中，在50-80℃下干燥至物料含水量为3-6wt％。然后将干料用18目筛整粒后储存备用。Disperse xanthan gum, maca composition, Luo Han Guo tincture, blueberry extract, menthol, poloxamer, etc. in deionized water to prepare a binder solution for later use; pass the raw and auxiliary materials through a 100-mesh sieve, and Weigh air-cured tobacco powder, xylitol, sorbitol, maltodextrin, microcrystalline cellulose, and sodium carbonate, mix thoroughly, and then use the binder solution to perform wet granulation on a granulator with a 20-mesh sieve. Put the wet material into a box dryer, and dry it at 50-80°C until the water content of the material is 3-6wt%. Then the dry material is sized with a 18-mesh sieve and stored for later use.
(3)、压片(3), tablet
在干料中加入山梨酸钾和硬脂酸镁，混合均匀后喂入压片机，按照每片1.0g的规格进行压片，得到烟草含化片素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。Potassium sorbate and magnesium stearate are added to the dry material, mixed evenly, fed into a tablet press, and compressed according to the specification of 1.0 g per tablet, to obtain plain tobacco-containing tablets. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
(4)、包衣抛光(4), coating and polishing
还可利用虫胶乙醇溶液、糖浆、阿拉伯胶、滑石粉等原料为素片制作糖包衣，利用食用级巴西棕榈蜡进行表面抛光处理后，包装即成烟草含化片。Shellac ethanol solution, syrup, gum arabic, talcum powder and other raw materials can also be used to make sugar coatings for plain tablets, and food-grade carnauba wax is used for surface polishing, and then packaged to form tobacco-containing tablets.
实施例2Example 2
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
其中，玛卡组合物的配方中各组分的重量比如下：玛卡提取物30份、枸杞提取物30份、绞股蓝提取物20份、卡姆果提取物20份。Wherein, the weight ratio of each component in the formula of the Maca composition is as follows: 30 parts of Maca extract, 30 parts of Lycium barbarum extract, 20 parts of Jiaogulan extract, and 20 parts of camu camu extract.
制备步骤如下：The preparation steps are as follows:
(1)、原料处理(1), raw material processing
将贵州地区晾晒烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理。按照金银花：水＝1：15的比例在80-90℃下煎制1-3小时，过滤后，在滤液中加入重量比为10％的玉米糖浆配制成香料液，冷却备用。将香料液喷洒到晾晒烟上，在30-60℃下浸润8-24小时，进行增香处理。从香料液中取出烟草材料，转笼脱除水分，在50-60℃下进行烘干至水分小于3wt％。将干燥后的烟草材料进行粉碎，过80目筛得到烟草粗粉。然后进行二次超微粉碎，过筛得到目粒度300-2000目的混合烟草粉末。The air-cured tobacco in Guizhou is naturally fermented and aged for one year, followed by stem extraction, cleaning and dehydration. Fry at 80-90°C for 1-3 hours according to the ratio of honeysuckle: water = 1:15. After filtering, add corn syrup with a weight ratio of 10% to the filtrate to prepare a spice liquid, and cool it for later use. The spice liquid is sprayed on the air-cured tobacco, soaked at 30-60°C for 8-24 hours, and the aroma-enhancing treatment is carried out. The tobacco material is taken out from the spice liquid, the moisture is removed by rotating the cage, and dried at 50-60°C until the moisture is less than 3wt%. The dried tobacco material is pulverized and passed through an 80-mesh sieve to obtain coarse tobacco powder. Then perform secondary ultrafine pulverization, and sieve to obtain mixed tobacco powder with a mesh particle size of 300-2000 mesh.
将玛卡提取物与枸杞提取物、绞股蓝提取物、卡姆果提取物等按比例复配后得到玛卡组合物。The Maca composition is obtained by compounding the Maca extract with wolfberry extract, Jiaogulan extract, camu camu extract and the like in proportion.
