CN103789090A - Flowering tobacco volatile extraction method and preparation method for microcapsules of flowering tobacco - Google Patents
Flowering tobacco volatile extraction method and preparation method for microcapsules of flowering tobaccoDownload PDFInfo
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- CN103789090A CN103789090ACN201410055423.3ACN201410055423ACN103789090ACN 103789090 ACN103789090 ACN 103789090ACN 201410055423 ACN201410055423 ACN 201410055423ACN 103789090 ACN103789090 ACN 103789090A
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- tobacco
- volatile matter
- preparation
- cyclodextrin
- microcapsule
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- 239000003094microcapsuleSubstances0.000titleclaimsabstractdescription31
- 238000002360preparation methodMethods0.000titleclaimsabstractdescription24
- 238000000605extractionMethods0.000titleclaimsabstractdescription13
- 244000061322Nicotiana alataSpecies0.000titleabstract7
- 241000208125NicotianaSpecies0.000claimsabstractdescription78
- 235000002637Nicotiana tabacumNutrition0.000claimsabstractdescription75
- 238000000034methodMethods0.000claimsabstractdescription21
- 229920000858CyclodextrinPolymers0.000claimsabstractdescription16
- XLYOFNOQVPJJNP-UHFFFAOYSA-NwaterChemical compoundOXLYOFNOQVPJJNP-UHFFFAOYSA-N0.000claimsabstractdescription16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-NEthanolChemical compoundCCOLFQSCWFLJHTTHZ-UHFFFAOYSA-N0.000claimsabstractdescription13
- 239000012153distilled waterSubstances0.000claimsabstractdescription13
- HFHDHCJBZVLPGP-UHFFFAOYSA-Nschardinger α-dextrinChemical compoundO1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2COHFHDHCJBZVLPGP-UHFFFAOYSA-N0.000claimsabstractdescription9
- FAPWRFPIFSIZLT-UHFFFAOYSA-MSodium chlorideChemical compound[Na+].[Cl-]FAPWRFPIFSIZLT-UHFFFAOYSA-M0.000claimsabstractdescription7
- 238000005406washingMethods0.000claimsabstractdescription6
- 239000011780sodium chlorideSubstances0.000claimsabstractdescription4
- 238000001035dryingMethods0.000claimsabstractdescription3
- 238000000967suction filtrationMethods0.000claimsabstractdescription3
- 239000000284extractSubstances0.000claimsdescription11
- 238000004821distillationMethods0.000claimsdescription9
- 150000003839saltsChemical class0.000claimsdescription6
- 238000010790dilutionMethods0.000claimsdescription5
- 239000012895dilutionSubstances0.000claimsdescription5
- 239000001116FEMA 4028Substances0.000claimsdescription4
- WHGYBXFWUBPSRW-FOUAGVGXSA-Nbeta-cyclodextrinChemical compoundOC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1COWHGYBXFWUBPSRW-FOUAGVGXSA-N0.000claimsdescription4
- 235000011175beta-cyclodextrineNutrition0.000claimsdescription4
- 229960004853betadexDrugs0.000claimsdescription4
- 238000003801millingMethods0.000claimsdescription4
- 238000001291vacuum dryingMethods0.000claimsdescription3
- 238000007605air dryingMethods0.000claimsdescription2
- 239000000243solutionSubstances0.000claimsdescription2
- 239000000084colloidal systemSubstances0.000abstractdescription4
- 230000006837decompressionEffects0.000abstract1
- 238000007865dilutingMethods0.000abstract1
- 238000000227grindingMethods0.000abstract1
- 238000002156mixingMethods0.000abstract1
- 238000002791soakingMethods0.000abstract1
- 238000001256steam distillationMethods0.000abstract1
- 238000005303weighingMethods0.000abstract1
- 150000001875compoundsChemical class0.000description9
- 238000003756stirringMethods0.000description5
- 235000019504cigarettesNutrition0.000description4
- 238000004519manufacturing processMethods0.000description4
- 241000208292SolanaceaeSpecies0.000description3
- 239000008367deionised waterSubstances0.000description3
- 229910021641deionized waterInorganic materials0.000description3
- 241000196324EmbryophytaSpecies0.000description2
- 239000003205fragranceSubstances0.000description2
- UGFAIRIUMAVXCW-UHFFFAOYSA-NCarbon monoxideChemical compound[O+]#[C-]UGFAIRIUMAVXCW-UHFFFAOYSA-N0.000description1
- 235000003255Carthamus tinctoriusNutrition0.000description1
- 244000020518Carthamus tinctoriusSpecies0.000description1
- 240000007472Leucaena leucocephalaSpecies0.000description1
- 235000010643Leucaena leucocephalaNutrition0.000description1
- 229950005162benexateDrugs0.000description1
- IAXUQWSLRKIRFR-SAABIXHNSA-Nchembl2104696Chemical compoundC1C[C@@H](CNC(=N)N)CC[C@@H]1C(=O)OC1=CC=CC=C1C(=O)OCC1=CC=CC=C1IAXUQWSLRKIRFR-SAABIXHNSA-N0.000description1
- 235000009508confectioneryNutrition0.000description1
- 239000003546flue gasSubstances0.000description1
- 239000000178monomerSubstances0.000description1
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
Description
Technical field
The present invention relates to a preparation method who grows tobacco colored volatile matter extracting method and microcapsule thereof, belong to light industry processing technique field.
