技术领域technical field
本发明属于烟草加工制备技术领域，具体涉及一种加热效率较高的加热非燃烧型卷烟烟块的制备方法。The invention belongs to the technical field of tobacco processing and preparation, and in particular relates to a method for preparing a heat-not-burn cigarette block with high heating efficiency.
背景技术Background technique
传统卷烟由于烟草燃烧和热裂解而产生的多种有害成分，而加热非燃烧型卷烟产生的烟气与传统卷烟较为接近，而且测流烟气和部分有害成分明显减少，为此国内外许多烟草企业、研究院所不断加大研发力度，致力于加热非燃烧型卷烟的研究及开发。Traditional cigarettes produce a variety of harmful components due to tobacco combustion and pyrolysis, while the smoke produced by heat-not-burn cigarettes is closer to that of traditional cigarettes, and the measured flow smoke and some harmful components are significantly reduced. For this reason, many tobacco products at home and abroad Enterprises and research institutes continue to increase research and development efforts, and are committed to the research and development of heat-not-burn cigarettes.
目前，加热非燃烧型卷烟主要有电加热卷烟、碳质加热卷烟和化学加热卷烟三种类型：（1）电加热卷烟。菲利普莫里斯生产公司先后推出的“Accord”、“Heatbar”、“EHP”三款电加热卷烟产品，均采用电加热器对卷烟制品进行加热的方式产生烟气，卷烟制品具有与传统卷烟类似的结构及外形；R.J.雷诺兹烟草公司的发明专利《含有烟草的吸烟物品》介绍了一种电加热卷烟，采用电阻加热元件对烟草进行加热而产生烟气，其中烟草通常为切丝填料；湖北中烟工业有限公司的实用新型专利《电加热式卷烟》公开了一种电加热卷烟，该卷烟通过多孔加热板和外加热壁对烟片进行加热发出烟气，但烟片的配方及其制作方法还未见公开。（2）碳质加热卷烟。R.J.雷诺兹烟草公司先后以商标Premier和Eclipse来销售该类型的卷烟，其中Eclipse卷烟采用碳质热源燃烧释放的热量加热膨胀烟草填料而产生烟气供人们抽吸，膨胀烟草填料为再造烟叶；日本烟草产业株式会社的发明专利《非燃烧型吸烟物品用碳质热源组成物和非燃烧型吸烟物品》公开了一种碳质加热卷烟，该卷烟也是采用碳质热源燃烧释放的热量加热烟片或烟丝。（3）化学加热卷烟。奥利格股份公司公开的发明专利《无烟香烟》属于化学加热卷烟，该卷烟采用可结晶物质结晶释放热量的原理来加热尼古丁储器释放出挥发性成分供消费者抽吸；斯泰格莫德有限公司公开了一项发明专利《吸烟制品》，该吸烟制品通过某些化合物的反应来提供热量加热烟草产生烟气，其中该烟草可为以许多不同方式加工的烟草。At present, there are three types of heat-not-burn cigarettes: electric heating cigarettes, carbonaceous heating cigarettes and chemical heating cigarettes: (1) electric heating cigarettes. Philip Morris Production Company has successively launched three electric heating cigarette products, "Accord", "Heatbar", and "EHP", all of which use electric heaters to heat cigarette products to generate smoke. Structure and shape; R.J. Reynolds Tobacco Company’s invention patent "Smoking Articles Containing Tobacco" introduces an electrically heated cigarette, which uses resistance heating elements to heat tobacco to generate smoke, in which tobacco is usually shredded filler; Hubei Zhong The utility model patent "Electric Heating Cigarette" of Tobacco Industry Co., Ltd. discloses an electric heating cigarette, which uses a porous heating plate and an external heating wall to heat the tobacco sheet to emit smoke, but the formula and production method of the tobacco sheet Not seen yet. (2) Carbonaceous heating cigarettes. R.J. Reynolds Tobacco Company successively sells this type of cigarettes under the trademarks Premier and Eclipse. Among them, Eclipse cigarettes use the heat released by the combustion of carbonaceous heat sources to heat and expand the tobacco filler to generate smoke for people to smoke. The expanded tobacco filler is reconstituted tobacco leaves; Japan The invention patent of Tobacco Industry Co., Ltd. "Carbonaceous Heat Source Composition for Non-combustible Smoking Articles and Non-combustible Smoking Articles" discloses a carbonaceous heating cigarette. cut tobacco. (3) Chemically heated cigarettes. The invention patent "Smokeless Cigarette" disclosed by Olig AG belongs to chemically heated cigarettes, which use the principle of crystallization of crystallized substances to release heat to heat the nicotine reservoir and release volatile components for consumers to smoke; Stegmore Germany Co., Ltd. has disclosed an invention patent "Smoking Article", which provides heat through the reaction of certain compounds to heat tobacco to produce smoke, wherein the tobacco can be processed in many different ways.
由上所述可知，国内外对各类加热非燃烧型卷烟的热源进行了大量的研究开发，但可能处于技术保密因素，很少提及加热非燃烧型卷烟的烟料制备方法。因此提供一种加热效率较高的烟块的制备方法，对于加热非燃烧型卷烟领域具有重要的意义。It can be seen from the above that a lot of research and development has been carried out on heat sources of various heat-not-burn cigarettes at home and abroad, but it may be due to technical confidentiality factors, and the smoke material preparation method of heat-not-burn cigarettes is rarely mentioned. Therefore, it is of great significance to provide a method for preparing a cigarette block with high heating efficiency for the field of heat-not-burn cigarettes.