(2)、压片(2), tablet
将海藻酸钠等分散在去离子水中，制成粘结剂溶液，备用；将原辅料过100目筛后，按配方称取混合烟草粉末、玛卡组合物、异麦芽酮糖醇、异麦芽低聚糖、绿茶粉、绿茶酊、玉米淀粉、薄荷醇、羧甲基淀粉钠、D-异抗坏血酸钠和巴西棕榈蜡，搅拌均匀后喂入压片机，按照每片1.0g的规格进行压片，得到烟草含化片素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。将片粒在烘箱中干燥后即得烟草含化片素片。Disperse sodium alginate etc. in deionized water to make a binder solution for later use; pass the raw and auxiliary materials through a 100-mesh sieve, weigh mixed tobacco powder, maca composition, isomalt, and isomalt according to the formula Oligosaccharides, green tea powder, green tea tincture, cornstarch, menthol, sodium carboxymethyl starch, D-sodium erythorbate, and carnauba wax are fed into the tablet machine after being stirred evenly, and compressed according to the specification of 1.0g per tablet slices to obtain tobacco-containing sliced plain slices. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait. Tobacco-containing flakes are obtained after the tablets are dried in an oven.
(3)、包衣抛光(3), coating polishing
利用明胶、糖浆、滑石粉、绿茶酊等原料为素片制作糖包衣，利用川蜡进行表面抛光处理后，包装即成具有绿茶风味的烟草含化片。Gelatin, syrup, talcum powder, green tea tincture and other raw materials are used as raw materials to make sugar-coated plain tablets, and after surface polishing is carried out with Sichuan wax, the tobacco-containing tablets with green tea flavor are packaged.
实施例3Example 3
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
其中，玛卡组合物的配方中各组分的重量比如下：玛卡提取物60份、菊粉20份、阿萨依果提取物10份、释迦提取物10份。Wherein, the weight ratio of each component in the formula of the Maca composition is as follows: 60 parts of Maca extract, 20 parts of inulin, 10 parts of Acai fruit extract, and 10 parts of Sakyamuni extract.
制备步骤如下：The preparation steps are as follows:
(1)、原料处理(1), raw material processing
将贵州地区晾晒烟自然发酵、陈化一年，进行抽梗、清洗、脱水处理，然后在80-90℃水中热处理1-2小时，取出后转笼脱除水分，在40-60℃下进行烘干。按照晾晒烟：香料烟＝4：1的重量比混合、粉碎，过80目筛得到烟草粗粉。然后进行二次超微粉碎，过筛得到目粒度400-3000目的混合烟草粉末。The air-dried tobacco in Guizhou is fermented naturally and aged for one year, followed by stem extraction, cleaning and dehydration, and then heat treatment in water at 80-90°C for 1-2 hours, after taking it out, turn it into a cage to remove water, and carry out at 40-60°C drying. According to the weight ratio of air-dried tobacco: oriental tobacco = 4:1, mix and pulverize, and pass through an 80-mesh sieve to obtain coarse tobacco powder. Then perform secondary superfine pulverization, and sieve to obtain mixed tobacco powder with a mesh particle size of 400-3000 mesh.
将重量比为1％佛手油、5％β-环糊精分散在乙醇中，强力搅拌、混合均匀制成香料液，均匀喷洒在烟草细粉中，并搅拌均匀，以不结块为准，平衡水分后即得增香混合烟草粉末。Disperse 1% bergamot oil and 5% β-cyclodextrin in ethanol by weight, stir vigorously and mix evenly to make flavor liquid, spray evenly on tobacco fine powder, and stir evenly, subject to no agglomeration, After balancing the moisture, the flavored mixed tobacco powder is obtained.
将玛卡提取物与菊粉、阿萨依果提取物、释迦提取物等按比例复配后得到玛卡组合物。The Maca composition is obtained by compounding Maca extract with inulin, Acai fruit extract, Sakyamuni extract and the like in proportion.
(2)、制粒(2), granulation
将阿拉伯胶、结冷胶、乌梅酊、大豆磷脂等分散在去离子水中，制成粘结剂溶液，备用；将原辅料过100目筛后，按配方称取混合烟草粉末、玛卡组合物、碳酸氢钠、木糖醇、甜菊糖苷、D-甘露糖醇等，充分混合，利用粘结剂溶液在制粒机上用18目筛进行湿法制粒。将湿料放入厢式干燥器中，在50-60℃下干燥至物料含水量小于3wt％。然后将干料用16目筛整粒后储存备用。Disperse gum arabic, gellan gum, ebony tincture, soybean lecithin, etc. in deionized water to make a binder solution for later use; after passing the raw and auxiliary materials through a 100-mesh sieve, weigh the mixed tobacco powder and Maca composition according to the formula , sodium bicarbonate, xylitol, steviol glycoside, D-mannitol, etc., fully mixed, using the binder solution to carry out wet granulation on the granulator with an 18-mesh sieve. Put the wet material into a box dryer and dry it at 50-60°C until the water content of the material is less than 3wt%. Then the dry material is sized with a 16-mesh sieve and stored for later use.
