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CN104621705B - A kind of tobacco juice for electronic smoke containing mushroom ma extract - Google Patents

A kind of tobacco juice for electronic smoke containing mushroom ma extract
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CN104621705B
CN104621705BCN201510028056.2ACN201510028056ACN104621705BCN 104621705 BCN104621705 BCN 104621705BCN 201510028056 ACN201510028056 ACN 201510028056ACN 104621705 BCN104621705 BCN 104621705B
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extract
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mushroom
tobacco
electronic smoke
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CN104621705A (en
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薛芳
戴亚
宋光富
袁月
黄玉川
朱立军
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China Tobacco Sichuan Industrial Co Ltd
China Tobacco Chongqing Industrial Co Ltd
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China Tobacco Chuanyu Industrial Co Ltd
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Abstract

Translated fromChinese

本发明公开了一种含菇娘提取物的电子烟烟液,它由按重量份计的烟草香精1~5份,丙二醇30~50份,丙三醇30~50份,纯净水5~15份,烟碱1~2份,菇娘提取物1~10份组成。所述菇娘提取物由菇娘粉碎后采用95%乙醇进行加速溶剂萃取后再用分子蒸馏方式获得。菇娘提取物采用加速溶剂萃取与分子蒸馏相结合的手段,不仅提取率高,且去除了热敏性的轻分子物质,有利于菇娘提取物制备成的电子烟烟气的风味稳定。同时菇娘提取物制备的电子烟,能有效预防和降低电子烟烟气对吸食者咽喉及肺部刺激性,提高吸食者的舒适感。The invention discloses an electronic cigarette liquid containing mushroom extract, which comprises 1-5 parts by weight of tobacco essence, 30-50 parts of propylene glycol, 30-50 parts of glycerin, and 5-15 parts of pure water. 1 to 2 parts of nicotine, 1 to 10 parts of mushroom extract. The mushroom extract is obtained by crushing the mushroom and using 95% ethanol for accelerated solvent extraction and then molecular distillation. The mushroom extract adopts the combination of accelerated solvent extraction and molecular distillation, which not only has a high extraction rate, but also removes heat-sensitive light molecular substances, which is conducive to the stability of the flavor of the e-cigarette smoke prepared from the extract of mushroom. At the same time, the e-cigarette prepared from the mushroom extract can effectively prevent and reduce the irritation of e-cigarette smoke to the smoker's throat and lungs, and improve the comfort of the smoker.

Description

Translated fromChinese
一种含菇娘提取物的电子烟烟液An electronic cigarette smoke liquid containing mushroom extract

技术领域technical field

本发明的实施方式涉及烟草领域,更具体地,本发明的实施方式涉及一种含菇娘提取物的电子烟烟液。Embodiments of the present invention relate to the field of tobacco, and more specifically, embodiments of the present invention relate to an electronic cigarette liquid containing mushroom extract.

背景技术Background technique

菇娘,别名酸浆果、灯笼草,属于茄科酸浆属,是一种多年生药食两用草本植物,具有清热解毒、润喉止咳,治疗慢性气管炎,生津开胃降血压功效。目前市场上菇娘主要用于中药、罐头、果酒、果汁。Mushroom, alias Physalis, Physalis, belongs to Solanaceae Physalis. It is a perennial medicinal and edible herb. It has the functions of clearing away heat and detoxification, moistening throat and relieving cough, treating chronic bronchitis, promoting body fluid, appetizing and lowering blood pressure. Currently on the market, mushrooms are mainly used in traditional Chinese medicine, canned food, fruit wine, and fruit juice.

随着世界各国对公共场所吸烟的限制,传统卷烟面临诸多困难。而卷烟吸食者对吸食卷烟的依赖,导致强制性戒烟成功率很低。电子烟作为新型烟草制品的一种,应运而生。电子烟让吸食者在抽吸时有一种类似吸烟的感觉,实现“吞云吐雾”;但又不产生焦油等有害成分,没有测流烟气,不会形成二手烟危害。With the restrictions on smoking in public places around the world, traditional cigarettes are facing many difficulties. The dependence of cigarette smokers on smoking cigarettes leads to a low success rate of compulsory smoking cessation. As a new type of tobacco products, electronic cigarettes emerged as the times require. E-cigarettes allow smokers to have a smoking-like feeling when they smoke, and realize "smoke"; but it does not produce harmful components such as tar, does not measure smoke, and will not cause second-hand smoke hazards.

