A kind of atomized liquid containing constituent of ginsengTechnical field
The invention belongs to electronic cigarette field, be specifically related to a kind of atomized liquid containing constituent of ginseng and preparation side thereofMethod.
Background technology
Along with people are more and more deep to the understanding of cigarette harm, smokers are highly desirable there is medicated cigarette substituteSave their health.Wherein, electronic cigarette is as one of medicated cigarette substitute, and smoking cessation effect is obvious.HealthyElectronic cigarette without tar, without harmful substances such as carbon monoxide, nitrogen dioxide, arsenic, lead, hydrargyrum, can avoid" second hand smoking " harm to surrounding population.Through the development of several generations, current electronic cigarette atomizing liquid taste is permissibleRealize variation, meet the demand that different taste is selected by different smoker.But electronic cigarette on the market producesProduct are main still to be given up in material addition atomized liquid formula using tobacco extract, nicotine etc. as craving for tobacco, it is impossible toReally meet the demand of consumer health's smoking cessation, especially can not meet the ring of the smoker suffering from some special diseaseCigarette Treatment need, has limited to the envelop of function of electronic cigarette product.Electronic cigarette product market potential is huge, marketUpper electronics atomized liquid function singleness, especially rare with product that Chinese medicine ingredients is tasty.
Chinese herbal medicine is the rarity of the Chinese nation, and Radix Ginseng has the good reputation of " king of BAICAO " since ancient times, more byOriental medicine circle is described as the superfine product of " YIN nourishing is mended raw, strengthening the body resistance ".Ginsenoside is the primary efficacy of Radix GinsengComposition, has strongly invigorating primordial QI, and multiple arteries and veins takes off admittedly, invigorating the spleen to benefit the lung, promoting the production of body fluid to quench thirst, the health cares such as Fructus Alpiniae Oxyphyllae of calming the nerves.
Summary of the invention
In place of shortcoming and defect for solution prior art, the primary and foremost purpose of the present invention is to provide one to containThe atomized liquid of constituent of ginseng.This atomized liquid contains ginsenoside, and nicotine content is zero, allows the ES can beProgressively while smoking cessation, absorb ginsenoside, regulate immunity of organism, improve diabetes, hypertension etc. respectivelyPlant cardiovascular disease.
Another object of the present invention is to provide the preparation method of the above-mentioned atomized liquid containing constituent of ginseng.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of atomized liquid containing constituent of ginseng, including following components in percentage by weight: 55-75% propylene glycol,10-20% glycerol, 5-10% constituent of ginseng and 5-15% distilled water；Described constituent of ginseng is ginseng essential oil and peopleGinseng extractum, above weight percentages of components sum is 100%.
Preferably, the described atomized liquid containing constituent of ginseng includes following components in percentage by weight: 72% the third twoAlcohol, 15% glycerol, 5% constituent of ginseng and 8% distilled water.
Preferably, the described atomized liquid containing constituent of ginseng includes following components in percentage by weight: 65% the third twoAlcohol, 12% glycerol, 8% constituent of ginseng and 15% distilled water.
Preferably, the described atomized liquid containing constituent of ginseng includes following components in percentage by weight: 63% the third twoAlcohol, 20% glycerol, 10% constituent of ginseng and 7% distilled water.
The preparation method of the above-mentioned atomized liquid containing constituent of ginseng, comprises the following steps:
(1) Radix Ginseng decoction pieces is pulverized and crossed 80 mesh sieves, add 95% ethanol extraction 3 of 2-3 times of Ginseng QualitySecondary, each 2h, Extracting temperature 40-50 DEG C, obtain volatile oil compositions and extracting solution；Volatile oil compositions is through oilEther extracts and is concentrated under reduced pressure to give ginseng essential oil, and extracting solution is through being concentrated under reduced pressure to give Radix Ginseng extractum；
(2) ginseng essential oil and the Radix Ginseng extractum weight sum that prepare in step (1) are calculated as constituent of ginsengWeight, weigh remaining component raw material according to the percentage by weight of each component；The Radix Ginseng that step (1) is preparedExtractum distilled water dissolves, and obtains middle drug solns；It is subsequently adding propylene glycol and glycerol stirring and evenly mixing, at the beginning of obtainingLevel atomized liquid；Add the ginseng essential oil that step (1) prepares, under the rotating speed of 3000-4000rpm allMatter emulsifying 5-10min, obtains the described atomized liquid containing constituent of ginseng.
