Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, setting forth the present invention further below.
Embodiment 1:
A kind of electronic cigarette cleaner ventilate stupalith, comprises the component of following weight percent:
Trichroite: 50 parts
Kaolin: 17 parts
Aluminum oxide: 15 parts
Calcium carbonate: 5 parts
Barium carbonate: 8 parts
Strontium carbonate powder: 5 parts.
A preparation method for electronic cigarette cleaner ventilate stupalith, its preparation method comprises the steps:
(1) weigh: take trichroite 50 parts, kaolin 17 parts, 15 parts, aluminum oxide, 5 parts, calcium carbonate, barium carbonate 8 parts, Strontium carbonate powder 5 parts;
(2) ball milling: use the mode that 100Kg numerical control dry type tumbling ball mill is 2:1 by ratio of grinding media to material, load weighted trichroite, kaolin, aluminum oxide, calcium carbonate, barium carbonate, Strontium carbonate powder and alumina balls are put into ball milling altar mix grinding 8 hours;
(3) pore-creating: add the pore-forming material that 5wt% Semen Maydis powder and 10wt% refining coke mix in body material, and mix 30 minutes, make it even, obtain compound;
(4) waxed slurry is added: the Chinese wax getting compound total amount 13%wt% adds heating for dissolving in the quick mixer that fills, heating top temperature is 85 DEG C, after Chinese wax all dissolves and when having slight black smoke to emerge, add compound total amount 0.3%wt% oleic acid and improve mobility, then gained compound after ball milling mixing is slowly put into quick mixer and fully stir 1h, then keep Heating temperature to be 65 DEG C and stir 2h again, obtain mixed slurry;
(5) injection forming: the mixed slurry be stirred is added in die casting board, as requested obtained ceramic form;
(6) de-waxing: to be fixedly buried in active wax removing powder by ceramic form with saggar and to carry out de-waxing, its heating curve is: intensification per hour 15 DEG C within 200 DEG C; 200 DEG C-500 DEG C intensifications per hour 30 DEG C; 500 DEG C-900 DEG C intensifications per hour 200 DEG C, finally control temperature, at 900 DEG C of insulation 1h, to naturally cool to room temperature and obtain biscuiting base substrate;
(7) sinter: be put in by biscuiting base substrate in the single hole push pedal of four-temperature region and sinter in warm electrical kiln, air vent aperture reduces gradually along with the rising of temperature, and its firing temperature curve is: intensification per hour 150 DEG C within 300 DEG C; 300 DEG C-800 DEG C intensifications per hour 200 DEG C; 800 DEG C-1310 DEG C intensifications per hour 100 DEG C, finally control temperature, 1310 DEG C of insulations 30 minutes, to naturally cool to room temperature, both electronic cigarette cleaner ventilate stupalith.
Embodiment 2:
A kind of electronic cigarette cleaner ventilate stupalith, comprises the component of following weight percent:
Trichroite: 50 parts
Kaolin: 17 parts
Aluminum oxide: 15 parts
Calcium carbonate: 5 parts
Barium carbonate: 8 parts
Strontium carbonate powder: 5 parts.
A preparation method for electronic cigarette cleaner ventilate stupalith, its preparation method comprises the steps:
(1) weigh: take trichroite 50 parts, kaolin 17 parts, 15 parts, aluminum oxide, 5 parts, calcium carbonate, barium carbonate 8 parts, Strontium carbonate powder 5 parts;
(2) ball milling: use the mode that 100Kg numerical control dry type tumbling ball mill is 2:1 by ratio of grinding media to material, load weighted trichroite, kaolin, aluminum oxide, calcium carbonate, barium carbonate, Strontium carbonate powder and alumina balls are put into ball milling altar mix grinding 12 hours;
(3) pore-creating: add the pore-forming material that 5wt% Semen Maydis powder and 10wt% refining coke mix in body material, and mix 30 minutes, make it even, obtain compound;
(4) waxed slurry is added: the Chinese wax getting compound total amount 13%wt% adds heating for dissolving in the quick mixer that fills, heating top temperature is 85 DEG C, after Chinese wax all dissolves and when having slight black smoke to emerge, add compound total amount 0.3%wt% oleic acid and improve mobility, then gained compound after ball milling mixing is slowly put into quick mixer and fully stir 1h, then keep Heating temperature to be 65 DEG C and stir 2h again, obtain mixed slurry;
(5) injection forming: the mixed slurry be stirred is added in die casting board, as requested obtained ceramic form;
(6) de-waxing: to be fixedly buried in active wax removing powder by ceramic form with saggar and to carry out de-waxing, its heating curve is: intensification per hour 15 DEG C within 200 DEG C; 200 DEG C-500 DEG C intensifications per hour 30 DEG C; 500 DEG C-900 DEG C intensifications per hour 200 DEG C, finally control temperature, at 900 DEG C of insulation 1h, to naturally cool to room temperature and obtain biscuiting base substrate;
(7) sinter: be put in by biscuiting base substrate in the single hole push pedal of four-temperature region and sinter in warm electrical kiln, air vent aperture reduces gradually along with the rising of temperature, and its firing temperature curve is: intensification per hour 150 DEG C within 300 DEG C; 300 DEG C-800 DEG C intensifications per hour 200 DEG C; 800 DEG C-1310 DEG C intensifications per hour 100 DEG C, finally control temperature, 1310 DEG C of insulations 30 minutes, to naturally cool to room temperature, both electronic cigarette cleaner ventilate stupalith.
