技术领域technical field
本发明涉及卷烟滤棒技术领域，更具体地说，涉及一种复合增香植物的三元烟草纤维纸质滤棒及其制备方法。The invention relates to the technical field of cigarette filter sticks, in particular to a three-element tobacco fiber paper filter stick compounded with flavoring plants and a preparation method thereof.
背景技术Background technique
卷烟烟气中包含有微粒，通常称之为焦油。焦油中含有大量的化学成分，有4000至5000种，都是烟草不完全燃烧的产物。除了焦油外，卷烟烟雾中还包含有其他物质，如“蒸汽”或“气体”相，也包括挥发性的烟草燃烧物质，如乙醛以及其它低分子重量成分。卷烟烟雾中的其他相，如“半挥发性”相，其中包括许多燃烧物质，与微粒和蒸汽相等同。Cigarette smoke contains particles, commonly known as tar. Tar contains a large number of chemical components, 4000 to 5000 kinds, all of which are products of incomplete combustion of tobacco. In addition to tar, cigarette smoke contains other substances, such as the "steam" or "gas" phase, which also includes volatile tobacco combustion substances such as acetaldehyde and other low molecular weight components. Other phases in cigarette smoke, such as the "semi-volatile" phase, which includes many combustion substances, are equivalent to particulate and vapor phases.
卷烟滤棒能够过滤烟雾成分。卷烟的滤棒是由滤芯和成型纸组成的。现有滤棒的滤芯一般都是采用醋酸纤维或聚丙烯纤维组成。由于这些含有纤维的滤芯直接与人体的嘴唇相接触，最近有媒体报道，纤维特别是聚丙烯纤维可能会随着卷烟的抽吸进入人体，并对人体健康造成损害。滤嘴是卷烟的重要组成部分，利用卷烟滤嘴里的吸附材料及其添加剂可以过滤掉烟支主流烟气里的有害物质。目前，滤嘴滤材主要有三种类型：醋酸纤维、聚丙烯纤维和纸。纸质滤嘴因对烟气截留效率较高，且较之丢弃的醋酸纤维滤嘴和聚丙烯纤维滤嘴更易降解而备受关注。Cigarette filter rods can filter smoke components. Cigarette filter rods are composed of filter elements and molding paper. The filter element of existing filter rod all is to adopt acetate fiber or polypropylene fiber to form generally. Because these fiber-containing filter elements are in direct contact with the lips of the human body, recently there have been media reports that fibers, especially polypropylene fibers, may enter the human body along with the smoking of cigarettes and cause damage to human health. The filter tip is an important part of the cigarette, and the harmful substances in the mainstream smoke of the cigarette can be filtered out by using the absorbent material and its additives in the cigarette filter tip. At present, there are three main types of filter media: acetate fiber, polypropylene fiber and paper. Paper filters have attracted much attention due to their higher smoke retention efficiency and easier degradation than discarded acetate and polypropylene filters.
目前现有技术中也有一些植物纤维烟用滤棒的报道，如（专利号200910185294）报道了一种植物纤维烟用滤棒及其制备方法。但该专利滤棒由稻草纤维、麦草纤维、烟草秸秆纤维和大豆秸秆纤维直接构成，主要是利用植物秸杆降低卷烟成本，减少使用后的滤嘴和丝束生产过程对环境的污染，此外并并不能提供更多符合卷烟滤棒要求的功能。At present, there are some reports of plant fiber tobacco filter sticks in the prior art, for example (Patent No. 200910185294) reports a plant fiber tobacco filter stick and its preparation method. However, the patented filter rod is directly composed of rice straw fiber, wheat straw fiber, tobacco straw fiber and soybean straw fiber. Can not provide more functions that meet the requirements of the cigarette filter rod.
