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CN104846685B - A kind of disinfecting armaticity tissue and preparation method thereof - Google Patents

A kind of disinfecting armaticity tissue and preparation method thereof
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Publication number
CN104846685B
CN104846685BCN201510203664.2ACN201510203664ACN104846685BCN 104846685 BCN104846685 BCN 104846685BCN 201510203664 ACN201510203664 ACN 201510203664ACN 104846685 BCN104846685 BCN 104846685B
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tissue
armaticity
disinfecting
ethanol
essence extract
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CN104846685A (en
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冯向华
冯子坚
宋建生
杨海萍
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ZHEJIANG HUACHUAN INDUSTRIAL GROUP Co Ltd
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ZHEJIANG HUACHUAN INDUSTRIAL GROUP Co Ltd
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Abstract

The invention discloses a kind of disinfecting armaticity tissue and preparation method thereof, including needlebush sulfite pulp, bamboo paper fiber, straw pulp, cationic starch solution, wet strength agent, potent antibacterial agent, aromatic, titanium dioxide;Described wet strength agent is polyethylene imine resin, described potent antibacterial agent is made up of pure oxygen based quaternary ammonium salt, Radix Sophorae Flavescentis, Fructus Cnidii, Flos Lonicerae, Borneolum Syntheticum, Radix Isatidis, ethanol, distilled water, described aromatic is made up of chitosan, ethanol, essence extract, deionized water, glycerol, tripolyphosphate;Making a kind of disinfecting armaticity tissue, it has nontoxic, environmental protection, high-efficiency antimicrobial and odoriferous feature, can effectively avoid contact cross infection pathogenic bacteria in public, use more safety relieved.

