Movatterモバイル変換


[0]ホーム

URL:


CN104026729B - An electronic cigarette liquid with burnt aroma - Google Patents

An electronic cigarette liquid with burnt aroma
Download PDF

Info

Publication number
CN104026729B
CN104026729BCN201410287554.4ACN201410287554ACN104026729BCN 104026729 BCN104026729 BCN 104026729BCN 201410287554 ACN201410287554 ACN 201410287554ACN 104026729 BCN104026729 BCN 104026729B
Authority
CN
China
Prior art keywords
electronic cigarette
cigarette liquid
cigarettes
aroma
tobacco
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201410287554.4A
Other languages
Chinese (zh)
Other versions
CN104026729A (en
Inventor
赵国玲
黎艳玲
杨华武
黄建国
李亚白
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hunan Industrial Co LtdfiledCriticalChina Tobacco Hunan Industrial Co Ltd
Priority to CN201410287554.4ApriorityCriticalpatent/CN104026729B/en
Publication of CN104026729ApublicationCriticalpatent/CN104026729A/en
Application grantedgrantedCritical
Publication of CN104026729BpublicationCriticalpatent/CN104026729B/en
Activelegal-statusCriticalCurrent
Anticipated expirationlegal-statusCritical

Links

Landscapes

Abstract

Translated fromChinese

本发明公开一种具有焦香香气的电子烟液,每10—50mL所述电子烟液体制备方法为:将20—40g白砂糖或者红糖,优选白砂糖溶于10—30mL的水中,在80—150℃条件下加热5—15min,然后加入5—10g烟末或者烟丝,优选烟末,升温至180—250℃回流加热10—20min,将回流加热后的产物溶于10—50mL甘油、乙醇和水的混合液,或者甘油,或者丙二醇中,过滤后即得电子烟液。本发明电子烟液可提高电子烟的内在抽吸品质,使电子烟更接近卷烟的香气、口味。The invention discloses an electronic cigarette liquid with burnt aroma. The preparation method of the electronic cigarette liquid per 10-50mL is as follows: dissolving 20-40g of white sugar or brown sugar, preferably white sugar, in 10-30mL of water; Heat at 150°C for 5-15min, then add 5-10g of tobacco powder or shredded tobacco, preferably tobacco powder, heat up to 180-250°C for 10-20min under reflux, and dissolve the product after reflux heating in 10-50mL of glycerin, ethanol and Mixture of water, or glycerin, or propylene glycol, after filtration, the e-cigarette liquid is obtained. The electronic cigarette liquid of the present invention can improve the internal smoking quality of the electronic cigarette, and make the electronic cigarette closer to the aroma and taste of cigarettes.

Description

Translated fromChinese
一种具有焦香香气的电子烟液An electronic cigarette liquid with burnt aroma

技术领域technical field

本发明属于电子烟技术领域,具体涉及一种具有焦香香气的电子烟液。The invention belongs to the technical field of electronic cigarettes, and in particular relates to an electronic cigarette liquid with burnt aroma.

背景技术Background technique

近年来,随着传统烟草制品的销量在一些发达国家市场出现停滞甚至下降,以及许多国家公共场所禁烟力度的不断加大,低温卷烟、无烟气烟草制品、电子烟等新型烟草制品正在快速兴起,菲莫国际、英美烟草、日本烟草等跨国烟草公司也从战略高度积极研发推广新型烟草制品。电子烟外形与普通香烟相似,是一种能够把尼古丁溶液汽化成雾气的装置,通过模拟抽真烟,给吸烟者带来刺激感。它由锂电池(可充电)、雾化器(加热元件)、烟弹(通常看到的烟嘴)等元件构成。电子烟是将含有烟碱的溶液雾化,通过肺部吸收,使消费者获得类似吸食传统卷烟的满足感。In recent years, as the sales of traditional tobacco products have stagnated or even declined in some developed countries, and the ban on smoking in public places in many countries has continued to increase, new tobacco products such as low-temperature cigarettes, smokeless tobacco products, and electronic cigarettes are rapidly emerging. At present, multinational tobacco companies such as Philip Morris International, British American Tobacco, and Japan Tobacco are also actively developing and promoting new tobacco products from a strategic height. E-cigarettes are similar in appearance to ordinary cigarettes. They are devices that can vaporize nicotine solution into mist. By simulating smoking real cigarettes, they can bring stimulation to smokers. It consists of lithium batteries (rechargeable), atomizers (heating elements), pods (commonly seen cigarette holders) and other components. Electronic cigarettes atomize a solution containing nicotine and absorb it through the lungs, so that consumers can obtain a sense of satisfaction similar to smoking traditional cigarettes.