由绉丝纸制成的卷烟过滤嘴首次在20世纪20年代引进欧洲卷烟市场，纸质的滤嘴比醋酸纤维有更强的去除焦油和尼古丁的能力，但消费者一直不能接受，直到20世纪50年代，随着醋酸纤维的开发，过滤嘴卷烟才开始得到消费者的广泛认可，主要原因是纸张有“纸张的味道”，消费者往往不喜欢这一点。而且纸张较软，在吸烟的过程中污染严重，因此不宜直接作为过滤嘴使用。目前，醋酸纤维制成的过滤嘴是被广泛应用的一种。随着消费者对于健康的不断追求，以醋酸纤维为主的经由化学物质制备得到的滤嘴因为非天然性特点逐渐受到抵触。但目前还没有找到完全替代醋酸纤维的新材料。Cigarette filters made of crepe paper were first introduced to the European cigarette market in the 1920s. Paper filters have a stronger ability to remove tar and nicotine than acetate fibers, but consumers have not accepted them until the 1950s. With the development of acetate in the 1990s, filter cigarettes only began to gain widespread acceptance among consumers, mainly because the paper had a "paper smell," which consumers often disliked. Moreover, the paper is relatively soft, and the pollution is serious during the smoking process, so it is not suitable to be directly used as a filter tip. At present, the filter tip made of acetate fiber is widely used. With the continuous pursuit of health by consumers, the filters made of cellulose acetate and prepared from chemical substances are gradually being resisted because of their unnatural characteristics. But there is no new material that can completely replace cellulose acetate.
现有技术采用干法纸作为制备卷烟滤嘴棒滤材的技术也得到了开发，大都采用木浆纤维为主要纤维材料，或辅以一定比例的复合纤维、热熔纤维或生态纤维以达到各自的目标。如中国专利（CN180167B）“干法纸卷烟滤棒及其制备方法”，其在木浆纤维中添加了5%～65%的热熔性皮芯纤维；再如中国专利申请（CN101171981A）“二元复合卷烟过滤嘴棒”采用膨化干法纸制备得到的材料作为靠近烟丝的一元滤嘴的滤芯，该材料由纯木浆或50%～95%木浆和5%～50%复合纤维直接组成；还有中国专利申请（CN101624756A）“生物降解型香烟过滤嘴用非织造布及其制备方法”采用了木浆纤维、高熔点聚乳酸纤维、低熔点聚乳酸纤维和水溶性胶。也有人直接将烟草纤维通过风机输送至成型工段铺网成型，在成型网带上形成蓬松均匀的纤维网，再经施胶、预热、辊压、固化和成型制成卷烟滤材纸，并在成型过程中添加天然药草废弃原料。这些干法纸用的纤维涉及了木浆纤维、复合纤维、热熔性皮芯纤维、聚乳酸纤维等纤维类型，这些纤维尽管可用于制作滤嘴的滤材，但过滤烟气的同时使得烟香损失较多，且带入一定的木质杂气，在抽吸时对卷烟吸味和吃味有一定的负面影响，不能保证卷烟品质，更重要的是这些现有材料的颜色和品质与天然烟草的感觉相差甚远，不能迎合卷烟消费者对天然烟草感觉的追求。The prior art adopts air-laid paper as the technology of preparing cigarette filter rod filter material and has also been developed, most of which adopt wood pulp fiber as the main fiber material, or supplemented by a certain proportion of composite fiber, hot-melt fiber or ecological fiber to achieve their respective The goal. Such as the Chinese patent (CN180167B) "dry paper cigarette filter rod and its preparation method", which adds 5% to 65% of heat-melting sheath-core fiber in the wood pulp fiber; another example of the Chinese patent application (CN101171981A) Elementary composite cigarette filter rod” uses the material prepared by puffed dry-laid paper as the filter element of the elemental filter near the shredded tobacco. The material is directly composed of pure wood pulp or 50% to 95% wood pulp and 5% to 50% composite fiber; There is also a Chinese patent application (CN101624756A) "Nonwoven fabric for biodegradable cigarette filter and its preparation method" which uses wood pulp fiber, high melting point polylactic acid fiber, low melting point polylactic acid fiber and water-soluble glue. There are also people who directly transport the tobacco fibers to the forming section through the blower to form a fluffy and uniform fiber web on the forming belt, and then through sizing, preheating, rolling, curing and forming to make cigarette filter paper, and Natural herb waste raw materials are added during the molding process. The fibers used for these airlaid papers involve fiber types such as wood pulp fibers, composite fibers, hot-melt sheath-core fibers, and polylactic acid fibers. Although these fibers can be used to make filter materials for filter tips, they filter smoke while making smoke There is a lot of loss of aroma, and a certain amount of woody gas is brought in, which has a certain negative impact on the taste and taste of cigarettes during smoking, and cannot guarantee the quality of cigarettes. What is more important is that the color and quality of these existing materials are consistent with natural The feeling of tobacco is very different, and it cannot cater to the pursuit of cigarette consumers for the feeling of natural tobacco.