发明内容Contents of the invention
本发明的目的在于针对现有技术的不足，提供一种加热非燃烧型卷烟烟块的制备方法，不仅填补了加热非燃烧型卷烟烟块制备领域的空白，而且烟块的加热效率有效提高，抽吸次数也明显增加。The object of the present invention is to address the deficiencies in the prior art, to provide a method for preparing a heat-not-burn cigarette block, which not only fills the gap in the field of heat-not-burn cigarette block preparation, but also effectively improves the heating efficiency of the cigarette block, The number of puffs also increased significantly.
本发明的目的通过以下技术方案予以实现。The purpose of the present invention is achieved through the following technical solutions.
*除非另有说明，本发明所采用的百分数均为质量百分数。* Unless otherwise specified, the percentages used in the present invention are all mass percentages.
一种加热非燃烧型卷烟烟块的制备方法，其特征在于：包括以下步骤：A method for preparing a heat-not-burn cigarette block, characterized in that it comprises the following steps:
（1）烟叶末的制备：取水分控制在6～13%的烟叶，用粉碎机粉碎后过40目筛得烟叶末，备用；(1) Preparation of tobacco powder: Take tobacco leaves with a water content of 6-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco powder for later use;
（2）烟梗末的制备：取水分控制在5～13%的烟梗，用粉碎机粉碎后过40目筛得烟梗末，备用；(2) Preparation of tobacco stem powder: Take tobacco stems with a moisture content of 5-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco stem powder for later use;
（3）烟用香料的配制：取罗汉果提取物3%、可可壳提取物4%、刺槐豆提取物3%、葡萄籽提取物5%、杏子提取物3%、苜蓿提取物5%、僧帽花提取物5%、柠檬油6%、红枣提取物5%、缬草根提取物3%、扁豆叶提取物4%、樱桃提取物8%、苹果提取物6%、去离子水15%和丙二醇25%，将上述组分混合后，于50～60℃条件下搅拌40分钟即得烟用香料，备用；(3) Preparation of spices for tobacco: 3% Luo Han Guo extract, 4% cocoa shell extract, 3% locust bean extract, 5% grape seed extract, 3% apricot extract, 5% alfalfa extract, monk Cap Flower Extract 5%, Lemon Oil 6%, Jujube Extract 5%, Valerian Root Extract 3%, Lentil Leaf Extract 4%, Cherry Extract 8%, Apple Extract 6%, Deionized Water 15% and Propylene glycol 25%, after mixing the above components, stir at 50-60°C for 40 minutes to obtain tobacco flavor, set aside;
（4）烟用香精的配制：取香兰素0.2%，薄荷脑0.2%，香紫苏油0.1%，大茴香油10%EA0.4%，吐鲁浸膏0.1%，麦芽酚0.1%，云烟净油0.6%，芫荽籽油1%EA2.5%，丁香花蕾油0.1%，香叶油1%EA3.0%，桂叶油1%EA0.1%，玫瑰花油1%EA1.2%，2-乙酰基吡嗪1.2%，2,3，5-三甲基吡嗪0.6%，薰衣草油1%EA1.0%，独活酊3.2%，香荚兰豆酊5.0%，枣子酊8.0%，3-甲基戊酸0.04%，乙醇51.36%和丙二醇21.0%，将上述组分混合后，于室温下搅拌1小时即得烟用香精，备用；(4) Preparation of tobacco essence: Take 0.2% of vanillin, 0.2% of menthol, 0.1% of fennel oil, 10% of fennel oil, 0.4% of EA, 0.1% of Tulu extract, 0.1% of maltol, Yunyan Absolute Oil 0.6%, Coriander Seed Oil 1% EA 2.5%, Clove Bud Oil 0.1%, Geranium Leaf Oil 1% EA 3.0%, Gui Ye Oil 1% EA 0.1%, Rose Oil 1% EA 1.2 %, 2-acetylpyrazine 1.2%, 2,3,5-trimethylpyrazine 0.6%, lavender oil 1% EA1.0%, lovage tincture 3.2%, vanilla bean tincture 5.0%, jujube tincture 8.0 %, 0.04% of 3-methylpentanoic acid, 51.36% of ethanol and 21.0% of propylene glycol. After mixing the above components, stir at room temperature for 1 hour to obtain the essence for tobacco, and set aside;
（5）烟浆制备：量取50～70%的烟叶末、5～20%的烟梗末，3～7%的烟用香料、10～20%的去离子水、7～11%的藻酸盐以及1～2%的甘油，混合后于室温下搅拌30分钟，形成烟浆；(5) Preparation of tobacco pulp: Measure 50-70% tobacco leaf powder, 5-20% tobacco stem powder, 3-7% tobacco flavor, 10-20% deionized water, 7-11% algae salt and 1-2% glycerin, after mixing, stir at room temperature for 30 minutes to form a smoke slurry;
（6）卷烟烟块的制备：将步骤（5）制得的烟浆用模具成型，形成具有孔洞的圆柱状烟块，置于烘箱中在40℃条件下烘烤10小时后，量取重量等于烟块重量1～3%的烟用香精均匀喷洒于烟块表面，待烟用香精被烟块吸收后，将烟块置于温度为22℃、湿度为60%的恒温恒湿箱中平衡48小时即得加热非燃烧性卷烟烟块。(6) Preparation of cigarette block: shape the smoke slurry prepared in step (5) with a mold to form a cylindrical cigarette block with holes, place it in an oven and bake it at 40°C for 10 hours, then measure the weight Tobacco essence equal to 1-3% of the weight of the cigarette block is evenly sprayed on the surface of the cigarette block. After the tobacco essence is absorbed by the block, the block is placed in a constant temperature and humidity box with a temperature of 22°C and a humidity of 60%. The heated non-combustible cigarette block can be obtained within 48 hours.