Embodiment 3:
A kind of electronic cigarette cleaner ventilate stupalith, comprises the component of following weight percent:
Trichroite: 55 parts
Kaolin: 15 parts
Aluminum oxide: 20 parts
Calcium carbonate: 2 parts
Barium carbonate: 5 parts
Strontium carbonate powder: 3 parts.
A preparation method for electronic cigarette cleaner ventilate stupalith, its preparation method comprises the steps:
(1) weigh: take trichroite 55 parts, kaolin 15 parts, 20 parts, aluminum oxide, 2 parts, calcium carbonate, barium carbonate 5 parts, Strontium carbonate powder 3 parts;
(2) ball milling: use the mode that 100Kg numerical control dry type tumbling ball mill is 2:1 by ratio of grinding media to material, load weighted trichroite, kaolin, aluminum oxide, calcium carbonate, barium carbonate, Strontium carbonate powder and alumina balls are put into ball milling altar mix grinding 8 hours;
(3) pore-creating: 5wt% Semen Maydis powder and 10wt% refining coke and pore-forming material are mixed together and add in body material, and mix 30 minutes, make it even, obtain compound;
(3) pore-creating: add the pore-forming material that 5wt% Semen Maydis powder and 10wt% refining coke mix in body material, and mix 30 minutes, make it even, obtain compound;
(4) waxed slurry is added: the Chinese wax getting compound total amount 13%wt% adds heating for dissolving in the quick mixer that fills, heating top temperature is 85 DEG C, after Chinese wax all dissolves and when having slight black smoke to emerge, add compound total amount 0.3%wt% oleic acid and improve mobility, then gained compound after ball milling mixing is slowly put into quick mixer and fully stir 1h, then keep Heating temperature to be 65 DEG C and stir 2h again, obtain mixed slurry;
(5) injection forming: the mixed slurry be stirred is added in die casting board, as requested obtained ceramic form;
(6) de-waxing: to be fixedly buried in active wax removing powder by ceramic form with saggar and to carry out de-waxing, its heating curve is: intensification per hour 15 DEG C within 200 DEG C; 200 DEG C-500 DEG C intensifications per hour 30 DEG C; 500 DEG C-900 DEG C intensifications per hour 200 DEG C, finally control temperature, at 900 DEG C of insulation 1h, to naturally cool to room temperature and obtain biscuiting base substrate;
(7) sinter: be put in by biscuiting base substrate in the single hole push pedal of four-temperature region and sinter in warm electrical kiln, air vent aperture reduces gradually along with the rising of temperature, and its firing temperature curve is: intensification per hour 150 DEG C within 300 DEG C; 300 DEG C-800 DEG C intensifications per hour 200 DEG C; 800 DEG C-1310 DEG C intensifications per hour 100 DEG C, finally control temperature, 1310 DEG C of insulations 30 minutes, to naturally cool to room temperature, both electronic cigarette cleaner ventilate stupalith.
Embodiment 4:
A kind of electronic cigarette cleaner ventilate stupalith, comprises the component of following weight percent:
Trichroite: 55 parts
Kaolin: 15 parts
Aluminum oxide: 20 parts
Calcium carbonate: 2 parts
Barium carbonate: 5 parts
Strontium carbonate powder: 3 parts.