Background technology
Tobacco is Solanaceae annual herb plant, and the nearly kind more than 60 of Nicotiana, but really for the manufacture of cigarette and pipe tobacco, substantially only have safflower tobacco also has small part in addition with Folium Nicotianae rusticae, and other kinds are seldom used.Tobacco is the plant of Solanaceae (nightshade family) that one belongs to Nicotiana (Nicotiana), at present, people are separated out in tobacco and flue gas and are had hundreds of aroma components by advanced analytical instrument, can adopt the technology such as extraction and synthetic to produce needed monomer essence.The essence extracting from tobacco is used further to production of cigarettes, can improves better the fragrance value of cigarette product.Tobacco extract can extract from the tobacco of any type, and wherein tobacco flower concrete has gentle tobacco flowery odour, like fresh and sweet as Acacia, can be directly used in cigarette and perfuming tobacco thin sheet.But the extractive technique to tobacco in existing technology and apply less.Patent of invention (201310178550.8) " is utilized supercritical CO2the method of tobacco extrait is prepared in extraction " disclose one and utilized supercritical CO2abstraction technique is prepared the method for tobacco extrait, and after tobacco extrait extracts, fragrance is difficult to ensure, application is restricted.
Summary of the invention
The object of the present invention is to provide a preparation method who grows tobacco colored volatile matter extracting method and microcapsule thereof.Tobacco volatile matter extracting method of the present invention is to utilize wet distillation to extract tobacco volatile matter, by tobacco is soaked, add salt, improve volatile matter extraction yield, then it is carried out to microcapsule preparation with colloid milling, use colloidal mill to prepare the microcapsule yield of Benexate Hydrochloride high, the inclusion time is short, temperature is low, output is large, take up room little, processing condition are easy to control, are applicable to enterprise's suitability for industrialized production.
Object of the present invention is achieved by the following technical programs:
Except as otherwise noted, percentage ratio of the present invention is weight percentage.
The one colored volatile matter extracting method that grows tobacco, is by tobacco chopping, weighs, and adds a certain amount of saliferous distilled water solution, soaks certain hour, and wet distillation is extracted, and collects cut, obtains tobacco volatile matter.
One preparation method who grows tobacco colored volatile matter microcapsule, gets tobacco volatile matter, adds equivalent 95% alcohol dilution, adds a certain amount of cyclodextrin and distilled water to mix, and grinds to form mashed prod with colloidal mill; By mashed prod decompress filter, with absolute ethanol washing, after suction filtration be deposited in 40-60 ℃ dry.
Tobacco volatile matter extracting method of the present invention, the mass ratio of described tobacco and saliferous distilled water is 1:10-15, the concentration of salt by weight percentage ratio is 1-10%.
The extracting method of tobacco volatile matter of the present invention, wet distillation extraction time is 2-4h.
The extracting method of tobacco volatile matter of the present invention, described salt is NaCl, Na2sO4, NaNO3one, soak time is 12-24h.
The preparation method of tobacco volatile matter microcapsule of the present invention, the mass ratio 1:3-6 of tobacco volatilization extract and cyclodextrin.
The preparation method of tobacco volatile matter microcapsule of the present invention, the mass ratio of cyclodextrin and distilled water is 1:3-6.