其中，所述烟叶为烤烟烟叶、香料烟烟叶、晾晒烟烟叶、白肋烟烟叶中的至少一种。Wherein, the tobacco leaves are at least one of flue-cured tobacco leaves, oriental tobacco leaves, air-cured tobacco leaves, and Burley tobacco leaves.
其中，所述烟梗为烤烟烟梗、香料烟烟梗、晾晒烟烟梗、白肋烟烟梗中的至少一种。Wherein, the tobacco stems are at least one of flue-cured tobacco stems, oriental tobacco stems, air-cured tobacco stems, and Burley tobacco stems.
其中，所述圆柱状烟块的孔洞为圆形、正方形、菱形或三角形且数量为1～19个。Wherein, the holes of the cylindrical cigarette block are circular, square, rhombus or triangular and the number is 1-19.
其中，所述圆柱状烟块的直径为5.0～12.0mm，长度为1～20mm。Wherein, the diameter of the cylindrical cigarette block is 5.0-12.0 mm, and the length is 1-20 mm.
与现有技术相比，本发明具有如下有益效果：Compared with the prior art, the present invention has the following beneficial effects:
1、本发明填补了加热非燃烧型卷烟烟块制备领域的空白，扩展了烟草类型。1. The present invention fills in the gap in the field of preparation of heat-not-burn cigarette blocks and expands the types of tobacco.
2、本发明制得的加热非燃烧型卷烟烟块采用有孔设计，使得加热元件可伸入烟块的内部，对烟块进行由内而外的均匀加热，显著提高其加热效率。2. The heat-not-burn cigarette block produced by the present invention adopts a hole design, so that the heating element can extend into the inside of the block, and uniformly heat the block from the inside to the outside, significantly improving its heating efficiency.
3、本发明采用固体块状的设计，加热的物料量增加，添加一次烟块后，卷烟的抽吸次数较加热烟丝的卷烟明显增加。3. The present invention adopts a solid block design, and the amount of heated material is increased. After adding a block of tobacco, the number of puffs of the cigarette is significantly increased compared with that of a cigarette with heated shredded tobacco.
4、本发明所述烟块制备简便，且可实现规模化生产。4. The cigarette block of the present invention is easy to prepare and can realize large-scale production.
附图说明Description of drawings
图1为本发明加热非燃烧型卷烟烟块的横截面示意图。Fig. 1 is a schematic cross-sectional view of a heat-not-burn cigarette block of the present invention.
图中：1-圆形孔洞的烟块；2-正方形孔洞的烟块；3-菱形孔洞的烟块；4-三角形孔洞的烟块。In the figure: 1-a cigarette block with a circular hole; 2-a cigarette block with a square hole; 3-a cigarette block with a diamond-shaped hole; 4-a cigarette block with a triangular hole.
具体实施方式Detailed ways
下面结合附图及具体实施例对本发明加以说明，应当注意，具体实施例不以任何方式对本发明加以限制，依据本发明的教导所作的任何变更或替换，均属于本发明的保护范围。The present invention will be described below in conjunction with the accompanying drawings and specific embodiments. It should be noted that the specific embodiments do not limit the present invention in any way, and any changes or replacements made according to the teaching of the present invention belong to the protection scope of the present invention.
实施例1Example 1
本实施例中所述的加热非燃烧型卷烟烟块的制备方法，包括以下步骤：The preparation method of the heat-not-burn cigarette block described in this embodiment comprises the following steps:
（1）烟叶末的制备：取水分控制在6～13%的烤烟烟叶，用粉碎机粉碎后过40目筛得烟叶末，备用；(1) Preparation of tobacco leaf powder: take flue-cured tobacco leaves with a moisture content of 6-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco leaf powder for later use;
（2）烟梗末的制备：取水分控制在5～13%的烤烟烟梗，用粉碎机粉碎后过40目筛得烟梗末，备用；(2) Preparation of tobacco stem powder: Take flue-cured tobacco stems with a moisture content of 5-13%, pulverize them with a pulverizer, pass through a 40-mesh sieve to obtain tobacco stem powder, and set aside;
（3）烟用香料的配制：取罗汉果提取物3%、可可壳提取物4%、刺槐豆提取物3%、葡萄籽提取物5%、杏子提取物3%、苜蓿提取物5%、僧帽花提取物5%、柠檬油6%、红枣提取物5%、缬草根提取物3%、扁豆叶提取物4%、樱桃提取物8%、苹果提取物6%、去离子水15%和丙二醇25%，将上述组分混合后，于50～60℃条件下搅拌40分钟即得烟用香料，备用；(3) Preparation of spices for tobacco: 3% Luo Han Guo extract, 4% cocoa shell extract, 3% locust bean extract, 5% grape seed extract, 3% apricot extract, 5% alfalfa extract, monk Cap Flower Extract 5%, Lemon Oil 6%, Jujube Extract 5%, Valerian Root Extract 3%, Lentil Leaf Extract 4%, Cherry Extract 8%, Apple Extract 6%, Deionized Water 15% and Propylene glycol 25%, after mixing the above components, stir at 50-60°C for 40 minutes to obtain tobacco flavor, set aside;