电子烟在满足人们抽烟的习惯的同时减少了对人的身体的伤害。概括而言,电子烟具有以下一些主要特征:一是不需要燃烧,极大减少因燃烧产生的焦油和有害成分,相比传统卷烟危害性较小;二是不会产生二手烟气,不会对公共环境产生影响,在一定程度上缓解了吸烟和公共场所禁烟的矛盾;三是能在一定程度上适应和满足消费者的生理需要。电子烟经过几代的发展,目前已和传统卷烟外型基本一致,口味可以实现多样化,同时电子烟中不含烟焦油,对人身体伤害较小。E-cigarettes reduce harm to people's bodies while satisfying people's smoking habits. In a nutshell, electronic cigarettes have the following main features: First, they do not need to be burned, which greatly reduces the tar and harmful components produced by burning, and are less harmful than traditional cigarettes; second, they do not produce second-hand smoke and do not It has an impact on the public environment, and to a certain extent, alleviates the contradiction between smoking and smoking bans in public places; third, it can adapt to and meet the physiological needs of consumers to a certain extent. After several generations of development, electronic cigarettes have basically the same appearance as traditional cigarettes, and the taste can be diversified. At the same time, electronic cigarettes do not contain tobacco tar, which is less harmful to human body.

中国专利CN201110184068.6公开的一种电子烟液的制备方法,称取电子烟液量的5-20%的烟叶投入提取罐,将配制好的溶媒加入到提取罐中浸泡烟叶30-100分钟,加热至40-60度,温浸提取2-8小时,过滤提取液,向滤液中加入电子烟液量的1-10%的可可豆提取物,搅拌混合20-40分钟;再以丙二醇或聚乙二醇补足到100%。虽然使用了烟叶提取物,但仍然是模拟香烟口味以烟叶提取物与其他香精香料调配的产品。由于越来越多的吸烟者开始接受使用电子烟代替香烟,用于这些电子烟的电子烟液的一些不足也越来越明显。据调查研究,电子烟与普通卷烟相比,虽然形状、手感、烟雾等感觉像卷烟,但用于这些电子烟液产生的烟雾在香气、口味方面,与真正的卷烟感觉差距较大,这些不足,大大影响了电子烟的品质。吸烟者普遍反映,电子烟与香烟相比,虽然形状、手感、烟雾等感觉像香烟,但在香气、口味等方面,与香烟的感觉差距比较大,尤其以各种香精香料调配成的产品,他们难以接受或习惯其香气和口味。这些不足大大影响了电子烟的品质,同时也制约着电子烟的普及及流行。而且传统的烟叶提取物主要是将烟叶或者烟丝用乙醇或者水在一定温度下回流提取,难以将烟叶中的焦香香气提取出来。Chinese patent CN201110184068.6 discloses a preparation method of e-cigarette liquid, weighing 5-20% of the amount of e-cigarette liquid into the extraction tank, adding the prepared solvent into the extraction tank to soak the tobacco leaves for 30-100 minutes, Heating to 40-60 degrees, soaking and extracting for 2-8 hours, filtering the extract, adding 1-10% cocoa bean extract to the filtrate, stirring and mixing for 20-40 minutes; Ethylene glycol make up to 100%. Although tobacco leaf extract is used, it is still a product that simulates the taste of cigarettes and blends tobacco leaf extract with other flavors and fragrances. As more and more smokers begin to accept the use of e-cigarettes instead of cigarettes, some shortcomings of the e-liquids used in these e-cigarettes are also becoming more and more obvious. According to investigations and studies, compared with ordinary cigarettes, electronic cigarettes feel like cigarettes in shape, feel, and smoke, but the smoke produced by these e-cigarette liquids has a large gap with real cigarettes in terms of aroma and taste. , which greatly affects the quality of electronic cigarettes. Smokers generally report that compared with cigarettes, electronic cigarettes feel like cigarettes in shape, feel, and smoke, but in terms of aroma, taste, etc., there is a big gap with the feeling of cigarettes, especially products that are blended with various flavors and fragrances. They have difficulty accepting or getting used to its aroma and taste. These deficiencies greatly affect the quality of electronic cigarettes, and also restrict the popularization and popularity of electronic cigarettes. Moreover, the traditional tobacco leaf extract mainly uses ethanol or water to reflux the tobacco leaves or shredded tobacco to extract at a certain temperature, so it is difficult to extract the burnt aroma in the tobacco leaves.