Preferably, the temperature of step (1) described extracting solution concentrating under reduced pressure is 60 DEG C.
Preferably, the emulsifying temperature described in step (2) is 25-30 DEG C.
Compared with prior art, the present invention has the following advantages and beneficial effect:
(1) traditional electronic cigarette atomizing liquid is the composition that skims the cream off milk from Nicotiana tabacum L., is dissolved in the solvent of food stageIn, add a small amount of essence and flavoring agent simultaneously.The essence of multiple green plants extracted, being inhaled into internal hasThe unique effects remove the tobacco poisoning resting in human body, removing craving for tobacco.But, atomized liquid still contains Buddhist nun ancientThe carcinogen such as fourth, the health of harmful to human.
In atomized liquid of the present invention without tobacco extract, without nicotine, the substitute is in the addition ofMedical herbs Radix Ginseng medicinal ingredient.The present invention, by selecting the Radix Ginseng decoction pieces of high-quality, uses abstraction technique, from Radix GinsengMain active such as ginsenoside and volatile oil are isolated in middle extraction, and wherein volatile oil component abnormal smells from the patient is aromatic,Have dissipate induce sweat, the effect of causing resuscitation with aromatic drugs, it is for replacing the not only abnormal smells from the patient of the atomized liquid obtained by tobacco essenceAromatic, also there is health-care effect.
(2) atomized liquid formula of the present invention, propylene glycol, G & W ratio suitable, atomized liquid smog is dense,To throat nonirritant；Without essence and flavoring agent, the substitute is the pure natural fragrance of ginseng essential oil,Endanger without second hand smoking；The principle active component of Radix Ginseng is ginsenoside, by atomization suck entrance internal after notCan produce drug effect while of the most strongly fragrant, reach strongly invigorating primordial QI, multiple arteries and veins takes off admittedly, invigorating the spleen to benefit the lung, promoting the production of body fluid to quench thirst,Calm the nerves the health cares such as Fructus Alpiniae Oxyphyllae.
Accompanying drawing explanation
Fig. 1 is the embodiment of the present invention 1 constituent of ginseng extraction process flow chart；
Fig. 2 is the embodiment of the present invention 1 atomized liquid preparation technology flow chart containing constituent of ginseng.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, the present invention is described in further detail, but the embodiment party of the present inventionFormula is not limited to this.
The invention discloses a kind of atomized liquid containing constituent of ginseng, it includes following components in percentage by weight:55-75% propylene glycol, 10-20% glycerol, 5-10% constituent of ginseng and 5-15% distilled water.Should be containing constituent of ginsengThe preparation process of atomized liquid as follows:
(1) Radix Ginseng decoction pieces is pulverized 80 mesh sieves, add 95% ethanol extraction 3 into 2-3 times of Ginseng QualitySecondary (Extracting temperature 40-50 DEG C), each 2h, obtain volatile oil compositions and extracting solution；Volatile oil compositions is through stoneOil ether extracts and is concentrated under reduced pressure to give ginseng essential oil, and extracting solution is through being concentrated under reduced pressure to give Radix Ginseng extractum；
(2) ginseng essential oil and the Radix Ginseng extractum weight sum that prepare in step (1) are calculated as constituent of ginsengWeight, weigh remaining component raw material according to the percentage by weight of each component；The Radix Ginseng that step (1) is preparedExtractum distilled water dissolves, and obtains middle drug solns；It is subsequently adding propylene glycol and glycerol stirs, at the beginning of obtainingLevel atomized liquid；Add the ginseng essential oil that step (1) prepares, homogenized milk under the rotating speed of 3000-4000rpmChange 5-10min, obtain the described atomized liquid containing constituent of ginseng.After the atomized liquid bottling capping obtained, through going outBacterium, lamp inspection, finally packaging warehouse-in stores.