(3)、压片(3), tablet
在干料中加入维生素C、硬脂酸镁等，搅拌均匀后喂入压片机，按照每片0.5g的规格进行压片，得到烟草含化片素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。Add vitamin C, magnesium stearate, etc. to the dry material, stir evenly, and then feed it into a tablet machine, and perform tablet compression according to the specification of 0.5 g per tablet to obtain plain tobacco-containing tablets. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
(4)、包衣抛光(4), coating and polishing
利用麦芽糖醇、明胶、乌梅酊等原料为素片制作糖包衣，利用小烛树蜡和巴西棕榈蜡进行表面抛光处理后，包装即成具有梅子风味的烟草含化片。Using maltitol, gelatin, ebony tincture and other raw materials as raw materials to make sugar coating for plain tablets, using candelilla wax and carnauba wax for surface polishing, and then packaging to form tobacco-containing tablets with plum flavor.
实施例4Example 4
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
其中，玛卡组合物的配方中各组分的重量比如下：玛卡提取物50份、可乐果提取物20份、苜蓿提取物10份、诺丽果提取物10份、达米阿那提取物10份。Wherein, the weight ratio of each component in the formula of the Maca composition is as follows: 50 parts of Maca extract, 20 parts of cola fruit extract, 10 parts of alfalfa extract, 10 parts of Noni fruit extract, 10 parts of Damiana fruit extract, Extract 10 parts.
制备步骤如下：The preparation steps are as follows:
(1)、原料处理(1), raw material processing
将贵州地区晾晒烟自然发酵、陈化一年，烤烟烤制、陈化一年，进行抽梗、清洗、脱水处理，在40-60℃下进行烘干。将香料烟在40-60℃下进行烘干。在按照烤烟：晾晒烟：香料烟＝5：3：2的重量比混合、粉碎，利用溶剂浸提法或者超临界萃取法制得混合烟草提取物。The air-dried tobacco in Guizhou is naturally fermented and aged for one year, and the flue-cured tobacco is cured and aged for one year, followed by stem extraction, cleaning, dehydration, and drying at 40-60°C. The oriental tobacco is dried at 40-60°C. The mixed tobacco extract is obtained by mixing and pulverizing flue-cured tobacco: air-dried tobacco: oriental tobacco in a weight ratio of 5:3:2, and using a solvent extraction method or a supercritical extraction method.
将烟草提取物：阿拉伯胶：β-环糊精＝1：2：3按重量比分散在去离子水中，强力搅拌成均匀乳状液，喷雾干燥形成烟草提取物复合物。Tobacco extract: gum arabic: β-cyclodextrin = 1:2:3 is dispersed in deionized water in a weight ratio, vigorously stirred to form a uniform emulsion, and spray-dried to form a tobacco extract compound.
将玛卡提取物与可乐果提取物、苜蓿提取物、诺丽果提取物、达米阿那提取物等按比例复配后得到玛卡组合物。The maca composition is obtained by compounding maca extract with kola nut extract, alfalfa extract, noni fruit extract, damiana extract and the like in proportion.