在近期的研究中，也有人将烟草纤维应用于干法制纸中，将烟草纤维通过风机输送至成型工段铺网成型，在成型网带上形成蓬松均匀的纤维网。再经施胶、预热、辊压、固化和成型制成卷烟滤材纸，并在成型过程中添加天然药草废弃原料。但是它的技术方案还是通过简单烟草纤维铺设而成，而且使用各种胶体粘合而成，所以它去除杂气的效果不佳，而且使用的胶体过多会给香烟烟嘴带来异味，另外，并不能解决减少烟草废弃料的问题，而且在生产过程中额外添加烟草纤维，反而提高了整只香烟的烟草使用量。In recent research, some people have also applied tobacco fiber in dry-laid papermaking, and the tobacco fiber is transported to the forming section by a fan for laying and forming, and a fluffy and uniform fiber web is formed on the forming belt. Then through sizing, preheating, rolling, curing and molding to make cigarette filter paper, and add natural herb waste raw materials in the molding process. However, its technical solution is still made by laying simple tobacco fibers, and it is bonded with various colloids, so it is not effective in removing miscellaneous gases, and using too much colloid will bring peculiar smell to the cigarette holder. In addition, It does not solve the problem of reducing tobacco waste, and adding additional tobacco fibers in the production process increases the tobacco consumption of the whole cigarette.
另外，现有的卷烟生产企业在生产中，产生很多废料，如废弃烟叶、烟末、碎片、烟梗等，目前对这些废料的利用主要是因为降焦的目的将这些废料再加工后加入卷烟的烟丝中替代少部分烟丝，但是众所周知，这些材料在烟丝中的添加量受到非常大的限制，不能完全解决烟草生产企业废料处置的问题和变废为宝的力度。In addition, the existing cigarette manufacturers produce a lot of waste during production, such as discarded tobacco leaves, tobacco powder, debris, tobacco stems, etc. The current utilization of these wastes is mainly for the purpose of reducing coke and adding these wastes to cigarettes after reprocessing However, as we all know, the amount of these materials added to cut tobacco is very limited, which cannot completely solve the problem of waste disposal in tobacco production enterprises and the efforts to turn waste into treasure.
目前还没有找到可完全替代醋酸纤维、给消费者天然烟草感觉的新的纸质滤嘴材料。At present, there is no new paper filter material that can completely replace cellulose acetate and give consumers a natural tobacco feeling.
发明内容Contents of the invention
本发明要解决的技术问题是克服现有滤棒技术的不足，提供一种复合保润植物的三元烟草纤维纸质滤棒。本发明设计三段滤芯结构的滤棒，基于烟草纤维纸质滤棒良好的过滤、吸附功能，降低卷烟烟气中的焦油含量，并通过烟气将香味植物的有效成分带出，补充降焦给烟气香韵和吃味带来的不足，保证卷烟丰富的香韵，有效增香。The technical problem to be solved by the present invention is to overcome the deficiency of the existing filter stick technology and provide a ternary tobacco fiber paper filter stick with composite moisture-retaining plants. The present invention designs a filter rod with a three-stage filter element structure, based on the good filtering and adsorption functions of the tobacco fiber paper filter rod, reduces the tar content in cigarette smoke, and brings out the effective components of the aroma plant through the smoke to supplement tar reduction Insufficient to the aroma and taste of the smoke, to ensure the rich aroma of the cigarette and effectively enhance the aroma.
本发明另一要解决的技术问题是提供所述滤棒的制备方法。Another technical problem to be solved by the present invention is to provide a preparation method of the filter stick.
本发明的目的通过以下技术方案予以实现：The purpose of the present invention is achieved through the following technical solutions:
提供一种复合增香植物的三元烟草纤维纸质滤棒，由滤芯和包裹滤芯的成型纸组成，所述滤芯包括两段烟草纤维纸质滤芯和设置于两段烟草纤维纸质滤芯之间的香味植物颗粒滤芯连接组成，所述的烟草纤维纸质滤芯由纸质纤维辊压、卷制而成，所述的香味植物颗粒滤芯采用香味植物材料制备得到；Provided is a ternary tobacco fiber paper filter rod for compounding flavoring plants, which is composed of a filter element and a forming paper wrapping the filter element, the filter element includes two sections of tobacco fiber paper filter elements and is arranged between the two sections of tobacco fiber paper filter elements The fragrance plant particle filter element is connected, the tobacco fiber paper filter element is rolled and rolled from paper fiber, and the fragrance plant particle filter element is prepared from fragrance plant material;
所述纸质纤维是采用烟草原料和长纤维原料分别磨浆得到烟草纤维浆和长纤维浆，将烟草纤维浆和长纤维浆进行配浆、抄片、压榨、干燥制成纤维纸基，纤维纸基经涂布、干燥即得；The paper fiber is obtained by grinding tobacco raw material and long fiber raw material respectively to obtain tobacco fiber pulp and long fiber pulp, and then the tobacco fiber pulp and long fiber pulp are mixed, sheeted, pressed, and dried to form a fiber paper base. The paper base is obtained by coating and drying;
所述香味植物材料为茶叶、薄荷、菊花、玫瑰、茉莉、薰衣草、百合、丁香、兰花、郁金香、杜鹃花或荷花中的一种或几种。The scented plant material is one or more of tea, mint, chrysanthemum, rose, jasmine, lavender, lily, clove, orchid, tulip, rhododendron or lotus.