（4）烟用香精的配制：取香兰素0.2%，薄荷脑0.2%，香紫苏油0.1%，大茴香油10%EA0.4%，吐鲁浸膏0.1%，麦芽酚0.1%，云烟净油0.6%，芫荽籽油1%EA2.5%，丁香花蕾油0.1%，香叶油1%EA3.0%，桂叶油1%EA0.1%，玫瑰花油1%EA1.2%，2-乙酰基吡嗪1.2%，2,3，5-三甲基吡嗪0.6%，薰衣草油1%EA1.0%，独活酊3.2%，香荚兰豆酊5.0%，枣子酊8.0%，3-甲基戊酸0.04%，乙醇51.36%和丙二醇21.0%，将上述组分混合后，于室温下搅拌1小时即得烟用香精，备用；(4) Preparation of tobacco essence: Take 0.2% of vanillin, 0.2% of menthol, 0.1% of fennel oil, 10% of fennel oil, 0.4% of EA, 0.1% of Tulu extract, 0.1% of maltol, Yunyan Absolute Oil 0.6%, Coriander Seed Oil 1% EA 2.5%, Clove Bud Oil 0.1%, Geranium Leaf Oil 1% EA 3.0%, Gui Ye Oil 1% EA 0.1%, Rose Oil 1% EA 1.2 %, 2-acetylpyrazine 1.2%, 2,3,5-trimethylpyrazine 0.6%, lavender oil 1% EA1.0%, lovage tincture 3.2%, vanilla bean tincture 5.0%, jujube tincture 8.0 %, 0.04% of 3-methylpentanoic acid, 51.36% of ethanol and 21.0% of propylene glycol. After mixing the above components, stir at room temperature for 1 hour to obtain the essence for tobacco, and set aside;
（5）烟浆制备：量取70%的烟叶末、6%的烟梗末，3%的烟用香料、10%的去离子水、10%的藻酸盐以及1%的甘油，混合后于室温下搅拌30分钟，形成烟浆；(5) Tobacco pulp preparation: Measure 70% tobacco leaf powder, 6% tobacco stem powder, 3% tobacco flavor, 10% deionized water, 10% alginate and 1% glycerin, mix them Stir at room temperature for 30 minutes to form a smoke slurry;
（6）卷烟烟块的制备：将步骤（5）制得的烟浆用模具成型，形成具有孔洞的圆柱状烟块，置于烘箱中在40℃条件下烘烤10小时后，量取重量等于烟块重量1%的烟用香精均匀喷洒于烟块表面，待烟用香精被烟块吸收后，将烟块置于温度为22℃、湿度为60%的恒温恒湿箱中平衡48小时即得加热非燃烧性卷烟烟块；其中，所述圆柱状烟块的孔洞为圆形、正方形、菱形或三角形且数量为9个；所述圆柱状烟块的直径为9.0mm，长度为10.0mm。(6) Preparation of cigarette block: shape the smoke slurry prepared in step (5) with a mold to form a cylindrical cigarette block with holes, place it in an oven and bake it at 40°C for 10 hours, then measure the weight Tobacco essence equal to 1% of the weight of the cigarette block is evenly sprayed on the surface of the cigarette block. After the tobacco essence is absorbed by the block, the block is placed in a constant temperature and humidity box with a temperature of 22°C and a humidity of 60% for 48 hours. Promptly get the heated non-combustible cigarette block; wherein, the holes of the cylindrical cigarette block are circular, square, rhombus or triangular and the number is 9; the diameter of the cylindrical cigarette block is 9.0 mm, and the length is 10.0 mm. mm.
实施例2Example 2
实施例中所述的加热非燃烧型卷烟烟块的制备方法，包括以下步骤：The preparation method of the heat-not-burn type cigarette block described in the embodiment comprises the following steps:
（1）烟叶末的制备：取水分控制在6～13%的烤烟烟叶，用粉碎机粉碎后过40目筛得烟叶末，备用；(1) Preparation of tobacco leaf powder: take flue-cured tobacco leaves with a moisture content of 6-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco leaf powder for later use;
（2）烟梗末的制备：取水分控制在5～13%的烤烟烟梗，用粉碎机粉碎后过40目筛得烟梗末，备用；(2) Preparation of tobacco stem powder: Take flue-cured tobacco stems with a moisture content of 5-13%, pulverize them with a pulverizer, pass through a 40-mesh sieve to obtain tobacco stem powder, and set aside;
（3）烟用香料的配制：取罗汉果提取物3%、可可壳提取物4%、刺槐豆提取物3%、葡萄籽提取物5%、杏子提取物3%、苜蓿提取物5%、僧帽花提取物5%、柠檬油6%、红枣提取物5%、缬草根提取物3%、扁豆叶提取物4%、樱桃提取物8%、苹果提取物6%、去离子水15%和丙二醇25%，将上述组分混合后，于50～60℃条件下搅拌40分钟即得烟用香料，备用；(3) Preparation of spices for tobacco: 3% Luo Han Guo extract, 4% cocoa shell extract, 3% locust bean extract, 5% grape seed extract, 3% apricot extract, 5% alfalfa extract, monk Cap Flower Extract 5%, Lemon Oil 6%, Jujube Extract 5%, Valerian Root Extract 3%, Lentil Leaf Extract 4%, Cherry Extract 8%, Apple Extract 6%, Deionized Water 15% and Propylene glycol 25%, after mixing the above components, stir at 50-60°C for 40 minutes to obtain tobacco flavor, set aside;