(2)、制粒(2), granulation
将普鲁兰多糖、天然康酿克油、酒花酊、卵磷脂和一半重量的交联聚乙烯基吡咯烷酮等分散在去离子水中，制成粘结剂溶液，备用；将原辅料过100目筛后，按配方称取有烟草提取物复合物、玛卡组合物、碳酸钠、异麦芽酮糖、枫树糖浆、环糊精等，充分混合，利用粘结剂溶液在制粒机上用20目筛进行湿法制粒。将湿料放入厢式干燥器中，在50-60℃下干燥至物料含水量小于3wt％。然后将干料用20目筛整粒后储存备用。Disperse pullulan polysaccharide, natural konjac oil, hop tincture, lecithin and half the weight of cross-linked polyvinylpyrrolidone in deionized water to make a binder solution for later use; pass the raw and auxiliary materials through a 100-mesh sieve Finally, weigh tobacco extract compound, Maca composition, sodium carbonate, isomaltulose, maple syrup, cyclodextrin, etc. according to the formula, mix them thoroughly, and use the binder solution on the granulator with 20 mesh Sieve for wet granulation. Put the wet material into a box dryer and dry it at 50-60°C until the water content of the material is less than 3wt%. Then the dry material is sized with a 20-mesh sieve and stored for later use.
(3)、压片(3), tablet
在干料中加入山梨酸钾、薄荷油、另一半重量的交联聚乙烯基吡咯烷酮、微晶石蜡等，搅拌均匀后喂入压片机，按照每片0.5g的规格进行压片，得到烟草含化片素片。压片的形状可以是圆形、椭圆形、菱形、锥形、叶形、花朵形、水果形、水滴形等，产品表面可以进行阴文或者阳文压花，比如企业名称、企业标识、字母缩写等。Add potassium sorbate, peppermint oil, the other half of the weight of cross-linked polyvinylpyrrolidone, microcrystalline paraffin, etc. to the dry material, stir it evenly, feed it into the tablet press, and press it according to the specification of 0.5g per tablet to obtain tobacco Contains chemical tablets. The shape of the pressed tablet can be round, oval, rhombus, cone, leaf, flower, fruit, water drop, etc. The surface of the product can be embossed in negative or positive, such as company name, company logo, initials Wait.
(4)、包衣抛光(4), coating and polishing
利用异麦芽酮糖、玉米糖浆、薄荷醇、普鲁兰多糖等原料为素片制作糖包衣，利用聚乙二醇、蜂蜡进行表面抛光处理后，包装即成具有酒香风味的烟草含化片。Isomaltulose, corn syrup, menthol, pullulan and other raw materials are used as raw materials to make sugar-coated plain tablets, and after surface polishing with polyethylene glycol and beeswax, the packaged tobacco-containing chemical with wine flavor piece.
对比例1Comparative example 1
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
其中，玛卡组合物配方中各组分的重量比如下：玛卡提取物40份、破壁蜂花粉30份、辣木提取物20份、瓜拉纳提取物10份。Wherein, the weight ratio of each component in the Maca composition formula is as follows: 40 parts of Maca extract, 30 parts of broken bee pollen, 20 parts of Moringa oleifera extract, and 10 parts of Guarana extract.
制备步骤同实施例1。The preparation steps are the same as in Example 1.
对比例2Comparative example 2
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
制备步骤同实施例4。The preparation steps are the same as in Example 4.
对比例3Comparative example 3
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
制备步骤同实施例2。The preparation steps are the same as in Example 2.
对比例4Comparative example 4
各组分所占的重量比如下：The weight ratio that each component occupies is as follows:
其中，玛卡组合物的配方中各组分的重量比如下：玛卡提取物60份、菊粉20份、阿萨依果提取物10份、释迦提取物10份。Wherein, the weight ratio of each component in the formula of the Maca composition is as follows: 60 parts of Maca extract, 20 parts of inulin, 10 parts of Acai fruit extract, and 10 parts of Sakyamuni extract.
制备步骤同实施例3。The preparation steps are the same as in Example 3.