Description

A kind of disinfecting armaticity tissue and preparation method thereof
Technical field
The present invention relates to a kind of disinfecting armaticity tissue and preparation method thereof.
Background technology
Tissue is also medicated napkin, is our usually relatively common in life a kind of paper, it be mainly used in some food and drink,Domestic, automobile-used, hotel and public place use, and its purposes ratio is wide, and less expensive, is deeply liked by consumerLike.
Existing tissue is all a common paper, does not possess other any characteristic, except pliability, water absorption ratioPreferably and cost ratio is beyond less expensive, just and common paper no difference, along with the requirement of the articles for daily use is improved constantly by people, listPure tissue cannot meet the demand of society, such as, the when of washing one's hands in some public arenas, typically all opens waterTap is washed one's hands, and the hands after washing is clean, but when water wring tap is closed, hands can contact again the faucet being stained with antibacterialHandle, some invisible pathogenic bacterias return on hand from newly again, at this moment would generally carry out wiping with hand towel, but general tissueThe most do not possesses antibacterial effect, it is impossible to the health of protection user;Meanwhile, some tissue all can savory produce on the market,Typically all with the addition of some chemical compositions, heard long and there will be dizzy situation, it is impossible to ensure the safety in utilization of tissue.
Summary of the invention
The technical problem to be solved in the present invention be to provide a kind of easy to use, have that antibacterial ability is strong and the fragrant effect of pure naturalThe disinfecting armaticity tissue of fruit.
For solving the problems referred to above, the present invention adopts the following technical scheme that a kind of disinfecting armaticity tissue, including withLower weight precentagewise content forms:
Needlebush sulfite pulp 14~75%
Bamboo paper fiber 12%~18%
Straw pulp 11%~23%
Cationic starch solution 1.3%~1.5%
Wet strength agent 0.3%~1%
Potent antibacterial agent 0.4%~1.3%
Aromatic 0.1%~1.6%%
Titanium dioxide 0.01%~0.3%
Described wet strength agent is polyethylene imine resin, and described potent antibacterial agent is by pure oxygen based quaternary ammonium salt 0.12%~0.23%, Radix Sophorae Flavescentis4%~7%, Fructus Cnidii 3%~5%, Flos Lonicerae 12%~16%, Borneolum Syntheticum 4%~5%, Radix Isatidis 8%~12%, 97%Ethanol 23%~35%, distilled water form, and described aromatic is carried by chitosan 5%~9%, ethanol 34%~56%, essenceTaking thing 4%~8%, deionized water 34%~56%, glycerol 6%~12%, tripolyphosphate 7%~12% forms.
Further, described cationic starch solution is cationic starch and distilled water and the mixed solution of deionized water.
Further, described essence extract is Fructus Citri Limoniae essence extract, fragrant citrus essence extract, grape essence extractionOne or more mixing in thing, tea essence extract and Mint Essence extract.
Further, described polyethylene imine resin is modified polyethyleneimine resin.
The preparation method of a kind of disinfecting armaticity tissue, comprises the following steps:
1), first needlebush sulfite pulp, bamboo paper fiber and straw pulp carrying out mix and blend in proportion, mixing time is20mim, then carries out defibrination, and making beating, the freedom making slurry is 300~400CSF;
2), then cationic starch solution and titanium dioxide join uniformly in slurry, stir and stop stirring to 50 DEG C, then addEntering wet strength agent, be subsequently adding alkali and carry out PH neutralization, pH value is more than or equal to 8;
3), again Radix Sophorae Flavescentis, Fructus Cnidii, Flos Lonicerae, Radix Isatidis grinder it is ground, obtains particulate matter, particulate matter is uniformJoin in the mixed liquor of ethanol and distilled water and mix, in mixed liquor, the most slowly drip pure oxygen based quaternary ammonium salt, Yi JijiaEntering Borneolum Syntheticum, dropping limit, limit is stirred to 60 DEG C, and mixing time is 10mim, is then cooled to room temperature temperature;
4), then chitosan join in ethanol and deionized water mixed liquor, add essence extract, glycerol, tripolyphosphateCarry out mix and blend, after having stirred, at room temperature keep 2h;
5), described step 2) in paper pulp carry out screen cloth molding, place into squeezer and squeeze, the squeezing time is30mim, then with spraying machine step 3) and step 4) mixed liquor is uniformly sprayed onto in the base paper after squeezing, is finally putting intoBe dried in dehydrator, baking temperature between 90 DEG C~100 DEG C, last molding be sterilized health care armaticity wipe handsPaper.
The invention has the beneficial effects as follows:
The most with low cost, needlebush sulfite pulp is main materials, and it is the most common materials manufacturing tissue, is simultaneously introduced bamboo pulpPaper fiber and straw pulp can effectively reduce production cost, make consumers in general all can accept;
2. good anti-bacterial effect, the bamboo paper fiber of addition has good antibacterial effect, and potent antibacterial agent uses common Chinese herbal medicineMixed liquor, and add pure oxygen based quaternary ammonium salt, it is achieved Chinese and Western combines, and has nontoxic, antibacterial effect outstanding feature;
3. having persistency fragrance, aromatic is by chitosan and essence and effective mixing of glycerol, and energy persistency is fragrant, simultaneouslyCan keep skin refreshing, chitosan has the effect well reducing bacterial activity.
4. effective guarantee user safety, all the components is all nontoxic, can be with direct skin contact, and paper qualitySoft comfortable.
Detailed description of the invention
Below the preferred embodiments of the present invention are described in detail, so that advantages and features of the invention can be easier to by thisSkilled person understands, thus protection scope of the present invention is made apparent clear and definite defining.
A kind of disinfecting armaticity tissue and preparation method thereof, forms including following weight precentagewise content:
Needlebush sulfite pulp 14~75%
Bamboo paper fiber 12%~18%
Straw pulp 11%~23%
Cationic starch solution 1.3%~1.5%
Wet strength agent 0.3%~1%
Potent antibacterial agent 0.4%~1.3%
Aromatic 0.1%~1.6%%
Titanium dioxide 0.01%~0.3%
Described wet strength agent is polyethylene imine resin, and described potent antibacterial agent is by pure oxygen based quaternary ammonium salt 0.12%~0.23%, Radix Sophorae Flavescentis4%~7%, Fructus Cnidii 3%~5%, Flos Lonicerae 12%~16%, Borneolum Syntheticum 4%~5%, Radix Isatidis 8%~12%, 97%Ethanol 23%~35%, distilled water form, and described aromatic is carried by chitosan 5%~9%, ethanol 34%~56%, essenceTaking thing 4%~8%, deionized water 34%~56%, glycerol 6%~12%, tripolyphosphate 7%~12% forms.
Described cationic starch solution is cationic starch and distilled water and the mixed solution of deionized water.
Described essence extract is Fructus Citri Limoniae essence extract, fragrant citrus essence extract, grape essence extract, tea essenceOne or more mixing in extract and Mint Essence extract.
