技术领域technical field
本发明涉及造纸法卷烟薄片及其制造方法，尤其涉及烤烟型高烟气浓度、高劲头卷烟薄片原料及其制备方法。The invention relates to a paper-making cigarette sheet and a manufacturing method thereof, in particular to a raw material of a flue-cured tobacco type cigarette sheet with high smoke concentration and high strength and a preparation method thereof.
背景技术Background technique
造纸法薄片在卷烟产品中的作用已得到国内外烟草界的普遍认可，具有填充值高、燃烧性能好、焦油释放量低等特性，在卷烟中添加再造烟叶不仅可降低卷烟成本、节约原料，还可协调烟气组分。然而，造纸法薄片也有其自身一些缺点，如烟气浓度低，劲头小，杂气、刺激性明显等。近年来，随着国内外对造纸法薄片研究的不断深入，增加其功能性，改善其缺陷的研究也有很大的进展，因而造纸法薄片的使用前景将更加广阔。The role of paper-making thin sheets in cigarette products has been generally recognized by the tobacco industry at home and abroad. It has the characteristics of high filling value, good combustion performance, and low tar release. Adding reconstituted tobacco leaves to cigarettes can not only reduce cigarette costs and save raw materials. The flue gas composition can also be coordinated. However, paper-making flakes also have their own disadvantages, such as low smoke concentration, low energy, miscellaneous gas, and obvious irritation. In recent years, with the continuous deepening of research on paper-making thin sheets at home and abroad, the research on increasing its functionality and improving its defects has also made great progress, so the use of paper-making thin sheets will have a broader prospect.
目前烤烟型造纸法薄片的原料基本上是烤烟梗和碎末，其产品的烟碱含量均较低，总体在0.6%左右，最高不超过0.8%，其吃味特点是浓度和劲头均偏低，在低档卷烟中应用有一定缺陷。另外当前通常所用的浓度较高和劲头较大的下低等上部烟叶采购量较小，无法满足低档卷烟大量高浓度、高劲头原料的需要。At present, the raw materials of flue-cured tobacco paper-making thin slices are basically flue-cured tobacco stems and shredded tobacco. The nicotine content of the products is relatively low, generally around 0.6%, and the highest is no more than 0.8%. The taste is characterized by low concentration and strength. , There are certain defects in the application of low-grade cigarettes. In addition, the currently used lower and lower upper tobacco leaves with higher concentration and greater strength are less purchased, which cannot meet the needs of low-grade cigarettes with a large amount of high concentration and high strength raw materials.
发明内容Contents of the invention
本发明利用晾晒烟烟梗的化学成分中具有比烤烟烟梗更高的烟碱、总氮含量的理化指标特性，用一定比例的晾晒烟烟梗和少量晾晒烟碎片，同时调整造纸法薄片制造的工艺条件，开发出一种烤烟型高浓度、高劲头的功能性造纸法薄片，以弥补低档卷烟原料缺乏的配方需求，同时达到降低生产成本的目的。The present invention utilizes the physical and chemical index characteristics of the chemical composition of air-dried tobacco stems having higher nicotine and total nitrogen content than that of flue-cured tobacco stems, uses a certain proportion of air-dried tobacco stems and a small amount of air-dried tobacco fragments, and simultaneously adjusts the papermaking method for sheet production. According to the technological conditions, a flue-cured tobacco-type high-density, high-strength functional paper-making sheet was developed to make up for the lack of low-grade cigarette raw materials and achieve the purpose of reducing production costs.
为实现本发明目的，这种烤烟型高烟气浓度造纸法卷烟薄片其特征是包括以下重量份数比的各原料：To achieve the purpose of the present invention, this flue-cured tobacco type high-smoke concentration paper-making cigarette sheet is characterized in that it includes the following raw materials in parts by weight:
烤烟烟梗28～32，晾晒烟烟梗28～32，烤烟烟叶碎片33～37，晾晒烟烟叶Flue-cured tobacco stems 28-32, air-dried tobacco stems 28-32, flue-cured tobacco leaf fragments 33-37, air-dried tobacco leaves
碎片3～7，木浆纤维5～8，碳酸钙8～12。Fragments 3-7, wood pulp fibers 5-8, calcium carbonate 8-12.