（4）烟用香精的配制：取香兰素0.2%，薄荷脑0.2%，香紫苏油0.1%，大茴香油10%EA0.4%，吐鲁浸膏0.1%，麦芽酚0.1%，云烟净油0.6%，芫荽籽油1%EA2.5%，丁香花蕾油0.1%，香叶油1%EA3.0%，桂叶油1%EA0.1%，玫瑰花油1%EA1.2%，2-乙酰基吡嗪1.2%，2,3，5-三甲基吡嗪0.6%，薰衣草油1%EA1.0%，独活酊3.2%，香荚兰豆酊5.0%，枣子酊8.0%，3-甲基戊酸0.04%，乙醇51.36%和丙二醇21.0%，将上述组分混合后，于室温下搅拌1小时即得烟用香精，备用；(4) Preparation of tobacco essence: Take 0.2% of vanillin, 0.2% of menthol, 0.1% of fennel oil, 10% of fennel oil, 0.4% of EA, 0.1% of Tulu extract, 0.1% of maltol, Yunyan Absolute Oil 0.6%, Coriander Seed Oil 1% EA 2.5%, Clove Bud Oil 0.1%, Geranium Leaf Oil 1% EA 3.0%, Gui Ye Oil 1% EA 0.1%, Rose Oil 1% EA 1.2 %, 2-acetylpyrazine 1.2%, 2,3,5-trimethylpyrazine 0.6%, lavender oil 1% EA1.0%, lovage tincture 3.2%, vanilla bean tincture 5.0%, jujube tincture 8.0 %, 0.04% of 3-methylpentanoic acid, 51.36% of ethanol and 21.0% of propylene glycol. After mixing the above components, stir at room temperature for 1 hour to obtain the essence for tobacco, and set aside;
（5）烟浆制备：量取50%的烟叶末、18%的烟梗末，5%的烟用香料、11.5%的去离子水、10%的藻酸盐以及1.5%的甘油，混合后于室温下搅拌30分钟，形成烟浆；(5) Preparation of tobacco pulp: Measure 50% tobacco leaf powder, 18% tobacco stem powder, 5% tobacco flavor, 11.5% deionized water, 10% alginate and 1.5% glycerin, mix them Stir at room temperature for 30 minutes to form a smoke slurry;
（6）卷烟烟块的制备：将步骤（5）制得的烟浆用模具成型，形成具有孔洞的圆柱状烟块，置于烘箱中在40℃条件下烘烤10小时后，量取重量等于烟块重量2%的烟用香精均匀喷洒于烟块表面，待烟用香精被烟块吸收后，将烟块置于温度为22℃、湿度为60%的恒温恒湿箱中平衡48小时即得加热非燃烧性卷烟烟块；其中，所述圆柱状烟块的孔洞为圆形、正方形、菱形或三角形且数量为9个；所述圆柱状烟块的直径为9.0mm，长度为10.0mm。(6) Preparation of cigarette block: shape the smoke slurry prepared in step (5) with a mold to form a cylindrical cigarette block with holes, place it in an oven and bake it at 40°C for 10 hours, then measure the weight Tobacco essence equal to 2% of the weight of the cigarette block is evenly sprayed on the surface of the cigarette block. After the tobacco essence is absorbed by the block, the block is placed in a constant temperature and humidity box with a temperature of 22°C and a humidity of 60% for 48 hours. Promptly get the heated non-combustible cigarette block; wherein, the holes of the cylindrical cigarette block are circular, square, rhombus or triangular and the number is 9; the diameter of the cylindrical cigarette block is 9.0 mm, and the length is 10.0 mm. mm.
实施例3Example 3
实施例中所述的加热非燃烧型卷烟烟块的制备方法，包括以下步骤：The preparation method of the heat-not-burn type cigarette block described in the embodiment comprises the following steps:
（1）烟叶末的制备：取水分控制在6～13%的烤烟烟叶，用粉碎机粉碎后过40目筛得烟叶末，备用；(1) Preparation of tobacco leaf powder: take flue-cured tobacco leaves with a moisture content of 6-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco leaf powder for later use;
（2）烟梗末的制备：取水分控制在5～13%的烤烟烟梗，用粉碎机粉碎后过40目筛得烟梗末，备用；(2) Preparation of tobacco stem powder: Take flue-cured tobacco stems with a moisture content of 5-13%, pulverize them with a pulverizer, pass through a 40-mesh sieve to obtain tobacco stem powder, and set aside;
（3）烟用香料的配制：取罗汉果提取物3%、可可壳提取物4%、刺槐豆提取物3%、葡萄籽提取物5%、杏子提取物3%、苜蓿提取物5%、僧帽花提取物5%、柠檬油6%、红枣提取物5%、缬草根提取物3%、扁豆叶提取物4%、樱桃提取物8%、苹果提取物6%、去离子水15%和丙二醇25%，将上述组分混合后，于50～60℃条件下搅拌40分钟即得烟用香料，备用；(3) Preparation of spices for tobacco: 3% Luo Han Guo extract, 4% cocoa shell extract, 3% locust bean extract, 5% grape seed extract, 3% apricot extract, 5% alfalfa extract, monk Cap Flower Extract 5%, Lemon Oil 6%, Jujube Extract 5%, Valerian Root Extract 3%, Lentil Leaf Extract 4%, Cherry Extract 8%, Apple Extract 6%, Deionized Water 15% and Propylene glycol 25%, after mixing the above components, stir at 50-60°C for 40 minutes to obtain tobacco flavor, set aside;
（4）烟用香精的配制：取香兰素0.2%，薄荷脑0.2%，香紫苏油0.1%，大茴香油10%EA0.4%，吐鲁浸膏0.1%，麦芽酚0.1%，云烟净油0.6%，芫荽籽油1%EA2.5%，丁香花蕾油0.1%，香叶油1%EA3.0%，桂叶油1%EA0.1%，玫瑰花油1%EA1.2%，2-乙酰基吡嗪1.2%，2,3，5-三甲基吡嗪0.6%，薰衣草油1%EA1.0%，独活酊3.2%，香荚兰豆酊5.0%，枣子酊8.0%，3-甲基戊酸0.04%，乙醇51.36%和丙二醇21.0%，将上述组分混合后，于室温下搅拌1小时即得烟用香精，备用；(4) Preparation of tobacco essence: Take 0.2% of vanillin, 0.2% of menthol, 0.1% of fennel oil, 10% of fennel oil, 0.4% of EA, 0.1% of Tulu extract, 0.1% of maltol, Yunyan Absolute Oil 0.6%, Coriander Seed Oil 1% EA 2.5%, Clove Bud Oil 0.1%, Geranium Leaf Oil 1% EA 3.0%, Gui Ye Oil 1% EA 0.1%, Rose Oil 1% EA 1.2 %, 2-acetylpyrazine 1.2%, 2,3,5-trimethylpyrazine 0.6%, lavender oil 1% EA1.0%, lovage tincture 3.2%, vanilla bean tincture 5.0%, jujube tincture 8.0 %, 0.04% of 3-methylpentanoic acid, 51.36% of ethanol and 21.0% of propylene glycol. After mixing the above components, stir at room temperature for 1 hour to obtain the essence for tobacco, and set aside;