电子烟的“吞云吐雾”会对吸食者的咽喉及肺产生一定的刺激,因此,在电子烟烟液中加入一些能够降低电子烟对人体咽喉及肺的刺激性的物质,有望有效降低电子烟烟气对吸食者咽喉、肺的刺激性,让吸食者体验更佳,然而目前并没有将菇娘用于电子烟烟液的报道。The "swallowing and puffing" of e-cigarettes will cause certain irritation to the throat and lungs of smokers. Therefore, adding some substances that can reduce the irritation of e-cigarettes to human throat and lungs in e-cigarette liquid is expected to effectively reduce the The irritation of e-cigarette smoke to the throat and lungs of smokers makes the experience of smokers better. However, there are no reports on the use of mushrooms in e-cigarette liquids.

发明内容Contents of the invention

本发明克服了现有技术的不足,提供一种含菇娘提取物的电子烟烟液的实施方式,以期望使电子烟烟液既能满足吸食者的吸食喜好,又能保护吸食者的咽喉及肺部,维护健康。The present invention overcomes the deficiencies of the prior art, and provides an embodiment of an e-cigarette liquid containing mushroom extract, in order to make the e-cigarette liquid not only meet the smoking preferences of smokers, but also protect the throats of smokers And lungs, maintain health.

为解决上述的技术问题,本发明的一种实施方式采用以下技术方案:In order to solve the above-mentioned technical problems, one embodiment of the present invention adopts the following technical solutions:

一种含菇娘提取物的电子烟烟液,它由按重量份计的以下组分组成:An electronic cigarette liquid containing mushroom extract, which consists of the following components by weight:

烟草香精1~5份,丙二醇30~50份,丙三醇30~50份,纯净水5~15份,烟碱1~2份,菇娘提取物1~10份。1-5 parts of tobacco essence, 30-50 parts of propylene glycol, 30-50 parts of glycerol, 5-15 parts of purified water, 1-2 parts of nicotine, and 1-10 parts of mushroom extract.

根据本发明一种优选的实施方式,所述的含菇娘提取物的电子烟烟液由按重量份计的以下组分组成:According to a preferred embodiment of the present invention, the e-cigarette liquid containing mushroom extract is composed of the following components in parts by weight:

烟草香精3份,丙二醇40份,丙三醇40份,纯净水12份,烟碱2份,菇娘提取物3份。3 parts of tobacco essence, 40 parts of propylene glycol, 40 parts of glycerin, 12 parts of purified water, 2 parts of nicotine, and 3 parts of mushroom extract.

进一步的技术方案是:所述烟草香精是津巴布韦烟叶提取物,购至广州华宝香精香料有限公司。A further technical solution is: the tobacco essence is Zimbabwean tobacco leaf extract, purchased from Guangzhou Huabao Flavors and Fragrances Co., Ltd.

更进一步的技术方案是:所述菇娘提取物的制备方法是:A further technical scheme is: the preparation method of the mushroom extract is:

将菇娘粉碎,加入浓度95%的乙醇在萃取温度40~60℃、萃取压力0.7×107~1.0×107Pa条件下进行加速溶剂萃取10~30分钟,加速溶剂萃取的方式为静态萃取,萃取循环2次,然后将萃取液浓缩成浸膏,再进行分子蒸馏,收集蒸余物,即为菇娘提取物。乙醇的浓度是指乙醇溶液中乙醇的体积分数。Crush the mushrooms, add ethanol with a concentration of 95%, and perform accelerated solvent extraction for 10 to 30 minutes at an extraction temperature of 40-60°C and an extraction pressure of 0.7×107 to 1.0×107 Pa. The method of accelerated solvent extraction is static extraction , the extraction cycle is twice, and then the extract is concentrated into an extract, and then molecularly distilled, and the residue is collected, which is the mushroom extract. The concentration of ethanol refers to the volume fraction of ethanol in the ethanol solution.

更进一步的技术方案是:所述乙醇与菇娘的质量比为2~5:1。A further technical solution is: the mass ratio of the ethanol to the mushroom is 2-5:1.

更进一步的技术方案是:所述分子蒸馏的条件是:蒸馏压力50~300Pa,蒸馏温度40~80℃,加料速率2~6mL/min,转子速率250~300r/min,所述蒸余物为40~80℃的蒸余物。A further technical solution is: the conditions for the molecular distillation are: distillation pressure 50-300Pa, distillation temperature 40-80°C, feeding rate 2-6mL/min, rotor speed 250-300r/min, and the residue is Distillation residue at 40-80°C.