将实施例1-4以及对比例1-4所制备的烟草含化片进行感官评价测试，感官质量评价方法，具体如下：Carry out sensory evaluation test with the tobacco-containing sheet prepared by Examples 1-4 and Comparative Examples 1-4, and the sensory quality evaluation method is as follows:
(1)感官质量评价指标(1) Sensory quality evaluation index
该感官质量评价方法共设置9项评价指标，包括入口口感、生理强度、特征香、烟草香、刺激感、舒适感、释放均匀性、释放持久性和口腔余味。所述入口口感是指无烟气烟草制品放入口腔后，使用者的嗅觉、味觉和触觉等初始综合感受。所述生理强度是指在使用过程中，使用者所感受到的生理满足感，即劲头。所述特征香是指在使用过程中，使用者所感受到的特征香气的量和质。所述烟草香是指在使用过程中，使用者所感受到的烟草本香的量和质。所述刺激感是指在使用过程中，使用者口腔、鼻腔、咽喉、食道等部位所感受到辛辣、干燥等不舒适感受。所述舒适感是指在使用过程中，使用者所感受到香味协调性、柔润感、无残渣异物感等愉悦性感受。所述释放均匀性是指在使用过程中，使用者所感受到香味、生理强度等随时间的释放稳定性。所述释放持久性是指在使用过程中，使用者所感受到香味、生理强度等持续时间长短。所述口腔余味是指在使用过程后，使用者口腔所残余的嗅觉、味觉和触觉的综合感受。The sensory quality evaluation method sets up 9 evaluation indicators, including mouthfeel, physiological strength, characteristic aroma, tobacco aroma, stimulation, comfort, release uniformity, release persistence and oral aftertaste. The mouthfeel refers to the user's initial comprehensive sense of smell, taste and touch after the smokeless tobacco product is put into the oral cavity. The physiological strength refers to the physiological satisfaction felt by the user during use, that is, energy. The characteristic fragrance refers to the quantity and quality of the characteristic fragrance felt by the user during use. The tobacco aroma refers to the quantity and quality of the tobacco aroma felt by the user during use. The irritating sensation refers to the uncomfortable feelings such as pungentness and dryness felt by the user's mouth, nasal cavity, throat, esophagus and other parts during use. The comfort refers to pleasant sensations such as fragrance coordination, softness, and no residue foreign body sensation felt by the user during use. The release uniformity refers to the release stability over time of the fragrance, physiological strength, etc. felt by the user during use. The release duration refers to the length of time that the user feels the fragrance, physiological intensity, etc. during use. The oral aftertaste refers to the comprehensive feeling of smell, taste and touch remaining in the user's oral cavity after use.
(2)感官质量评价计分规则(2) Sensory quality evaluation scoring rules
所述感官质量评价计分规则采用百分制评分法。所述百分制评分法是指依据各项感官质量评价指标对无烟气烟草制品感官质量的影响程度，赋予各个感官质量评价指标不同的权重，即不同分值，9个感官质量评价指标分别按5分、10分或20分制进行评分，并且9个感官质量评价指标的最高评分值加和为一百分。The scoring rules for the evaluation of sensory quality adopt the 100-point scoring method. The 100-point scoring method refers to assigning different weights to each sensory quality evaluation index based on the degree of influence of each sensory quality evaluation index on the sensory quality of smokeless tobacco products, that is, different scores. 10 points, 10 points or 20 points, and the sum of the highest scores of the 9 sensory quality evaluation indicators is 100 points.
所述9项感官质量评价指标的计分规则如下：所述感官质量评价指标分为6个等级，各项所占权重、评分标度及评分区间如表1所示，最小计分单位为0.5分。The scoring rules of the 9 sensory quality evaluation indicators are as follows: the sensory quality evaluation indicators are divided into 6 grades, and the weights, scoring scales and scoring intervals of each item are shown in Table 1, and the minimum scoring unit is 0.5 point.
所述感官质量评价指标权重是指该项感官质量评价指标在感官质量评价过程中所能得到的最高评分值。所述感官质量评价指标计分区间是指该项感官质量评价指标在感官质量评价过程中某一评价标度所对应的分值区间，其中较高分包含在该段计分中，较低分不包含在该段计分中。The weight of the sensory quality evaluation index refers to the highest scoring value of the sensory quality evaluation index that can be obtained during the sensory quality evaluation process. The score interval of the sensory quality evaluation index refers to the score interval corresponding to a certain evaluation scale in the sensory quality evaluation process of the sensory quality evaluation index, wherein the higher score is included in the score of this section, and the lower score is included in the score of this section. Not included in scoring for this segment.