发明内容Contents of the invention

本发明的目的在于针对现有电子烟液在香气、口感等抽吸感觉方面的不足,提供一种利用白砂糖或者红糖为原料,在一定温度下和烟末或者烟丝进行焦糖化反应,得到的具有焦香香气的电子烟液。The purpose of the present invention is to address the shortcomings of existing e-cigarette liquids in terms of aroma and mouthfeel, and to provide a product that uses white sugar or brown sugar as a raw material, and carries out caramelization reaction with tobacco powder or shredded tobacco at a certain temperature. E-liquid with burnt aroma.

为了达到上述目的,本发明提供的技术方案为:In order to achieve the above object, the technical solution provided by the invention is:

每10—50mL所述具有焦香香气的电子烟液制备方法如下:The preparation method of the e-cigarette liquid with burnt aroma per 10-50mL is as follows:

将20—40g糖,优选白砂糖或红糖,更优选白砂糖溶于10—30mL的水中,在80—150℃条件下加热5—15min,然后加入5—10g烟末或者烟丝,优选烟末,升温至180—250℃回流加热10—20min,将回流加热后的产物溶于10—50mL的甘油、乙醇和水的混合液,或者甘油,或者丙二醇中,过滤后即得电子烟液。一般来说,电子烟液的溶剂是70%甘油(质量百分比)、20%乙醇(质量百分比)和10%水(质量百分比),可以溶解不同极性的物质,本发明的溶剂可以是甘油、乙醇和水的混合溶剂,也可以是只用甘油或丙二醇。Dissolve 20-40g of sugar, preferably white sugar or brown sugar, more preferably white sugar, in 10-30mL of water, heat at 80-150°C for 5-15min, then add 5-10g of tobacco powder or shredded tobacco, preferably tobacco powder, Raise the temperature to 180-250°C and reflux for 10-20 minutes, dissolve the reflux-heated product in 10-50mL of a mixture of glycerin, ethanol and water, or glycerin, or propylene glycol, and filter to obtain e-cigarette liquid. Generally speaking, the solvent of e-cigarette liquid is 70% glycerin (mass percentage), 20% ethanol (mass percentage) and 10% water (mass percentage), which can dissolve substances of different polarities. The solvent of the present invention can be glycerin, A mixed solvent of ethanol and water, or only glycerin or propylene glycol.

本发明利用白砂糖或者红糖为原料,在一定温度下和烟末、烟丝或者烟灰进行焦糖化反应,得到具有焦香香气的产物。这种香型的致香物和传统卷烟燃烧过程中产生焦香香气成分相似,这种具有焦香香型的电子烟液经过雾化器雾化后,抽吸者感觉这种电子烟液和传统卷烟燃烧过程中的感受一致,有卷烟燃烧过程中的焦香。本发明电子烟液可提高电子烟的内在抽吸品质,使电子烟更接近卷烟的香气、口味。The invention uses white granulated sugar or brown sugar as a raw material, and carries out caramelization reaction with tobacco powder, shredded tobacco or soot at a certain temperature to obtain a product with a burnt aroma. The fragrance-inducing substance of this flavor is similar to the burnt aroma components produced in the burning process of traditional cigarettes. After the e-liquid with burnt aroma is atomized by the atomizer, the smoker feels that the e-cigarette liquid is different from traditional cigarettes. The feeling during the burning process is the same, with the burnt aroma of the cigarette burning process. The electronic cigarette liquid of the present invention can improve the internal smoking quality of the electronic cigarette, and make the electronic cigarette closer to the aroma and taste of cigarettes.

具体实施方式Detailed ways

实施例1Example 1

所述具有焦香香气的电子烟液制备方法如下:The preparation method of the e-cigarette liquid with burnt aroma is as follows:

将20g白砂糖溶于10mL的水中,在150℃条件下加热10min,然后加入7g云南邵通B3F烟末,升温至180℃回流加热15min,将回流加热后的产物溶于20mL的甘油中,过滤后即得电子烟液。Dissolve 20g of white granulated sugar in 10mL of water, heat at 150°C for 10min, then add 7g of Yunnan Shaotong B3F tobacco powder, heat up to 180°C for 15min under reflux, dissolve the product after reflux heating in 20mL of glycerin, filter After that, the electronic cigarette liquid is obtained.

取1mL电子烟液加入雾化器中,请专业的评吸人员评吸,有烤烟的焦甜香,同时还有烤烟的烘烤香。Take 1mL of e-cigarette liquid and add it to the atomizer, and ask professional vapers to smoke it. It has the burnt and sweet aroma of flue-cured tobacco, as well as the roasted aroma of flue-cured tobacco.