（5）烟浆制备：量取50%的烟叶末、18%的烟梗末，7%的烟用香料、13%的去离子水、10%的藻酸盐以及2%的甘油，混合后于室温下搅拌30分钟，形成烟浆；(5) Preparation of tobacco pulp: Measure 50% tobacco leaf powder, 18% tobacco stem powder, 7% tobacco flavor, 13% deionized water, 10% alginate and 2% glycerin, mix them Stir at room temperature for 30 minutes to form a smoke slurry;
（6）卷烟烟块的制备：将步骤（5）制得的烟浆用模具成型，形成具有孔洞的圆柱状烟块，置于烘箱中在40℃条件下烘烤10小时后，量取重量等于烟块重量3%的烟用香精均匀喷洒于烟块表面，待烟用香精被烟块吸收后，将烟块置于温度为22℃、湿度为60%的恒温恒湿箱中平衡48小时即得加热非燃烧性卷烟烟块；其中，所述圆柱状烟块的孔洞为圆形、正方形、菱形或三角形且数量为9个；所述圆柱状烟块的直径为9.0mm，长度为10.0mm。(6) Preparation of cigarette block: shape the smoke slurry prepared in step (5) with a mold to form a cylindrical cigarette block with holes, place it in an oven and bake it at 40°C for 10 hours, then measure the weight Tobacco essence equal to 3% of the weight of the cigarette block is evenly sprayed on the surface of the cigarette block. After the tobacco essence is absorbed by the block, the block is placed in a constant temperature and humidity box with a temperature of 22°C and a humidity of 60% for 48 hours. Promptly get the heated non-combustible cigarette block; wherein, the holes of the cylindrical cigarette block are circular, square, rhombus or triangular and the number is 9; the diameter of the cylindrical cigarette block is 9.0 mm, and the length is 10.0 mm. mm.
实施例4Example 4
实施例中所述的加热非燃烧型卷烟烟块的制备方法，包括以下步骤：The preparation method of the heat-not-burn type cigarette block described in the embodiment comprises the following steps:
（1）烟叶末的制备：取水分控制在6～13%的烤烟烟叶，用粉碎机粉碎后过40目筛得烟叶末，备用；(1) Preparation of tobacco leaf powder: take flue-cured tobacco leaves with a moisture content of 6-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco leaf powder for later use;
（2）烟梗末的制备：取水分控制在5～13%的烤烟烟梗，用粉碎机粉碎后过40目筛得烟梗末，备用；(2) Preparation of tobacco stem powder: Take flue-cured tobacco stems with a moisture content of 5-13%, pulverize them with a pulverizer, pass through a 40-mesh sieve to obtain tobacco stem powder, and set aside;
（3）烟用香料的配制：取罗汉果提取物3%、可可壳提取物4%、刺槐豆提取物3%、葡萄籽提取物5%、杏子提取物3%、苜蓿提取物5%、僧帽花提取物5%、柠檬油6%、红枣提取物5%、缬草根提取物3%、扁豆叶提取物4%、樱桃提取物8%、苹果提取物6%、去离子水15%和丙二醇25%，将上述组分混合后，于50～60℃条件下搅拌40分钟即得烟用香料，备用；(3) Preparation of spices for tobacco: 3% Luo Han Guo extract, 4% cocoa shell extract, 3% locust bean extract, 5% grape seed extract, 3% apricot extract, 5% alfalfa extract, monk Cap Flower Extract 5%, Lemon Oil 6%, Jujube Extract 5%, Valerian Root Extract 3%, Lentil Leaf Extract 4%, Cherry Extract 8%, Apple Extract 6%, Deionized Water 15% and Propylene glycol 25%, after mixing the above components, stir at 50-60°C for 40 minutes to obtain tobacco flavor, set aside;
（4）烟用香精的配制：取香兰素0.2%，薄荷脑0.2%，香紫苏油0.1%，大茴香油10%EA0.4%，吐鲁浸膏0.1%，麦芽酚0.1%，云烟净油0.6%，芫荽籽油1%EA2.5%，丁香花蕾油0.1%，香叶油1%EA3.0%，桂叶油1%EA0.1%，玫瑰花油1%EA1.2%，2-乙酰基吡嗪1.2%，2,3，5-三甲基吡嗪0.6%，薰衣草油1%EA1.0%，独活酊3.2%，香荚兰豆酊5.0%，枣子酊8.0%，3-甲基戊酸0.04%，乙醇51.36%和丙二醇21.0%，将上述组分混合后，于室温下搅拌1小时即得烟用香精，备用；(4) Preparation of tobacco essence: Take 0.2% of vanillin, 0.2% of menthol, 0.1% of fennel oil, 10% of fennel oil, 0.4% of EA, 0.1% of Tulu extract, 0.1% of maltol, Yunyan Absolute Oil 0.6%, Coriander Seed Oil 1% EA 2.5%, Clove Bud Oil 0.1%, Geranium Leaf Oil 1% EA 3.0%, Gui Ye Oil 1% EA 0.1%, Rose Oil 1% EA 1.2 %, 2-acetylpyrazine 1.2%, 2,3,5-trimethylpyrazine 0.6%, lavender oil 1% EA1.0%, lovage tincture 3.2%, vanilla bean tincture 5.0%, jujube tincture 8.0 %, 0.04% of 3-methylpentanoic acid, 51.36% of ethanol and 21.0% of propylene glycol. After mixing the above components, stir at room temperature for 1 hour to obtain the essence for tobacco, and set aside;