与现有技术相比,本发明的有益效果之一是:菇娘提取物采用加速溶剂萃取与分子蒸馏相结合的手段,不仅提取率高,且去除了热敏性的轻分子物质,有利于菇娘提取物制备成的电子烟烟气的风味稳定。同时菇娘提取物制备的电子烟,能有效预防和降低电子烟烟气对吸食者咽喉及肺部刺激性,提高吸食者的舒适感。Compared with the prior art, one of the beneficial effects of the present invention is: the extract of mushroom extract adopts the means of combining accelerated solvent extraction and molecular distillation, which not only has a high extraction rate, but also removes heat-sensitive light molecular substances, which is beneficial to the extraction of mushroom extract. The flavor of the e-cigarette smoke prepared from the extract is stable. At the same time, the e-cigarette prepared from the mushroom extract can effectively prevent and reduce the irritation of e-cigarette smoke to the smoker's throat and lungs, and improve the comfort of the smoker.

具体实施方式detailed description

为了使本发明的目的、技术方案及优点更加清楚明白,以下结合实施例,对本发明进行进一步详细说明。应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明。In order to make the object, technical solution and advantages of the present invention more clear, the present invention will be further described in detail below in conjunction with the examples. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

实施例1Example 1

一种含菇娘提取物的电子烟烟液,它由按重量份计的津巴布韦烟叶提取物3份,丙二醇40份,丙三醇40份,纯净水12份,烟碱2份,菇娘提取物3份组成。An electronic cigarette liquid containing mushroom extract, which consists of 3 parts by weight of Zimbabwean tobacco leaf extract, 40 parts of propylene glycol, 40 parts of glycerin, 12 parts of purified water, 2 parts of nicotine, and extract of mushroom Composition of 3 parts.

菇娘提取物的制备方法是:将0.1kg菇娘粉碎,加入0.25L浓度95%的乙醇在萃取温度60℃、萃取压力1.0×107Pa条件下进行加速溶剂萃取10分钟,加速溶剂萃取的方式为静态萃取,萃取循环2次,然后将萃取液浓缩成浸膏,再进行分子蒸馏,条件是:蒸馏压力50Pa,蒸馏温度40~60℃,加料速率2mL/min,转子速率250r/min,收集40~60℃蒸余物,即为菇娘提取物。The preparation method of the mushroom extract is as follows: crush 0.1kg of mushroom, add 0.25L of ethanol with a concentration of 95%, and carry out accelerated solvent extraction for 10 minutes at an extraction temperature of 60°C and an extraction pressure of 1.0×107 Pa. The method is static extraction, the extraction cycle is 2 times, and then the extract is concentrated into an extract, and then molecular distillation is carried out. The conditions are: distillation pressure 50Pa, distillation temperature 40-60°C, feeding rate 2mL/min, rotor speed 250r/min, Collect the steamed residue at 40-60°C, which is the mushroom extract.

实施例2Example 2

一种含菇娘提取物的电子烟烟液,它由按重量份计的津巴布韦烟叶提取物5份,丙二醇40份,丙三醇32份,纯净水15份,烟碱1份,菇娘提取物7份组成。An electronic cigarette liquid containing mushroom extract, which consists of 5 parts by weight of Zimbabwean tobacco leaf extract, 40 parts of propylene glycol, 32 parts of glycerin, 15 parts of purified water, 1 part of nicotine, and extract of mushroom Composition of 7 parts.

菇娘提取物的制备方法是:将0.1kg菇娘粉碎,加入0.625L浓度95%的乙醇在萃取温度50℃、萃取压力0.9×107Pa条件下进行加速溶剂萃取20分钟,加速溶剂萃取的方式为静态萃取,萃取循环2次,然后将萃取液浓缩成浸膏,再进行分子蒸馏,条件是:蒸馏压力100Pa,蒸馏温度60~80℃,加料速率4mL/min,转子速率300r/min,收集60~80℃蒸余物,即为菇娘提取物。The preparation method of the mushroom extract is as follows: crush 0.1kg mushroom, add 0.625L of ethanol with a concentration of 95%, and carry out accelerated solvent extraction for 20 minutes at an extraction temperature of 50°C and an extraction pressure of 0.9×107 Pa. The method is static extraction, the extraction cycle is 2 times, then the extract is concentrated into an extract, and then molecular distillation is carried out, the conditions are: distillation pressure 100Pa, distillation temperature 60-80°C, feeding rate 4mL/min, rotor speed 300r/min, Collect the steamed residue at 60-80°C, which is the mushroom extract.