实施例2Example 2

所述具有焦香香气的电子烟液制备方法如下:The preparation method of the e-cigarette liquid with burnt aroma is as follows:

将25g白砂糖溶于15mL的水中,在130℃条件下加热10min,然后加入5g桑植B3F烟末,升温至180℃回流加热20min,将回流加热后的产物溶于25mL质量百分比为10%的水、质量百分比为70%的甘油、质量百分比为20%的乙醇的混合液中,过滤后即得电子烟液。Dissolve 25g of white sugar in 15mL of water, heat at 130°C for 10min, then add 5g of Sangzhi B3F tobacco powder, heat up to 180°C for 20min under reflux, and dissolve the product after reflux heating in 25mL of 10% by mass Water, glycerin with a mass percentage of 70%, and ethanol with a mass percentage of 20% are mixed, and the electronic cigarette liquid is obtained after filtering.

取1mL电子烟液加入雾化器中,请专业的评吸人员评吸,有烤烟的焦甜香。Take 1mL of e-cigarette liquid and add it to the atomizer, ask professional vapers to smoke it, it has the burnt and sweet aroma of flue-cured tobacco.

实施例3Example 3

所述具有焦香香气的电子烟液制备方法如下:The preparation method of the e-cigarette liquid with burnt aroma is as follows:

将35g白砂糖溶于30mL的水中,在140℃条件下加热10min,然后加入8g津巴布韦L1OF烟末,升温至180℃回流加热20min,将回流加热后的产物溶于30mL的甘油中,过滤后即得电子烟液。Dissolve 35g of white sugar in 30mL of water, heat at 140°C for 10min, then add 8g of Zimbabwean L1OF tobacco powder, heat up to 180°C for 20min under reflux, dissolve the product after reflux heating in 30mL of glycerin, and filter it Get e-liquid.

取1mL电子烟液加入雾化器中,请专业的评吸人员评吸,有烤烟的焦甜香。Take 1mL of e-cigarette liquid and add it to the atomizer, ask professional vapers to smoke it, it has the burnt and sweet aroma of flue-cured tobacco.

Claims (2)

CN201410287554.4A2014-06-252014-06-25 An electronic cigarette liquid with burnt aromaActiveCN104026729B (en)

Priority Applications (1)

Application NumberPriority DateFiling DateTitle
CN201410287554.4ACN104026729B (en)2014-06-252014-06-25 An electronic cigarette liquid with burnt aroma

Applications Claiming Priority (1)

Application NumberPriority DateFiling DateTitle
CN201410287554.4ACN104026729B (en)2014-06-252014-06-25 An electronic cigarette liquid with burnt aroma

Publications (2)

Publication NumberPublication Date
CN104026729A CN104026729A (en)2014-09-10
CN104026729Btrue CN104026729B (en)2015-11-04

Family

ID=51457897

Family Applications (1)

Application NumberTitlePriority DateFiling Date
CN201410287554.4AActiveCN104026729B (en)2014-06-252014-06-25 An electronic cigarette liquid with burnt aroma

Country Status (1)

CountryLink
CN (1)CN104026729B (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
CN104432481B (en)*2014-10-222016-03-30浙江中烟工业有限责任公司Electronic cigarette liquid solvent using polypropylene glycol, electronic cigarette liquid prepared from electronic cigarette liquid solvent, and electronic cigarette
CN104287084B (en)*2014-11-122016-06-08湖南中烟工业有限责任公司 A kind of electronic cigarette liquid and electronic cigarette
CN106947596B (en)*2017-04-122020-12-25安徽中烟工业有限责任公司Preparation method of maltose caramel spice for cigarettes
CN107692318A (en)*2017-10-132018-02-16上海烟草集团有限责任公司A kind of tobacco juice for electronic smoke and preparation method
CN111248489A (en)*2020-01-162020-06-09四川中烟工业有限责任公司 Preparation method of burnt sweet burnt aroma cigar tobacco leaves
CN111254014A (en)*2020-03-052020-06-09四川中烟工业有限责任公司Caramel aroma spice, preparation method and application method thereof
CN111588073A (en)*2020-03-052020-08-28四川中烟工业有限责任公司Burnt sweet-fragrance electronic cigarette tobacco tar, preparation method and application method
CN111411020A (en)*2020-03-052020-07-14四川中烟工业有限责任公司Burnt sweet-fragrance bead-blasting oil, preparation method and application method
CN112369651B (en)*2020-04-162022-11-11湖北中烟工业有限责任公司 A kind of tobacco flavor electronic lampblack and preparation method thereof
CN111602838A (en)*2020-06-122020-09-01山东瑞博斯烟草有限公司Feed liquid for increasing scorched and sweet aroma of tobacco leaves and method for treating tobacco leaves
CN112205663A (en)*2020-09-282021-01-12四川中烟工业有限责任公司Composite burnt sweet aroma flavor, extrusion puffing preparation method and application method thereof
CN112205659A (en)*2020-09-282021-01-12四川中烟工业有限责任公司 A kind of compound coke sweet aroma spice, baking preparation method and application
CN114903196B (en)*2022-05-112023-03-24河北中烟工业有限责任公司Coloring additive for tobacco, preparation method thereof and heated cigarette