（5）烟浆制备：量取60%的烟叶末、5%的烟梗末，5%的烟用香料、10%的去离子水、7%的藻酸盐以及1%的甘油，混合后于室温下搅拌30分钟，形成烟浆；(5) Preparation of tobacco pulp: Measure 60% of tobacco leaf powder, 5% of tobacco stem powder, 5% of tobacco flavor, 10% of deionized water, 7% of alginate and 1% of glycerin, mix them Stir at room temperature for 30 minutes to form a smoke slurry;
（6）卷烟烟块的制备：将步骤（5）制得的烟浆用模具成型，形成具有孔洞的圆柱状烟块，置于烘箱中在40℃条件下烘烤10小时后，量取重量等于烟块重量1%的烟用香精均匀喷洒于烟块表面，待烟用香精被烟块吸收后，将烟块置于温度为22℃、湿度为60%的恒温恒湿箱中平衡48小时即得加热非燃烧性卷烟烟块；其中，所述圆柱状烟块的孔洞为圆形、正方形、菱形或三角形且数量为1个；所述圆柱状烟块的直径为5.0mm，长度为1.0mm。(6) Preparation of cigarette block: shape the smoke slurry prepared in step (5) with a mold to form a cylindrical cigarette block with holes, place it in an oven and bake it at 40°C for 10 hours, then measure the weight Tobacco essence equal to 1% of the weight of the cigarette block is evenly sprayed on the surface of the cigarette block. After the tobacco essence is absorbed by the block, the block is placed in a constant temperature and humidity box with a temperature of 22°C and a humidity of 60% for 48 hours. That is to obtain the heated non-combustible cigarette block; wherein, the hole of the cylindrical cigarette block is circular, square, rhombus or triangular and the number is 1; the diameter of the cylindrical cigarette block is 5.0 mm, and the length is 1.0 mm. mm.
实施例5Example 5
实施例中所述的加热非燃烧型卷烟烟块的制备方法，包括以下步骤：The preparation method of the heat-not-burn type cigarette block described in the embodiment comprises the following steps:
（1）烟叶末的制备：取水分控制在6～13%的烤烟烟叶，用粉碎机粉碎后过40目筛得烟叶末，备用；(1) Preparation of tobacco leaf powder: take flue-cured tobacco leaves with a moisture content of 6-13%, pulverize them with a pulverizer, and pass through a 40-mesh sieve to obtain tobacco leaf powder for later use;
（2）烟梗末的制备：取水分控制在5～13%的烤烟烟梗，用粉碎机粉碎后过40目筛得烟梗末，备用；(2) Preparation of tobacco stem powder: Take flue-cured tobacco stems with a moisture content of 5-13%, pulverize them with a pulverizer, pass through a 40-mesh sieve to obtain tobacco stem powder, and set aside;
（3）烟用香料的配制：取罗汉果提取物3%、可可壳提取物4%、刺槐豆提取物3%、葡萄籽提取物5%、杏子提取物3%、苜蓿提取物5%、僧帽花提取物5%、柠檬油6%、红枣提取物5%、缬草根提取物3%、扁豆叶提取物4%、樱桃提取物8%、苹果提取物6%、去离子水15%和丙二醇25%，将上述组分混合后，于50～60℃条件下搅拌40分钟即得烟用香料，备用；(3) Preparation of spices for tobacco: 3% Luo Han Guo extract, 4% cocoa shell extract, 3% locust bean extract, 5% grape seed extract, 3% apricot extract, 5% alfalfa extract, monk Cap Flower Extract 5%, Lemon Oil 6%, Jujube Extract 5%, Valerian Root Extract 3%, Lentil Leaf Extract 4%, Cherry Extract 8%, Apple Extract 6%, Deionized Water 15% and Propylene glycol 25%, after mixing the above components, stir at 50-60°C for 40 minutes to obtain tobacco flavor, set aside;
（4）烟用香精的配制：取香兰素0.2%，薄荷脑0.2%，香紫苏油0.1%，大茴香油10%EA0.4%，吐鲁浸膏0.1%，麦芽酚0.1%，云烟净油0.6%，芫荽籽油1%EA2.5%，丁香花蕾油0.1%，香叶油1%EA3.0%，桂叶油1%EA0.1%，玫瑰花油1%EA1.2%，2-乙酰基吡嗪1.2%，2,3，5-三甲基吡嗪0.6%，薰衣草油1%EA1.0%，独活酊3.2%，香荚兰豆酊5.0%，枣子酊8.0%，3-甲基戊酸0.04%，乙醇51.36%和丙二醇21.0%，将上述组分混合后，于室温下搅拌1小时即得烟用香精，备用；(4) Preparation of tobacco essence: Take 0.2% of vanillin, 0.2% of menthol, 0.1% of fennel oil, 10% of fennel oil, 0.4% of EA, 0.1% of Tulu extract, 0.1% of maltol, Yunyan Absolute Oil 0.6%, Coriander Seed Oil 1% EA 2.5%, Clove Bud Oil 0.1%, Geranium Leaf Oil 1% EA 3.0%, Gui Ye Oil 1% EA 0.1%, Rose Oil 1% EA 1.2 %, 2-acetylpyrazine 1.2%, 2,3,5-trimethylpyrazine 0.6%, lavender oil 1% EA1.0%, lovage tincture 3.2%, vanilla bean tincture 5.0%, jujube tincture 8.0 %, 0.04% of 3-methylpentanoic acid, 51.36% of ethanol and 21.0% of propylene glycol. After mixing the above components, stir at room temperature for 1 hour to obtain the essence for tobacco, and set aside;
（5）烟浆制备：量取65%的烟叶末、20%的烟梗末，7%的烟用香料、20%的去离子水、11%的藻酸盐以及1.5%的甘油，混合后于室温下搅拌30分钟，形成烟浆；(5) Tobacco pulp preparation: Measure 65% tobacco leaf powder, 20% tobacco stem powder, 7% tobacco flavor, 20% deionized water, 11% alginate and 1.5% glycerin, mix them Stir at room temperature for 30 minutes to form a smoke slurry;