Described polyethylene imine resin is modified polyethyleneimine resin.
The preparation method of a kind of disinfecting armaticity tissue, comprises the following steps:
1), first needlebush sulfite pulp, bamboo paper fiber and straw pulp carrying out mix and blend in proportion, mixing time is20mim, then carries out defibrination, and making beating, the freedom making slurry is 300~400CSF;
2), then cationic starch solution and titanium dioxide join uniformly in slurry, stir and stop stirring to 50 DEG C, then addEntering wet strength agent, be subsequently adding alkali and carry out PH neutralization, pH value is more than or equal to 8;
3), again Radix Sophorae Flavescentis, Fructus Cnidii, Flos Lonicerae, Radix Isatidis grinder it is ground, obtains particulate matter, particulate matter is uniformJoin in the mixed liquor of ethanol and distilled water and mix, in mixed liquor, the most slowly drip pure oxygen based quaternary ammonium salt, Yi JijiaEntering Borneolum Syntheticum, dropping limit, limit is stirred to 60 DEG C, and mixing time is 10mim, is then cooled to room temperature temperature;
4), then chitosan join in ethanol and deionized water mixed liquor, add essence extract, glycerol, tripolyphosphateCarry out mix and blend, after having stirred, at room temperature keep 2h;
5), described step 2) in paper pulp carry out screen cloth molding, place into squeezer and squeeze, the squeezing time is30mim, then with spraying machine step 3) and step 4) mixed liquor is uniformly sprayed onto in the base paper after squeezing, is finally putting intoBe dried in dehydrator, baking temperature between 90 DEG C~100 DEG C, last molding be sterilized health care armaticity wipe handsPaper.
Embodiments of the invention are presented herein below:
Embodiment one
Needlebush sulfite pulp 65%, bamboo paper fiber 18%, straw pulp 20%, cationic starch solution 1.3%, wet strength agent 0.7%, potent antibacterial agent 0.8%, aromatic 1%, titanium dioxide 0.08%;
1), first needlebush sulfite pulp, bamboo paper fiber and straw pulp carrying out mix and blend in proportion, mixing time is20mim, then carries out defibrination, and making beating, the freedom making slurry is 320CSF;
2), then cationic starch solution and titanium dioxide join uniformly in slurry, stir and stop stirring to 50 DEG C, then addEntering wet strength agent, be subsequently adding alkali and carry out PH neutralization, pH value is more than or equal to 8;
3), again Radix Sophorae Flavescentis, Fructus Cnidii, Flos Lonicerae, Radix Isatidis grinder it is ground, obtains particulate matter, particulate matter is uniformJoin in the mixed liquor of ethanol and distilled water and mix, in mixed liquor, the most slowly drip pure oxygen based quaternary ammonium salt, Yi JijiaEntering Borneolum Syntheticum, dropping limit, limit is stirred to 60 DEG C, and mixing time is 10mim, is then cooled to room temperature temperature;
4), then chitosan join in ethanol and deionized water mixed liquor, add essence extract, glycerol, tripolyphosphateCarry out mix and blend, after having stirred, at room temperature keep 2h;
5), described step 2) in paper pulp carry out screen cloth molding, place into squeezer and squeeze, the squeezing time is30mim, then with spraying machine step 3) and step 4) mixed liquor is uniformly sprayed onto in the base paper after squeezing, is finally putting intoBe dried in dehydrator, baking temperature at 90 DEG C, last molding be sterilized health care armaticity tissue.
Embodiment two
Needlebush sulfite pulp 63%, bamboo paper fiber 17%, straw pulp 16%, cationic starch solution 1.5%, wet strength agent 0.5%, potent antibacterial agent 0.6%, aromatic 1.2%, titanium dioxide 0.2%;
1), first needlebush sulfite pulp, bamboo paper fiber and straw pulp carrying out mix and blend in proportion, mixing time is20mim, then carries out defibrination, and making beating, the freedom making slurry is 355CSF;
2), then cationic starch solution and titanium dioxide join uniformly in slurry, stir and stop stirring to 50 DEG C, then addEntering wet strength agent, be subsequently adding alkali and carry out PH neutralization, pH value is more than or equal to 8;
3), again Radix Sophorae Flavescentis, Fructus Cnidii, Flos Lonicerae, Radix Isatidis grinder it is ground, obtains particulate matter, particulate matter is uniformJoin in the mixed liquor of ethanol and distilled water and mix, in mixed liquor, the most slowly drip pure oxygen based quaternary ammonium salt, Yi JijiaEntering Borneolum Syntheticum, dropping limit, limit is stirred to 60 DEG C, and mixing time is 10mim, is then cooled to room temperature temperature;
4), then chitosan join in ethanol and deionized water mixed liquor, add essence extract, glycerol, tripolyphosphateCarry out mix and blend, after having stirred, at room temperature keep 2h;
5), described step 2) in paper pulp carry out screen cloth molding, place into squeezer and squeeze, the squeezing time is30mim, then with spraying machine step 3) and step 4) mixed liquor is uniformly sprayed onto in the base paper after squeezing, is finally putting intoBe dried in dehydrator, baking temperature at 94 DEG C, last molding be sterilized health care armaticity tissue.
Embodiment three
Needlebush sulfite pulp 59%, bamboo paper fiber 16%, straw pulp 21%, cationic starch solution 1.45%, wet strength agent0.9%, potent antibacterial agent 0.11%, aromatic 1.32%, titanium dioxide 0.22%;
1), first needlebush sulfite pulp, bamboo paper fiber and straw pulp carrying out mix and blend in proportion, mixing time is20mim, then carries out defibrination, and making beating, the freedom making slurry is 375CSF;
2), then cationic starch solution and titanium dioxide join uniformly in slurry, stir and stop stirring to 50 DEG C, then addEntering wet strength agent, be subsequently adding alkali and carry out PH neutralization, pH value is more than or equal to 8;
3), again Radix Sophorae Flavescentis, Fructus Cnidii, Flos Lonicerae, Radix Isatidis grinder it is ground, obtains particulate matter, particulate matter is uniformJoin in the mixed liquor of ethanol and distilled water and mix, in mixed liquor, the most slowly drip pure oxygen based quaternary ammonium salt, Yi JijiaEntering Borneolum Syntheticum, dropping limit, limit is stirred to 60 DEG C, and mixing time is 10mim, is then cooled to room temperature temperature;
4), then chitosan join in ethanol and deionized water mixed liquor, add essence extract, glycerol, tripolyphosphateCarry out mix and blend, after having stirred, at room temperature keep 2h;
5), described step 2) in paper pulp carry out screen cloth molding, place into squeezer and squeeze, the squeezing time is30mim, then with spraying machine step 3) and step 4) mixed liquor is uniformly sprayed onto in the base paper after squeezing, is finally putting intoBe dried in dehydrator, baking temperature at 95 DEG C, last molding be sterilized health care armaticity tissue.
The above, the only detailed description of the invention of the present invention, but protection scope of the present invention is not limited thereto, and anyThe change expected without creative work or replacement, all should contain and be as the criterion at the new protection domain of this practicality.