A preparation method for electronic cigarette cleaner ventilate stupalith, its preparation method comprises the steps:
(1) weigh: take trichroite 55 parts, kaolin 15 parts, 20 parts, aluminum oxide, 2 parts, calcium carbonate, barium carbonate 5 parts, Strontium carbonate powder 3 parts;
(2) ball milling: use the mode that 100Kg numerical control dry type tumbling ball mill is 2:1 by ratio of grinding media to material, load weighted trichroite, kaolin, aluminum oxide, calcium carbonate, barium carbonate, Strontium carbonate powder and alumina balls are put into ball milling altar mix grinding 8 hours;
(3) pore-creating: add the pore-forming material that 8wt% Semen Maydis powder and 15wt% refining coke mix in body material, and mix 30 minutes, make it even, obtain compound;
(4) waxed slurry is added: the Chinese wax getting compound total amount 13%wt% adds heating for dissolving in the quick mixer that fills, heating top temperature is 85 DEG C, after Chinese wax all dissolves and when having slight black smoke to emerge, add compound total amount 0.3%wt% oleic acid and improve mobility, then gained compound after ball milling mixing is slowly put into quick mixer and fully stir 1h, then keep Heating temperature to be 65 DEG C and stir 2h again, obtain mixed slurry;
(5) injection forming: the mixed slurry be stirred is added in die casting board, as requested obtained ceramic form;
(6) de-waxing: to be fixedly buried in active wax removing powder by ceramic form with saggar and to carry out de-waxing, its heating curve is: intensification per hour 15 DEG C within 200 DEG C; 200 DEG C-500 DEG C intensifications per hour 30 DEG C; 500 DEG C-900 DEG C intensifications per hour 200 DEG C, finally control temperature, at 900 DEG C of insulation 1h, to naturally cool to room temperature and obtain biscuiting base substrate;
(7) sinter: be put in by biscuiting base substrate in the single hole push pedal of four-temperature region and sinter in warm electrical kiln, air vent aperture reduces gradually along with the rising of temperature, and its firing temperature curve is: intensification per hour 150 DEG C within 300 DEG C; 300 DEG C-800 DEG C intensifications per hour 200 DEG C; 800 DEG C-1310 DEG C intensifications per hour 100 DEG C, finally control temperature, 1310 DEG C of insulations 30 minutes, to naturally cool to room temperature, both electronic cigarette cleaner ventilate stupalith.
Embodiment 5:
A kind of electronic cigarette cleaner ventilate stupalith, comprises the component of following weight percent:
Trichroite: 70 parts
Kaolin: 10 parts
Aluminum oxide: 15 parts
Calcium carbonate: 1 part
Barium carbonate: 3 parts
Strontium carbonate powder: 1 part
A preparation method for electronic cigarette cleaner ventilate stupalith, its preparation method comprises the steps:
(1) weigh: take trichroite 70 parts, kaolin 10 parts, 15 parts, aluminum oxide, 1 part, calcium carbonate, barium carbonate 3 parts, Strontium carbonate powder 1 part;
(2) ball milling: use the mode that 100Kg numerical control dry type tumbling ball mill is 2:1 by ratio of grinding media to material, load weighted trichroite, kaolin, aluminum oxide, calcium carbonate, barium carbonate, Strontium carbonate powder and alumina balls are put into ball milling altar mix grinding 8 hours, along with the prolongation of Ball-milling Time, the intensity of gained gas hole ceramic increases gradually, and air vent aperture reduces gradually;
(3) pore-creating: add the pore-forming material that 5wt% Semen Maydis powder and 10wt% refining coke mix in body material, and mix 30 minutes, make it even, obtain compound;
(4) waxed slurry is added: the Chinese wax getting compound total amount 13%wt% adds heating for dissolving in the quick mixer that fills, heating top temperature is 85 DEG C, after Chinese wax all dissolves and when having slight black smoke to emerge, add compound total amount 0.3%wt% oleic acid and improve mobility, then gained compound after ball milling mixing is slowly put into quick mixer and fully stir 1h, then keep Heating temperature to be 65 DEG C and stir 2h again, obtain mixed slurry;
(5) injection forming: the mixed slurry be stirred is added in die casting board, as requested obtained ceramic form;
(6) de-waxing: to be fixedly buried in active wax removing powder by ceramic form with saggar and to carry out de-waxing, its heating curve is: intensification per hour 15 DEG C within 200 DEG C; 200 DEG C-500 DEG C intensifications per hour 30 DEG C; 500 DEG C-900 DEG C intensifications per hour 200 DEG C, finally control temperature, at 900 DEG C of insulation 1h, to naturally cool to room temperature and obtain biscuiting base substrate;
(7) sinter: be put in by biscuiting base substrate in the single hole push pedal of four-temperature region and sinter in warm electrical kiln, air vent aperture reduces gradually along with the rising of temperature, and its firing temperature curve is: intensification per hour 150 DEG C within 300 DEG C; 300 DEG C-800 DEG C intensifications per hour 200 DEG C; 800 DEG C-1310 DEG C intensifications per hour 100 DEG C, finally control temperature, 1310 DEG C of insulations 30 minutes, to naturally cool to room temperature, both electronic cigarette cleaner ventilate stupalith.