（6）卷烟烟块的制备：将步骤（5）制得的烟浆用模具成型，形成具有孔洞的圆柱状烟块，置于烘箱中在40℃条件下烘烤10小时后，量取重量等于烟块重量1%的烟用香精均匀喷洒于烟块表面，待烟用香精被烟块吸收后，将烟块置于温度为22℃、湿度为60%的恒温恒湿箱中平衡48小时即得加热非燃烧性卷烟烟块；其中，所述圆柱状烟块的孔洞为圆形、正方形、菱形或三角形且数量为19个；所述圆柱状烟块的直径为12.0mm，长度为20.0mm。(6) Preparation of cigarette block: shape the smoke slurry prepared in step (5) with a mold to form a cylindrical cigarette block with holes, place it in an oven and bake it at 40°C for 10 hours, then measure the weight Tobacco essence equal to 1% of the weight of the cigarette block is evenly sprayed on the surface of the cigarette block. After the tobacco essence is absorbed by the block, the block is placed in a constant temperature and humidity box with a temperature of 22°C and a humidity of 60% for 48 hours. Promptly get heating non-combustible cigarette block; Wherein, the hole of described cylindrical cigarette block is circular, square, rhombus or triangle and quantity is 19; The diameter of described cylindrical cigarette block is 12.0mm, and length is 20.0mm. mm.
实施例6Example 6
重复实施例1，有以下不同点：所用烟叶为香料烟烟叶，所用烟梗为香料烟烟梗。Repeat Example 1, with the following differences: the tobacco leaves used are oriental tobacco leaves, and the tobacco stems used are oriental tobacco stems.
实施例7Example 7
重复实施例2，有以下不同点：所用烟叶为晾晒烟烟叶，所用烟梗为晾晒烟烟梗。Repeat Example 2, with the following differences: the tobacco leaves used are air-cured tobacco leaves, and the tobacco stems used are air-cured tobacco stems.
实施例8Example 8
重复实施例3，有以下不同点：所用烟叶为白肋烟烟叶，所用烟梗为白肋烟烟梗。Repeat Example 3, with the following differences: the tobacco leaves used are Burley tobacco leaves, and the tobacco stems used are Burley tobacco stems.
实施例9Example 9
重复实施例4，有以下不同点：所用烟叶为烤烟烟叶和香料烟烟叶，所用烟梗为烤烟烟梗和香料烟烟梗。Repeat Example 4, with the following differences: the tobacco leaves used are flue-cured tobacco leaves and oriental tobacco leaves, and the tobacco stems used are flue-cured tobacco stems and oriental tobacco stems.
实施例10Example 10
重复实施例4，有以下不同点：所用烟叶为烤烟烟叶、香料烟烟叶、晾晒烟烟叶和白肋烟烟叶，所用烟梗为烤烟烟梗、香料烟烟梗、晾晒烟烟梗和白肋烟烟梗。Repeat Example 4, with the following differences: the tobacco leaves used are flue-cured tobacco leaves, oriental tobacco leaves, air-cured tobacco leaves and Burley tobacco leaves, and the tobacco stems used are flue-cured tobacco stems, oriental tobacco stems, air-cured tobacco stems and Burley tobacco Tobacco stems.
应用实施例1Application Example 1
将实施例1～3所制备得到的烟块分别安装在相同的电加热卷烟上，并进行抽吸口数、每口烟雾量的均一性以及感官质量评价，结果见下表：The cigarette blocks prepared in Examples 1-3 were installed on the same electric heating cigarettes respectively, and the number of puffs, the uniformity of the amount of smoke per puff and the sensory quality evaluation were carried out. The results are shown in the following table:
以上所述仅为本发明的较佳实施例而已，并不用以限制本发明，凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等，均应包含在本发明的保护范围之内。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. Any modifications, equivalent replacements and improvements made within the spirit and principles of the present invention should be included in the protection of the present invention. within range.
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410030011.4ACN103750535B (en) | 2014-01-22 | 2014-01-22 | Preparation method of heating non-combustion type cigarette block |
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410030011.4ACN103750535B (en) | 2014-01-22 | 2014-01-22 | Preparation method of heating non-combustion type cigarette block |
| Publication Number | Publication Date |
|---|---|
| CN103750535A CN103750535A (en) | 2014-04-30 |
| CN103750535Btrue CN103750535B (en) | 2015-12-02 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410030011.4AActiveCN103750535B (en) | 2014-01-22 | 2014-01-22 | Preparation method of heating non-combustion type cigarette block |
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