所述烤烟烟梗采用云南烤烟烟梗或福建烤烟烟梗；所述烤烟烟叶碎片采用云南烤烟烟叶碎片；所述晾晒烟烟叶碎片采用湖北白肋晾烟烟叶碎片；所述晾晒烟烟梗由湖北白肋烟梗和吉林晒烟梗组成，湖北白肋烟梗和吉林晒烟烟梗的重量份数比为1∶1。The flue-cured tobacco stems are Yunnan flue-cured tobacco stems or Fujian flue-cured tobacco stems; the flue-cured tobacco leaf fragments are Yunnan flue-cured tobacco leaf fragments; the air-cured tobacco leaf fragments are Hubei Burley air-cured tobacco leaf fragments; the air-cured tobacco stems are from Hubei Burley tobacco stems and Jilin sun-cured tobacco stems are composed of Hubei Burley tobacco stems and Jilin sun-cured tobacco stems at a weight ratio of 1:1.
本发明制备方法包括以下步骤：The preparation method of the present invention comprises the following steps:
a、将上述各重量份数比的烤烟烟梗、晾晒烟烟梗和烤烟烟叶碎片、晾晒烟烟叶碎片原料分别与水以1∶8的重量比混合后在50℃下浸泡；a. Mix the raw materials of flue-cured tobacco stems, air-cured tobacco stems, flue-cured tobacco leaf fragments, and air-cured tobacco leaf fragments with water at a weight ratio of 1:8 and soak at 50° C. in the above-mentioned parts by weight ratio;
b、浸泡60分钟后固液分离，分离出的固体混合后加入上述比例的木浆纤维和碳酸钙后经抄造、脱水、干燥，得到片基绝干定量为61±2g/m2的纤维薄片基片；b. After soaking for 60 minutes, solid-liquid separation, after mixing the separated solids, adding wood pulp fiber and calcium carbonate in the above ratio, papermaking, dehydration, and drying, to obtain fiber flakes with an absolute dry weight of the film base of 61 ±2g /m2 Substrate;
c、将分离出的烤烟烟叶碎片浸泡液和晾晒烟烟叶碎片浸泡液混合后在0.08～0.09Mpa、65～72℃条件下浓缩制成相对密度为1.200±0.008的烟叶碎片浓缩液；c. Mix the separated soaking solution of flue-cured tobacco leaf fragments and the soaking liquid of air-cured tobacco leaf fragments, then concentrate at 0.08-0.09Mpa and 65-72°C to prepare a concentrated solution of tobacco leaf fragments with a relative density of 1.200±0.008;
d、在上述烟叶碎片浓缩液中加入分别占浓缩液体积5‰的50%葡萄糖溶液和3‰的氨基酸溶液后制成涂布液，然后在40～50℃下将涂布液以33±2g/m2的涂布量涂布到b步骤制得的纤维薄片片基上，再经干燥后制得烤烟型造纸法卷烟薄片。d. Add 50% glucose solution and 3‰ amino acid solution respectively accounting for 5‰ of the concentrated liquid volume to the above-mentioned concentrated liquid of tobacco leaves to make a coating liquid, and then make the coating liquid at 40～50°C at 33±2g The coating amount of /m2 is applied to the fiber sheet base prepared in the b step, and then dried to obtain a flue-cured tobacco type papermaking cigarette sheet.
本发明烤烟型造纸法薄片成品与未加晾晒的烟梗、烟末对照样相比较，其常规化学分析数据和感官评吸结果如下：The flue-cured tobacco type papermaking method sheet finished product of the present invention is compared with the tobacco stem and tobacco dust control sample without drying, and its conventional chemical analysis data and sensory evaluation results are as follows:
常规化学分析数据Routine chemical analysis data
从上表可以看出，本发明方法制造的造纸法薄片比对照样烟碱、总氮有所升高，总糖、还原糖则降低，氯离子与钾离子变化不明显。It can be seen from the above table that compared with the control sample, nicotine and total nitrogen in the paper-making sheet produced by the method of the present invention are increased, total sugar and reducing sugar are decreased, and chloride ion and potassium ion have no obvious changes.