The preparation method of tobacco volatile matter microcapsule of the present invention, milling time is 10-20min.
The preparation method of tobacco volatile matter microcapsule of the present invention, cyclodextrin is the one of beta-cyclodextrin, hydroxypropyl-belta-cyclodextrin.
The preparation method of tobacco volatile matter microcapsule of the present invention, drying mode is the one of vacuum-drying and forced air drying method.
With respect to prior art, the present invention has following remarkable advantage:
1, the present invention utilizes wet distillation to extract tobacco volatile component, by tobacco is soaked, adds salt, improves volatile matter extraction yield.
2, with colloid milling, tobacco volatile matter is carried out to micro-capsule embedding, yield is high, and the inclusion time is short, temperature is low, output is large, takes up room little, and processing condition are easy to control, is applicable to enterprise's suitability for industrialized production.
3, the tobacco volatile matter microcapsule of preparation, are easy to use in tobacco processing.
Embodiment
Below in conjunction with embodiment, the present invention is further described, but protection scope of the present invention is not limited to this.
embodiment 1
(1) tobacco volatile matter extracts: claim chopping rear fresh tobacco 100g, add deionized water 1000g, NaCl 30g, stir, soak 18h, wet distillation is extracted 2 h, collects cut, obtains tobacco volatile matter 0.269g.
(2) tobacco volatile matter microcapsule preparation: get 100g tobacco volatilization extract, add 100g 95% alcohol dilution, add 300g beta-cyclodextrin and 900g distilled water to mix, grind 15min with colloidal mill, decompress filter, uses absolute ethanol washing inclusion compound, dry in 40 ℃ of air dry ovens, obtain 300g inclusion compound, i.e. tobacco volatile matter microcapsule, inclusion compound yield is 75%.
embodiment 2
(1) tobacco volatile matter extracts: claim chopping rear fresh tobacco 100g, add deionized water 1200g, Na2sO415g, stirs, and soaks 24h, stirs, and wet distillation is extracted 3h, collects cut, obtains tobacco volatile matter 0.260g.
(2) tobacco volatile matter microcapsule preparation: get 100g tobacco volatilization extract, add 100g95% alcohol dilution, add 400g hydroxypropyl-belta-cyclodextrin and 2000g distilled water to mix, grind 20min with colloidal mill, decompress filter, uses absolute ethanol washing inclusion compound, dry in 50 ℃ of air dry ovens, obtain 355g inclusion compound, i.e. tobacco volatile matter microcapsule, inclusion compound yield is 71%.
embodiment 3
(1) tobacco volatile matter extracts: claim chopping rear fresh tobacco 100g, add deionized water 1500g, NaNO350g, stirs, and soaks 12h, stirs, and wet distillation is extracted 4h, collects cut, obtains tobacco volatile matter 0.263g.
(2) tobacco volatile matter microcapsule preparation: get 100g tobacco volatilization extract, add 100g95% alcohol dilution, add 600g beta-cyclodextrin and 3600g distilled water to mix, grind 10min with colloidal mill, decompress filter, uses absolute ethanol washing inclusion compound, dry in 50 ℃ of vacuum drying ovens, obtain 490g inclusion compound, i.e. tobacco volatile matter microcapsule, inclusion compound yield is 70%.
Carry out extraction yield and inclusion rate contrast with embodiment 1, see the following form.
Different Extraction Method and inclusion method contrast table
Claims (10)
1. the colored volatile matter extracting method that grows tobacco, is characterized in that: by tobacco chopping, weigh, add a certain amount of saliferous distilled water solution, soak certain hour, wet distillation is extracted, and collects cut, obtains tobacco volatile matter.
2. a preparation method who grows tobacco colored volatile matter microcapsule, is characterized in that comprising: get tobacco volatile matter, add equivalent 95% alcohol dilution, add a certain amount of cyclodextrin and distilled water to mix, grind to form mashed prod with colloidal mill; By mashed prod decompress filter, with absolute ethanol washing, after suction filtration be deposited in 40-60 ℃ dry.
3. tobacco volatile matter extracting method according to claim 1, is characterized in that: the mass ratio of described tobacco and saliferous distilled water is 1:10-15, the concentration of salt by weight percentage ratio is 1-10%.
4. the extracting method of tobacco volatile matter according to claim 1, is characterized in that: wet distillation extraction time is 2-4h.