Embodiment 6:
A kind of electronic cigarette cleaner ventilate stupalith, comprises the component of following weight percent:
Trichroite: 70 parts
Kaolin: 10 parts
Aluminum oxide: 15 parts
Calcium carbonate: 1 part
Barium carbonate: 3 parts
Strontium carbonate powder: 1 part
A preparation method for electronic cigarette cleaner ventilate stupalith, its preparation method comprises the steps:
(1) weigh: take trichroite 70 parts, kaolin 10 parts, 15 parts, aluminum oxide, 1 part, calcium carbonate, barium carbonate 3 parts, Strontium carbonate powder 1 part;
(2) ball milling: use the mode that 100Kg numerical control dry type tumbling ball mill is 2:1 by ratio of grinding media to material, load weighted trichroite, kaolin, aluminum oxide, calcium carbonate, barium carbonate, Strontium carbonate powder and alumina balls are put into ball milling altar mix grinding 8 hours;
(3) pore-creating: add the pore-forming material that 5wt% Semen Maydis powder and 10wt% refining coke mix in body material, and mix 30 minutes, make it even, obtain compound;
(4) waxed slurry is added: the Chinese wax getting compound total amount 13%wt% adds heating for dissolving in the quick mixer that fills, heating top temperature is 85 DEG C, after Chinese wax all dissolves and when having slight black smoke to emerge, add compound total amount 0.3%wt% oleic acid and improve mobility, then gained compound after ball milling mixing is slowly put into quick mixer and fully stir 1h, then keep Heating temperature to be 65 DEG C and stir 2h again, obtain mixed slurry;
(5) injection forming: the mixed slurry be stirred is added in die casting board, as requested obtained ceramic form;
(6) de-waxing: to be fixedly buried in active wax removing powder by ceramic form with saggar and to carry out de-waxing, its heating curve is: intensification per hour 15 DEG C within 200 DEG C; 200 DEG C-500 DEG C intensifications per hour 30 DEG C; 500 DEG C-900 DEG C intensifications per hour 200 DEG C, finally control temperature, at 900 DEG C of insulation 1h, to naturally cool to room temperature and obtain biscuiting base substrate;
(7) sinter: be put in by biscuiting base substrate in the single hole push pedal of four-temperature region and sinter in warm electrical kiln, air vent aperture reduces gradually along with the rising of temperature, and its firing temperature curve is: intensification per hour 150 DEG C within 300 DEG C; 300 DEG C-800 DEG C intensifications per hour 200 DEG C; 800 DEG C-1500 DEG C intensifications per hour 100 DEG C, finally control temperature, 1500 DEG C of insulations 30 minutes, to naturally cool to room temperature, both electronic cigarette cleaner ventilate stupalith.
The Ball-milling Time that embodiment 1 is embodiment 1 steps (2) with the difference of embodiment 2 is 8 hours, the Ball-milling Time of embodiment 2 step (2) is 12 hours, the electronic cigarette cleaner ventilate stupalith intensity of relative embodiment 2 gained of embodiment 1 is relatively low, but porosity is relatively high.
Embodiment 3 in body material, adds 5wt% Semen Maydis powder when being embodiment 3 step (3) pore-creating with the difference of embodiment 4 and 10wt% refining coke mixes pore-forming material, in body material, the pore-forming material that 8wt% Semen Maydis powder and 15wt% refining coke mix is added during embodiment 4 step (3) pore-creating, its Semen Maydis powder is not identical with the additional proportion of refining coke, the intensity of the electronic cigarette cleaner ventilate stupalith of relative embodiment 4 gained of embodiment 3 is relatively low, but porosity is relatively high.
Embodiment 5 and the difference of embodiment 6 are that temperature finally controls to be incubated at 1310 DEG C when sintering by embodiment 5 step (7), finally temperature is controlled 1500 DEG C of insulations during embodiment 6 step (7) sintering, the intensity of the electronic cigarette cleaner ventilate stupalith of relative embodiment 6 gained of embodiment 5 is relatively high, but porosity is relatively little.
Can obtain according to embodiment, the intensity of gas hole ceramic pore size and stupalith is relevant with the Ball-milling Time of matrix material, pore-forming material and sintering temperature.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.