Claims (5)

CN201510203664.2A2015-04-272015-04-27A kind of disinfecting armaticity tissue and preparation method thereofActiveCN104846685B (en)

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CN105568741A (en)*2015-12-242016-05-11浙江华川实业集团有限公司Antibacterial drug wrapping paper and preparation method thereof
CN105568771A (en)*2015-12-242016-05-11浙江华川实业集团有限公司Strong antibacterial ability medical packaging raw paper and preparation method thereof
WO2017216602A1 (en)*2016-06-142017-12-21Karimi JavadPaper products and methods of making paper products with antimicrobial properties
CN106283887A (en)*2016-08-172017-01-04安庆市新宜纸业有限公司A kind of preparation method of the napkin with stimulating effect
CN106835816A (en)*2016-12-302017-06-13安徽比伦生活用纸有限公司A kind of disinfecting tissue
CN107354817A (en)*2017-06-302017-11-17广西点图包装有限公司Toilet paper and preparation method thereof
CN108130811A (en)*2017-12-262018-06-08合肥洁诺无纺布制品有限公司A kind of medical tissue of soft comfortable
CN108130798A (en)*2017-12-262018-06-08合肥洁诺无纺布制品有限公司A kind of antibacterial medical tissue
CN108103847A (en)*2017-12-262018-06-01合肥洁诺无纺布制品有限公司A kind of medical tissue of disinfection
CN107869091A (en)*2017-12-262018-04-03合肥洁诺无纺布制品有限公司A kind of comfortable medical tissue of fragrance
CN108166308A (en)*2017-12-262018-06-15合肥洁诺无纺布制品有限公司A kind of a softer and smoother touch medical tissue
CN108130799A (en)*2017-12-282018-06-08合肥洁诺无纺布制品有限公司A kind of medical tissue of hydrophilic antimicrobial
CN108166314A (en)*2017-12-282018-06-15合肥洁诺无纺布制品有限公司A kind of low cost toughening antibacterial medical tissue
CN109330454B (en)*2018-10-252021-11-19何炽斌Production method of antibacterial colorful fragrant paper towel
CN113737565B (en)*2021-07-312022-12-02黄昱龙Preparation method of coated paper for plant functional children's readings

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CN1598139A (en)*2003-09-162005-03-23梁立Antibiotic and disinfect facial tissue and its processing method
CN102251438B (en)*2011-07-142013-01-23谷雪贤Antibacterial disinfecting fragrant hand towel and manufacturing method thereof
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