所述感官质量评价指标“刺激感”感受越强，得分越低；所述感官质量评价指标“入口口感”、“口腔余味”感受越好，得分越高；所述感官质量评价指标“生理强度”、“特征香”、“烟草香”、“舒适感”、“释放均匀性”、“释放持久性”感受越强，得分越高；The stronger the sensory quality evaluation index "stimulation", the lower the score; the better the sensory quality evaluation index "mouthfeel" and "mouth aftertaste", the higher the score; the sensory quality evaluation index "physiological strength ", "Characteristic Fragrance", "Tobacco Fragrance", "Comfort", "Uniformity of Release", and "Durability of Release", the stronger the feeling, the higher the score;
所述感官质量评价总分由各分项感官质量评价指标得分的算术加和得到。总分得分越高，则表示该款无烟气烟草制品的感官质量评价效果越好。The total sensory quality evaluation score is obtained by the arithmetic sum of the sensory quality evaluation index scores of each sub-item. The higher the total score, the better the sensory quality evaluation effect of the smokeless tobacco product.
表1无烟气烟草制品感官质量评价计分规则Table 1 Scoring rules for sensory quality evaluation of smokeless tobacco products
(3)感官质量评价实施方法(3) Implementation method of sensory quality evaluation
a、评价员设置a. Evaluator settings
优选地，设置包含9位评价员的评价团队。Preferably, an evaluation team comprising 9 evaluators is set up.
b、评价实施过程b. Evaluate the implementation process
将待评价的一批无烟气烟草制品样品以3位数字代码进行盲标(若样品数大于999，则可将数字代码升级为4位，依此类推)，并将样品顺序随机处理；依照处理后的样品顺序进行感官质量评价，每个样品开始评价前，分发给评价团队每人一份无烟气烟草制品感官质量评价记录表，对无烟气烟草制品进行感官评价；依据表1中9个感官质量评价指标的权重、评价标度及计分区间，评价员应对各项评价指标进行感官质量评价，并在感官评价记录表中记录评价结果，然后将评价团队的所有感官质量评价汇总到单样品感官质量评价汇总表中，并进行评价结果统计处理；依次完成所有样品的感官质量评价后，将所有样品的感官质量评价汇总到批样品感官质量评价汇总表中。Blind label a batch of smokeless tobacco product samples to be evaluated with a 3-digit code (if the number of samples is greater than 999, the digital code can be upgraded to 4 digits, and so on), and the order of the samples is randomly processed; according to The processed samples were evaluated for sensory quality sequentially. Before the evaluation of each sample, a copy of the sensory quality evaluation record sheet for smokeless tobacco products was distributed to each member of the evaluation team, and the sensory evaluation of smokeless tobacco products was performed; according to Table 1 The weights, evaluation scales and scoring intervals of the 9 sensory quality evaluation indicators, the evaluators should conduct sensory quality evaluation for each evaluation index, and record the evaluation results in the sensory evaluation record sheet, and then summarize all the sensory quality evaluations of the evaluation team Enter the single-sample sensory quality evaluation summary table, and perform statistical processing of the evaluation results; after completing the sensory quality evaluation of all samples in turn, summarize the sensory quality evaluation of all samples into the batch sample sensory quality evaluation summary table.
c、评价结果统计分析c. Statistical analysis of evaluation results
优选地，单项感官质量评价指标得分的计算方法是：在9个参加感官质量评价的评价员对该项感官质量评价指标的所有评分中去掉一个最低分及一个最高分，剩余7个评分为有效得分，有效得分的算术平均值即为该项感官质量评价指标得分，结果保留两位小数；Preferably, the calculation method for the score of a single sensory quality evaluation index is: remove the lowest score and the highest score from all the ratings of the sensory quality evaluation index by the 9 evaluators participating in the sensory quality evaluation, and the remaining 7 ratings are valid. Score, the arithmetic mean of valid scores is the score of the sensory quality evaluation index, and the result is rounded to two decimal places;
各单项感官质量评价指标得分的算术平均值加和即为无烟气烟草制品的感官质量评价总分，结果保留两位小数。总分分值越高，则表示该款无烟气烟草制品的感官评价效果越好。具体结果如表2所示：The sum of the arithmetic mean of the individual sensory quality evaluation index scores is the total sensory quality evaluation score of smokeless tobacco products, and the results are rounded to two decimal places. The higher the total score, the better the sensory evaluation effect of the smokeless tobacco product. The specific results are shown in Table 2:
表2烟草含化片的感官质量评价统计表Table 2 Statistical Table of Sensory Quality Evaluation of Tobacco Containing Tablets
由表2可见，本发明的烟草含化片以贵州晾晒烟为主要烟草原料，添加的玛卡组分经过特殊工艺处理，并与优选植物组分复配成玛卡组合物，产品具有特征香气明显、刺激性小、口感舒适、释放稳定、余味好等特点，而仅以烤烟为烟草原料或直接以玛卡粉作为添加组分无法实现同样的效果。It can be seen from Table 2 that the tobacco-containing sheet of the present invention uses Guizhou air-cured tobacco as the main tobacco raw material, and the added Maca component is processed through a special process, and is compounded with the preferred plant component to form a Maca composition, and the product has a characteristic aroma Obvious, less irritating, comfortable mouthfeel, stable release, good aftertaste, etc., but only using flue-cured tobacco as tobacco raw material or directly using Maca powder as an added component cannot achieve the same effect.