5. the extracting method of tobacco volatile matter according to claim 1, is characterized in that: described salt is NaCl, Na2sO4, NaNO3one, soak time is 12-24h.
6. the preparation method of tobacco volatile matter microcapsule according to claim 2, is characterized in that: the mass ratio 1:3-6 of tobacco volatilization extract and cyclodextrin.
7. the preparation method of tobacco volatile matter microcapsule according to claim 2, is characterized in that: the mass ratio of cyclodextrin and distilled water is 1:3-6.
8. the preparation method of tobacco volatile matter microcapsule according to claim 2, is characterized in that: milling time is 10-20min.
9. the preparation method of tobacco volatile matter microcapsule according to claim 2, is characterized in that: cyclodextrin is the one of beta-cyclodextrin, hydroxypropyl-belta-cyclodextrin.
10. the preparation method of tobacco volatile matter microcapsule according to claim 2, is characterized in that: drying mode is the one of vacuum-drying and forced air drying method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410055423.3ACN103789090A (en) | 2014-02-19 | 2014-02-19 | Flowering tobacco volatile extraction method and preparation method for microcapsules of flowering tobacco |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410055423.3ACN103789090A (en) | 2014-02-19 | 2014-02-19 | Flowering tobacco volatile extraction method and preparation method for microcapsules of flowering tobacco |
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| CN103789090Atrue CN103789090A (en) | 2014-05-14 |
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| CN201410055423.3APendingCN103789090A (en) | 2014-02-19 | 2014-02-19 | Flowering tobacco volatile extraction method and preparation method for microcapsules of flowering tobacco |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104824837A (en)* | 2015-03-31 | 2015-08-12 | 川渝中烟工业有限责任公司 | Method for applying tobacco flavor extracted from tobacco flowers to suns |
| CN105199852A (en)* | 2015-09-29 | 2015-12-30 | 广西中烟工业有限责任公司 | Process using Chongqing Fengjie Yunyan 87 flower buds as raw materials to extract essential oil and application of essential oil |
| CN105886121A (en)* | 2014-11-14 | 2016-08-24 | 上海霖成生物科技有限公司 | Preparation method of high-quality citrus essential oil |
| CN107446693A (en)* | 2017-09-12 | 2017-12-08 | 中国热带农业科学院农产品加工研究所 | A kind of method of ultrasonic wave vapour-liquid coexistence state ethanol fluid oil and grease extracting |
| CN108424813A (en)* | 2018-03-14 | 2018-08-21 | 河南科技大学 | A kind of fresh flower aromatic water, compound salt and compound salt solution for extracting fresh flower aromatic water |
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| CN1032953A (en)* | 1987-10-31 | 1989-05-17 | 中国科学院广州化学研究所 | The straight run distillation cinnamon leaf extracts oil of bay |
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| CN103146484A (en)* | 2013-02-28 | 2013-06-12 | 青海红璟天生物科技有限公司 | Method for fast preparing betadex embedded object of rhododendron anthopogonoide volatile oil |
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- 2014
- 2014-02-19CNCN201410055423.3Apatent/CN103789090A/enactivePending
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Non-Patent Citations (1)
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| 刘煜宇，等: "响应面法优化烟草花超临界二氧化碳萃取工艺及香气分析", 《烟草科技》, no. 6, 31 December 2013 (2013-12-31), pages 45 - 49* |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105886121A (en)* | 2014-11-14 | 2016-08-24 | 上海霖成生物科技有限公司 | Preparation method of high-quality citrus essential oil |
| CN104824837A (en)* | 2015-03-31 | 2015-08-12 | 川渝中烟工业有限责任公司 | Method for applying tobacco flavor extracted from tobacco flowers to suns |
| CN105199852A (en)* | 2015-09-29 | 2015-12-30 | 广西中烟工业有限责任公司 | Process using Chongqing Fengjie Yunyan 87 flower buds as raw materials to extract essential oil and application of essential oil |
| CN107446693A (en)* | 2017-09-12 | 2017-12-08 | 中国热带农业科学院农产品加工研究所 | A kind of method of ultrasonic wave vapour-liquid coexistence state ethanol fluid oil and grease extracting |
| CN108424813A (en)* | 2018-03-14 | 2018-08-21 | 河南科技大学 | A kind of fresh flower aromatic water, compound salt and compound salt solution for extracting fresh flower aromatic water |
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