The preparation process of above-mentioned atomized liquid is after determining rational formula, mainly by abstraction technique and breastChange technology realizes.Make electronic atomized liquid have medical value and reach optimal atomizing effect, must selectSuitably extraction of panax ginseng and prepare good properties and stable atomized liquid, its each composition especially Radix GinsengVolatile oil can be uniformly distributed with aqueous phase, without effects such as composition delays during atomization.Good properties to be prepared is with steadyFixed electronic atomized liquid, needs to solve the difficult problem in stirring and emulsifying hybrid technology, designs optimal parameter, whereinTemperature, emulsification times, mixing speed all play vital effect.
Being found by experiment that, the atomized liquid water-oil phase prepared after using emulsifying stirring is uniformly dispersed, andCan keep stable, biphase being not easy separates again.This system water oil is liquid, the most i.e. can reachGood emulsifying effectiveness, higher than this temperature (40-70 DEG C) emulsifying effectiveness without writing change, the energy that high temperature consumesMore, from cost-effective angle, emulsifying temperature is set to 25-30 DEG C.
Test finding, the water-oil phase dispersion effect of the prepared atomized liquid of high rotating speed (4000-6000rpm) is good,But the foam produced during high speed emulsifying is more, and the stirring at low speed of 3000rpm can eliminate bubble.Rotating speed is too small(1000-2000rpm) shearing force is not enough so that the biphase of atomized liquid completes dispersion uniform, fine and smoothly.
Emulsification times will also result in impact to the quality of atomized liquid, owing to volatilizing in the atomized liquid formula of the present inventionThe component content of oil is less, and viscosity is relatively low, can complete dispersion within a short period of time.5-10min, is atomized vacuoleThe few oil slick of foam is few, emulsion-stabilizing.Less than 3min, owing to the time is too short, the not up to effect of stable dispersion.
Embodiment 1
The preparation method of a kind of atomized liquid containing constituent of ginseng, as illustrated in fig. 1 and 2, comprises the following steps:
(1) Radix Ginseng decoction pieces was pulverized 80 mesh sieves, added 95% ethanol of 2 times of Ginseng Qualities, extracted 3Secondary (Extracting temperature 40 DEG C), each 2h, obtain volatile oil compositions and extracting solution；Volatile oil compositions is through oilEther extracts and is concentrated under reduced pressure to give ginseng essential oil, and extracting solution is through being concentrated under reduced pressure to give Radix Ginseng extractum；
(2) ginseng essential oil and the Radix Ginseng extractum weight sum that prepare in step (1) are calculated as constituent of ginsengWeight, weigh remaining component raw material according to the percentage by weight of each component；The Radix Ginseng that step (1) is preparedExtractum distilled water dissolves, and obtains middle drug solns；It is subsequently adding propylene glycol and glycerol stirs, at the beginning of obtainingLevel atomized liquid；Add the ginseng essential oil that step (1) prepares, with vacuum homogeneous emulsifying machine at 3000rpmRotating speed under emulsifying 10min, emulsifying temperature is room temperature (25-30 DEG C), obtains described containing constituent of ginsengAtomized liquid；After the atomized liquid bottling capping obtained, sterilized, lamp inspection；
The most above-mentioned atomized liquid containing constituent of ginseng includes following components in percentage by weight: 72% propylene glycol,15% glycerol, 5% constituent of ginseng and 8% distilled water；Described constituent of ginseng is the Radix Ginseng prepared in step (1)Volatile oil and Radix Ginseng extractum.
In this embodiment, constituent of ginseng ratio is less than normal, and smog is dense, and be suitable for just having given up smoking crowd.