将本发明制备的添加玛卡组合物的烟草含化片和不添加玛卡组合物的烟草含化片交于有吸烟习惯的人士使用后进行评价。参与人数共100人，年龄在25-55之间。将参与使用评价的人员分成两组，每组人员的年龄及吸烟年数相当，分别使用添加和不添加玛卡组合物的烟草含化片，使用时间为3个月；然后在一周、一个月、三个月的时间点分别填写使用感受评价表，汇总结果列入表3。The tobacco-containing tablets with Maca composition added and the tobacco-containing tablets without Maca composition prepared by the present invention are given to people with smoking habits for evaluation. A total of 100 participants, aged between 25-55. The personnel participating in the use evaluation were divided into two groups, and the age and smoking years of each group of personnel were equivalent, and the tobacco buccal tablets with and without Maca composition were used respectively for 3 months; Fill in the use experience evaluation form at the time point of three months, and the summary results are listed in Table 3.
表3烟草含化片的使用感受评价表Table 3 Tobacco buccal tablets evaluation form for use experience
由表3结果可以发现，与不添加玛卡组合物的烟草含化片相比，添加玛卡组合物的烟草含化片具有更有效的减少烟碱依赖感的作用；并且随着使用时间的延长，相当一部分评价人员还感受到缓解疲劳、增强体力等作用；添加玛卡组合物的烟草含化片使用后基本无明显的口腔不适感、呼吸道不适感、消化道不适感或其他不良感受，人体耐受性良好。As can be found from the results in Table 3, compared with the tobacco-containing tablets without adding the Maca composition, the tobacco-containing tablets that add the Maca composition have a more effective effect of reducing the feeling of nicotine dependence; and with the use of time Prolonged, a considerable number of evaluators also felt the effects of relieving fatigue and enhancing physical strength; the tobacco buccal tablets added with maca composition basically had no obvious oral discomfort, respiratory discomfort, digestive tract discomfort or other adverse feelings after use. It is well tolerated by humans.
综上所述，本发明有效克服了现有技术中的种种缺点而具高度产业利用价值。To sum up, the present invention effectively overcomes various shortcomings in the prior art and has high industrial application value.
虽然，上文中已经用一般性说明及具体实施方案对本发明作了详尽的描述，但在本发明基础上，可以对之作一些修改或改进，这对本领域技术人员而言是显而易见的。因此，在不偏离本发明精神的基础上所做的这些修改或改进，均属于本发明要求保护的范围。Although the present invention has been described in detail with general descriptions and specific embodiments above, it is obvious to those skilled in the art that some modifications or improvements can be made on the basis of the present invention. Therefore, the modifications or improvements made on the basis of not departing from the spirit of the present invention all belong to the protection scope of the present invention.
| Application Number | Priority Date | Filing Date | Title |
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| CN201510683008.7ACN105595404B (en) | 2015-10-20 | 2015-10-20 | Tobacco buccal tablet and preparation method thereof |
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| CN201510683008.7ACN105595404B (en) | 2015-10-20 | 2015-10-20 | Tobacco buccal tablet and preparation method thereof |
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| CN105595404Atrue CN105595404A (en) | 2016-05-25 |
| CN105595404B CN105595404B (en) | 2021-03-26 |
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| CN201510683008.7AActiveCN105595404B (en) | 2015-10-20 | 2015-10-20 | Tobacco buccal tablet and preparation method thereof |
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