将本发明与对照样制成的卷烟进行评吸，评吸结果如下：The cigarettes made by the present invention and the reference sample are evaluated and smoked, and the smoked results are as follows:
从感官质量分析总的来说，本发明比对照样稍好，主要表现在浓度和劲头方面，而且晾晒烟气息并不明显。在刺激性和舒适性方面虽表现稍有欠缺，但经卷烟加料处理后可以满足卷烟生产需求。Generally speaking, the present invention is slightly better than the control sample in terms of sensory quality analysis, mainly in terms of concentration and vigor, and the smell of air-dried smoke is not obvious. Although it is slightly lacking in terms of irritation and comfort, it can meet the needs of cigarette production after being treated with cigarette additives.
本发明取得的技术进步：本发明制成的烤烟型造纸法薄片与未加晾晒烟梗、烟末采用普通工艺的对照样相比，采用了较传统方法较低的梗、末萃取温度，较长的萃取时间，较大的涂布量等工艺，改善了传统烤烟型造纸法薄片浓度和劲头较低的缺点，使卷烟烟气浓度和劲头得到明显提升，化学成分中烟碱、总氮含量也有所提高，而且晾晒烟气息不明显，在保证薄片感官质量和保持原有口感的前提下，最大限度增加了烟气浓度。本发明可直接应用于烤烟型卷烟中，不会影响产品风格，既可有效改善卷烟因添加造纸法薄片而导致的烟气浓度和劲头不足的现象，又能弥补高浓度低档卷烟原料缺乏的配方需求，可直接应用于烤烟型卷烟生产，具有较强的应用性和现实意义。The technical progress achieved by the present invention: the flue-cured tobacco paper-making method sheet made by the present invention is compared with the control sample that does not add air-dried tobacco stems and tobacco dust and adopts a common process, and adopts a lower stem and tobacco extraction temperature than the traditional method. Long extraction time, large coating amount and other processes have improved the disadvantages of the traditional flue-cured tobacco papermaking method, such as the low concentration and strength of the flakes, and significantly improved the smoke concentration and strength of the cigarette. The content of nicotine and total nitrogen in the chemical composition It has also improved, and the smell of air-dried smoke is not obvious. On the premise of ensuring the sensory quality of the slices and maintaining the original taste, the smoke concentration has been increased to the maximum. The invention can be directly applied to flue-cured cigarettes without affecting the product style, can effectively improve the smoke concentration and lack of strength caused by the addition of paper-making flakes, and can make up for the lack of high-concentration and low-grade cigarette raw materials. It can be directly applied to the production of flue-cured cigarettes, and has strong applicability and practical significance.
具体实施方式Detailed ways
实施例1：Example 1:
本发明烤烟型高烟气浓度造纸法卷烟薄片包括以下重量份数比的各原料：The flue-cured tobacco-type high-smoke-concentration paper-making method cigarette sheet of the present invention comprises the following raw materials in the ratio of parts by weight:
烤烟烟梗28～32，晾晒烟烟梗28～32，烤烟烟叶碎片33～37，晾晒烟烟叶Flue-cured tobacco stems 28-32, air-dried tobacco stems 28-32, flue-cured tobacco leaf fragments 33-37, air-dried tobacco leaves
碎片3～7，木浆纤维5～8，碳酸钙8～12。Fragments 3-7, wood pulp fibers 5-8, calcium carbonate 8-12.
所述烤烟烟梗采用云南烤烟烟梗或福建烤烟烟梗；所述烤烟烟叶碎片采用云南烤烟烟叶碎片；所述晾晒烟烟叶碎片采用湖北白肋晾烟烟叶碎片；所述晾晒烟烟梗由湖北白肋烟梗和吉林晒烟梗组成，湖北白肋烟梗和吉林晒烟烟梗的重量份数比为1∶1。The flue-cured tobacco stems are Yunnan flue-cured tobacco stems or Fujian flue-cured tobacco stems; the flue-cured tobacco leaf fragments are Yunnan flue-cured tobacco leaf fragments; the air-cured tobacco leaf fragments are Hubei Burley air-cured tobacco leaf fragments; the air-cured tobacco stems are from Hubei It consists of Burley tobacco stems and Jilin sun-cured tobacco stems, and the weight ratio of Hubei Burley tobacco stems and Jilin sun-cured tobacco stems is 1:1.