Embodiment 2
The preparation method of a kind of atomized liquid containing constituent of ginseng, comprises the following steps:
(1) Radix Ginseng decoction pieces was pulverized 80 mesh sieves, added 95% ethanol of 3 times of Ginseng Qualities, extracted 3Secondary, each 2h, obtain volatile oil compositions and extracting solution；Volatile oil compositions is through petroleum ether extraction and concentrating under reduced pressureObtaining ginseng essential oil, extracting solution is through being concentrated under reduced pressure to give Radix Ginseng extractum；
(2) ginseng essential oil and the Radix Ginseng extractum weight sum that prepare in step (1) are calculated as constituent of ginsengWeight, weigh remaining component raw material according to the percentage by weight of each component；The Radix Ginseng that step (1) is preparedExtractum adds distilled water, obtains middle drug solns；It is subsequently adding propylene glycol and glycerol, obtains primary atomization liquid；Add the ginseng essential oil that step (1) prepares, with vacuum homogeneous emulsifying machine under the rotating speed of 4000rpm allMatter emulsifying 5min, emulsifying temperature is room temperature (25-30 DEG C), sterilizing, lamp inspection after bottling capping, obtains describedAtomized liquid containing constituent of ginseng；
The most above-mentioned atomized liquid containing constituent of ginseng includes following components in percentage by weight: 65% propylene glycol,12% glycerol, 8% constituent of ginseng and 15% distilled water；Described constituent of ginseng is the Radix Ginseng prepared in step (1)Volatile oil and Radix Ginseng extractum.
In this embodiment, constituent of ginseng ratio is moderate, can play a role in health care.
Embodiment 3
The preparation method of a kind of atomized liquid containing constituent of ginseng, comprises the following steps:
(1) Radix Ginseng decoction pieces was pulverized 80 mesh sieves, added 95% ethanol of 2 times of Ginseng Qualities, extracted 3Secondary, each 2h, obtain volatile oil compositions and extracting solution；Volatile oil compositions is through petroleum ether extraction and concentrating under reduced pressureObtaining ginseng essential oil, extracting solution is through being concentrated under reduced pressure to give Radix Ginseng extractum；
(2) ginseng essential oil and the Radix Ginseng extractum weight sum that prepare in step (1) are calculated as constituent of ginsengWeight, weigh remaining component raw material according to the percentage by weight of each component；The Radix Ginseng that step (1) is preparedExtractum adds distilled water, obtains middle drug solns；It is subsequently adding propylene glycol and glycerol, obtains primary atomization liquid；Add the ginseng essential oil that step (1) prepares, with vacuum homogeneous emulsifying machine under the rotating speed of 3000rpm allMatter emulsifying 10min, emulsifying temperature is room temperature (25-30 DEG C), sterilizing, lamp inspection after bottling capping, obtains describedAtomized liquid containing constituent of ginseng；
The most above-mentioned atomized liquid containing constituent of ginseng includes following components in percentage by weight: 63% propylene glycol,20% glycerol, 10% constituent of ginseng and 7% distilled water；Described constituent of ginseng is the Radix Ginseng prepared in step (1)Volatile oil and Radix Ginseng extractum.
In this embodiment, Radix Ginseng medicinal ingredient ratio is higher, and atomizing effect is good, and health-care effect is obvious.
For verifying smoking cessation effect and the health-care effect of atomized liquid of the present invention, the atomized liquid in embodiment 3 is used to joinSide tests after making electronic cigarette, randomly draws 100 example smokers, all has lack of appetite, asthenia, empty cough with asthma to promoteDeng ill symptoms.Put into electronic cigarette atomizing inhaler with atomized liquid 5ml of the present invention, suck 10 every day, 2Within individual month, draw 80ml altogether.Test effect, 87% craving for tobacco is remarkably decreased, and it is equal that 63% tired and empty cough with asthma promotees symptomMake moderate progress, illustrate that atomized liquid of the present invention has remarkable result to smoking cessation, there is strongly invigorating primordial QI, spleen reinforcing benefit simultaneouslyThe health-care effects such as lung.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention are not by above-mentioned realityExecute the restriction of example, the change made under other any spirit without departing from the present invention and principle, modification,Substitute, combine, simplify, all should be the substitute mode of equivalence, within being included in protection scope of the present invention.