Citations (6)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
US3920026A (en)*1972-03-071975-11-18Liggett & Myers IncTobacco with flavor enhancer
CN1106640A (en)*1994-02-031995-08-16锦州卷烟厂Method for preparing health cigarette of reduced tar content
CN101461566A (en)*2009-01-082009-06-24华健Atomized liquid of electronic smoke
CN101580757A (en)*2009-06-022009-11-18上海英华香精香料有限公司Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method
CN103783658A (en)*2014-01-212014-05-14杨成云Preparation method of nicotine liquid perfume
CN103849467A (en)*2014-03-122014-06-11河南中烟工业有限责任公司Method for preparing tobacco flavor through maillard reaction with tobacco flower buds as raw material

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
US3920026A (en)*1972-03-071975-11-18Liggett & Myers IncTobacco with flavor enhancer
CN1106640A (en)*1994-02-031995-08-16锦州卷烟厂Method for preparing health cigarette of reduced tar content
CN101461566A (en)*2009-01-082009-06-24华健Atomized liquid of electronic smoke
CN101580757A (en)*2009-06-022009-11-18上海英华香精香料有限公司Preparation method of Coca-Cola flavour for tobacco and product and application thereof adopting the method
CN103783658A (en)*2014-01-212014-05-14杨成云Preparation method of nicotine liquid perfume
CN103849467A (en)*2014-03-122014-06-11河南中烟工业有限责任公司Method for preparing tobacco flavor through maillard reaction with tobacco flower buds as raw material

Also Published As

Publication numberPublication date
CN104026729A (en)2014-09-10

Similar Documents

PublicationPublication DateTitle
CN104026729B (en) An electronic cigarette liquid with burnt aroma
CN102349699B (en)Preparation method for electronic cigarette liquid
RU2593362C2 (en)Nicotine replacement cytisine oral atomised liquid and method of its preparation
CN101536737B (en) A kind of preparation method of chewing tobacco
CN104585860B (en)There is the preparation method of the tobacco juice for electronic smoke of the fragrant feature of baking
CN104939305B (en)A kind of tobacco extract and electronic cigarette liquid
CN105249524A (en)Fragrance type heating nonflammable tobacco product and preparation method thereof
CN104403794A (en)Preparation method and application of Pu'er tea extract to cigarettes
CN104026728A (en)Electronic tobacco juice with baking aroma
CN104531356B (en)Sweet fragrant additive and the electronic cigarette liquid with sweet perfume
CN101233890A (en)Hard sugar containing tobacco component
CN110771936A (en)Tobacco shred and preparation method and application thereof
CN106381225A (en)Nut-flavored cigarette midline adhesive essence, and preparation method and application thereof
CN108949347A (en) Essence for increasing the moistness of heat-not-burn cigarette smoke and its preparation method and application
CN104544546A (en)Electronic cigarette smoke solution with appetite improving and digestion prompting functions
CN104068469B (en)A kind of electronic cigarette liquid with sootiness fragrance
CN102423120A (en)Litsea cubeba skin type smoke-free tobacco product
CN114468345B (en) An electronic cigarette smoke liquid with prickly ash flavor and preparation method thereof
CN108991589B (en) Flavor for reducing thorns and impurities in heat-not-burn tobacco, preparation method and application thereof
CN102823940A (en)Cigarette aroma-enhancement humectant as well as preparation method and application thereof
CN105011351A (en)Electronic cigarette liquid with tartary buckwheat fragrance
CN107692318A (en)A kind of tobacco juice for electronic smoke and preparation method
CN103892437B (en)A kind of production method of novel tobacco goods
KR20130046729A (en)Manufacturing method of electronic cigarette liquid
CN108669634A (en)The tobacco compositions of drink style, smoke section and heating are not burnt cigarette cigarette stick

Legal Events

DateCodeTitleDescription
C06Publication
PB01Publication
C10Entry into substantive examination
SE01Entry into force of request for substantive examination
C14Grant of patent or utility model
GR01Patent grant

[8]ページ先頭

©2009-2025 Movatter.jp