本发明采用以下制备工艺：The present invention adopts following preparation technology:
a、分别称取云南烤烟烟梗30kg、云南烤烟烟叶碎片35kg、湖北白肋烟梗15kg、吉林晒烟烟梗15kg、湖北白肋烟叶碎片5kg后，分别与水以1∶8的重量比混合后在50℃下进行浸泡；a. After weighing 30kg of Yunnan flue-cured tobacco stems, 35kg of Yunnan flue-cured tobacco leaf fragments, 15kg of Hubei Burley tobacco stems, 15kg of Jilin sun-cured tobacco stems, and 5kg of Hubei Burley tobacco leaf fragments, mix them with water at a weight ratio of 1:8 Then soak at 50°C;
b、浸泡60分钟后固液分离，分离出的固体混合后加入5kg木浆纤维和10kg碳酸钙制成3.2～3.5%重量浓度的抄造液，抄造液依次经纸机抄造、压榨脱水、干燥，得到片基绝干定量为61±2g/m2的纤维薄片基片；b. After soaking for 60 minutes, the solid-liquid is separated. After the separated solid is mixed, 5kg of wood pulp fiber and 10kg of calcium carbonate are added to make a papermaking solution with a weight concentration of 3.2 to 3.5%. Obtain the fibrous flake base sheet of sheet base absolute dry weight of 61 ± 2g/m2 ;
c、将分离出的烤烟烟叶碎片浸泡液和晾晒烟烟叶碎片浸泡液混合后在浓缩罐内0.08～0.09Mpa、65～72℃条件下浓缩制成相对密度为1.200±0.008的烟叶碎片浓缩液；c. Mix the separated soaking solution of flue-cured tobacco leaf fragments and the soaking liquid of air-cured tobacco leaf fragments, then concentrate in the concentration tank under the conditions of 0.08-0.09Mpa and 65-72°C to prepare a concentrated solution of tobacco leaf fragments with a relative density of 1.200±0.008;
d、在上述烟叶碎片浓缩液中加入分别占浓缩液体积5‰的50%葡萄糖水溶液和3‰的氨基酸溶液后制成涂布液（其中氨基酸溶液采用体积比为1∶1的纯度分别≥99%的L-色氨酸和L-组氨酸混配而成），然后在40～50℃下将涂布液以33±2g/m2的涂布量涂布到上述b步骤制得的纤维薄片片基上，再经干燥、碎片工序，得到本发明烤烟型造纸法卷烟薄片成品。d. Add 50% glucose aqueous solution and 3‰ amino acid solution respectively accounting for 5‰ of the concentrated liquid volume to the above-mentioned concentrated liquid of tobacco leaf fragments to make a coating liquid (wherein the amino acid solution adopts a volume ratio of 1:1 with a purity of ≥99 % of L-tryptophan and L-histidine), and then at 40-50°C, apply the coating solution at a coating amount of 33±2g /m2 to the above-mentioned step b The fibrous sheet base is dried and shredded to obtain the finished flue-cured tobacco paper-making cigarette sheet of the present invention.
实施例2：本实施例与实施例1不同之处是分别称取福建烤烟烟梗28kg、云南烤烟烟叶碎片33kg、湖北白肋烟梗16kg、吉林晒烟烟梗16kg、湖北白肋烟叶碎片7kg后，分别与水以1∶8的重量比混合后在50℃下进行浸泡；Example 2: The difference between this example and Example 1 is that 28kg of Fujian flue-cured tobacco stems, 33kg of Yunnan flue-cured tobacco leaf fragments, 16kg of Hubei Burley tobacco stems, 16kg of Jilin sun-cured tobacco stems, and 7kg of Hubei Burley tobacco leaf fragments were weighed. Afterwards, mix with water respectively at a weight ratio of 1:8 and soak at 50°C;
以下其余过程及结果与实施例1相同。Following remaining process and result are identical with embodiment 1.