实施例3Example 3

一种含菇娘提取物的电子烟烟液,它由按重量份计的津巴布韦烟叶提取物1份,丙二醇30份,丙三醇50份,纯净水7份,烟碱2份,菇娘提取物10份组成。An electronic cigarette liquid containing mushroom extract, which consists of 1 part by weight of Zimbabwean tobacco leaf extract, 30 parts of propylene glycol, 50 parts of glycerol, 7 parts of purified water, 2 parts of nicotine, and extract of mushroom Composition of 10 parts.

菇娘提取物的制备方法是:将0.1kg菇娘粉碎,加入0.375L浓度95%的乙醇在萃取温度40℃、萃取压力0.7×107Pa条件下进行加速溶剂萃取30分钟,加速溶剂萃取的方式为静态萃取,萃取循环2次,然后将萃取液浓缩成浸膏,再进行分子蒸馏,条件是:蒸馏压力300Pa,蒸馏温度40~80℃,加料速率6mL/min,转子速率260r/min,收集40~80℃蒸余物,即为菇娘提取物。The preparation method of the mushroom extract is as follows: crush 0.1kg mushroom, add 0.375L of ethanol with a concentration of 95%, and carry out accelerated solvent extraction for 30 minutes at an extraction temperature of 40°C and an extraction pressure of 0.7×107 Pa. The method is static extraction, the extraction cycle is 2 times, and then the extract is concentrated into an extract, and then molecular distillation is carried out. The conditions are: distillation pressure 300Pa, distillation temperature 40-80°C, feeding rate 6mL/min, rotor speed 260r/min, Collect the steamed residue at 40-80°C, which is the mushroom extract.

实施例4Example 4

一种含菇娘提取物的电子烟烟液,它由按重量份计的津巴布韦烟叶提取物3份,丙二醇50份,丙三醇38份,纯净水6份,烟碱2份,菇娘提取物1份组成。An electronic cigarette liquid containing mushroom extract, which consists of 3 parts by weight of Zimbabwean tobacco leaf extract, 50 parts of propylene glycol, 38 parts of glycerol, 6 parts of purified water, 2 parts of nicotine, and extract of mushroom Composition of 1 part.

菇娘提取物的制备方法是:将0.1kg菇娘粉碎,加入0.375L浓度95%的乙醇在萃取温度40℃、萃取压力0.8×107Pa条件下进行加速溶剂萃取25分钟,加速溶剂萃取的方式为静态萃取,萃取循环2次,然后将萃取液浓缩成浸膏,再进行分子蒸馏,条件是:蒸馏压力200Pa,蒸馏温度60~80℃,加料速率4mL/min,转子速率280r/min,收集60~80℃蒸余物,即为菇娘提取物。The preparation method of the mushroom extract is as follows: crush 0.1kg mushroom, add 0.375L of ethanol with a concentration of 95%, and carry out accelerated solvent extraction for 25 minutes at an extraction temperature of 40°C and an extraction pressure of 0.8×107 Pa. The method is static extraction, the extraction cycle is 2 times, and then the extract is concentrated into an extract, and then molecular distillation is carried out. The conditions are: distillation pressure 200Pa, distillation temperature 60-80℃, feeding rate 4mL/min, rotor speed 280r/min, Collect the steamed residue at 60-80°C, which is the mushroom extract.

尽管这里参照本发明的多个解释性实施例对本发明进行了描述,但是,应该理解,本领域技术人员可以设计出很多其他的修改和实施方式,这些修改和实施方式将落在本申请公开的原则范围和精神之内。更具体地说,在本申请公开和权利要求的范围内,可以对主题组合布局的组成部件和/或布局进行多种变型和改进。除了对组成部件和/或布局进行的变型和改进外,对于本领域技术人员来说,其他的用途也将是明显的。Although the invention has been described herein with reference to a number of illustrative embodiments thereof, it is to be understood that numerous other modifications and implementations can be devised by those skilled in the art which will fall within the scope of the disclosure disclosed in this application. within the scope and spirit of the principles. More specifically, within the scope of the disclosure and claims of the present application, various modifications and improvements can be made to the components and/or layout of the subject combination layout. In addition to modifications and improvements in component parts and/or layout, other uses will be apparent to those skilled in the art.

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CN104856216A (en)*2015-05-312015-08-26中国烟草总公司郑州烟草研究院Treatment method for concrete and absolute type natural extractive suitable for electronic cigarette
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