实施例3：本实施例与实施例1不同之处是分别称取福建烤烟烟梗32kg、云南烤烟烟叶碎片37kg、湖北白肋烟梗14kg、吉林晒烟烟梗14kg、湖北白肋烟叶碎片3kg后，分别与水以1∶8的重量比混合后加水在50℃下进行浸泡。Example 3: The difference between this example and Example 1 is that 32kg of Fujian flue-cured tobacco stems, 37kg of Yunnan flue-cured tobacco leaf fragments, 14kg of Hubei Burley tobacco stems, 14kg of Jilin sun-cured tobacco stems, and 3kg of Hubei Burley tobacco leaf fragments were weighed. Finally, mix with water at a weight ratio of 1:8, add water and soak at 50°C.
分别称取云南烤烟烟梗30kg、云南烤烟烟叶碎片35kg、湖北白肋烟梗15kg、吉林晒烟烟梗15kg、湖北白肋烟叶碎片5kg后，分别与水以1∶8的重量比混合后在50℃下进行浸泡；Weigh respectively 30kg of Yunnan flue-cured tobacco stems, 35kg of Yunnan flue-cured tobacco leaf fragments, 15kg of Hubei Burley tobacco stems, 15kg of Jilin sun-cured tobacco stems, and 5kg of Hubei Burley tobacco leaf fragments, mix them with water at a weight ratio of 1:8 Soaking at 50°C;
以下其余过程及结果与实施例1相同。Following remaining process and result are identical with embodiment 1.
| Application Number | Priority Date | Filing Date | Title |
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| CN201510289049.8ACN105029668A (en) | 2015-06-01 | 2015-06-01 | High-smoke-concentration cigarette sheet prepared by paper-making process and preparation method of high-smoke-concentration cigarette sheet |
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| CN201510289049.8ACN105029668A (en) | 2015-06-01 | 2015-06-01 | High-smoke-concentration cigarette sheet prepared by paper-making process and preparation method of high-smoke-concentration cigarette sheet |
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| CN105029668Atrue CN105029668A (en) | 2015-11-11 |
| Application Number | Title | Priority Date | Filing Date |
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| CN201510289049.8APendingCN105029668A (en) | 2015-06-01 | 2015-06-01 | High-smoke-concentration cigarette sheet prepared by paper-making process and preparation method of high-smoke-concentration cigarette sheet |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110150720A (en)* | 2019-06-20 | 2019-08-23 | 中烟施伟策（云南）再造烟叶有限公司 | The method for preparing Chinese style flue-cured tobacco type reconstituted tobacco based on suncured tabacco type tobacco material |
| CN113712239A (en)* | 2021-09-07 | 2021-11-30 | 河北中烟工业有限责任公司 | Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102217784A (en)* | 2011-04-26 | 2011-10-19 | 范运涛 | Flue-cured type high-smoke-concentration sheet produced with paper making method and manufacturing method thereof |
| CN103005661A (en)* | 2012-12-28 | 2013-04-03 | 上海烟草集团有限责任公司 | Mixed paper-making reconstituted tobacco as well as preparation method and application thereof |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102217784A (en)* | 2011-04-26 | 2011-10-19 | 范运涛 | Flue-cured type high-smoke-concentration sheet produced with paper making method and manufacturing method thereof |
| CN103005661A (en)* | 2012-12-28 | 2013-04-03 | 上海烟草集团有限责任公司 | Mixed paper-making reconstituted tobacco as well as preparation method and application thereof |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110150720A (en)* | 2019-06-20 | 2019-08-23 | 中烟施伟策（云南）再造烟叶有限公司 | The method for preparing Chinese style flue-cured tobacco type reconstituted tobacco based on suncured tabacco type tobacco material |
| CN113712239A (en)* | 2021-09-07 | 2021-11-30 | 河北中烟工业有限责任公司 | Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler |
| CN113712239B (en)* | 2021-09-07 | 2022-11-25 | 河北中烟工业有限责任公司 | Preparation method of high-nicotine paper-making reconstituted tobacco with burley tobacco particles as filler |
| Publication | Publication Date | Title |
|---|---|---|
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | Application publication date:20151111 |