优选地，所述香味植物颗粒为粒度为8目～50目的粉末或者厚度≦0.1mm的薄片。Preferably, the fragrant plant particles are powders with a particle size of 8 mesh to 50 mesh or flakes with a thickness≦0.1mm.
优选地所述两段烟草纤维纸质滤芯和设置于两段烟草纤维纸质滤芯之间的香味植物颗粒滤芯的长度比例为1:1:1。Preferably, the length ratio of the two sections of tobacco fiber paper filter element to the aroma plant particle filter element arranged between the two sections of tobacco fiber paper filter element is 1:1:1.
所述长纤维浆的原料为烟梗、烟秸秆、烟茎、藤蔓、甘草、棉纤维、木质纤维或竹纤维中的一种或几种。优选使用烟梗、烟秸秆制备得到的长纤维，因其本身来自于烟草，对卷烟香气会有提升作用，和烟丝的一致性会更加地强。作为另一优选，本发明所述长纤维的原料可以选择竹纤维，因其来源广泛，成本适中，纤维结构与烟草原料制备得到的（短）纤维相得益彰，保证了纸质滤棒材料的抗张指数、抗张强度、撕裂指数、松厚度、紧度等性能优良，保证很好地烟气截留效率和卷烟烟气的香味。本发明可以采用常规购买的长纤维浆。所述的烟草原料包括烟梗、烟叶及碎片、烟末中的一种或几种，这几种纤维主要来源于烟草产生企业生产过程中的废弃原料，这些废弃原料需要耗费生产企业的人力、物力、财力和空间来堆置或和处置，用于制备滤棒，可以让废弃原料得到更加充分地利用。The raw material of the long-fiber pulp is one or more of tobacco stems, tobacco stalks, tobacco stems, vines, licorice, cotton fibers, wood fibers or bamboo fibers. It is preferable to use long fibers prepared from tobacco stems and tobacco stalks, because they are derived from tobacco, which can improve the aroma of cigarettes and have a stronger consistency with shredded tobacco. As another preference, bamboo fiber can be selected as the raw material of the long fiber of the present invention, because of its wide source, moderate cost, fiber structure and (short) fiber prepared from tobacco raw materials complement each other, ensuring the tensile strength of the paper filter rod material Index, tensile strength, tear index, bulk, tightness and other properties are excellent, ensuring good smoke retention efficiency and cigarette smoke flavor. The present invention can use conventionally purchased long fiber pulp. The tobacco raw materials include one or more of tobacco stems, tobacco leaves and chips, and tobacco powder. These fibers are mainly derived from waste materials in the production process of tobacco production enterprises. These waste materials need to consume manpower, Material resources, financial resources and space are used to stack or dispose of filter rods, so that waste materials can be more fully utilized.
优选地，所述烟草纤维浆和长纤维浆进行配浆的质量比例为1:0.5～3；更为优选1:1～2。Preferably, the mass ratio of the tobacco fiber pulp and the long fiber pulp is 1:0.5-3; more preferably 1:1-2.
本发明同时提供了所述复合增香植物的三元烟草纤维纸质滤棒的制备方法，其特征在于，包括以下步骤：The present invention simultaneously provides the preparation method of the ternary tobacco fiber paper filter stick of the compound aroma-enhancing plant, which is characterized in that it comprises the following steps:
S1.制备烟草纤维纸质基材；S1. Prepare tobacco fiber paper substrate;
S2.制备香味植物颗粒滤芯：将香味植物颗粒用成型纸包裹或将香味植物颗粒洒于烟草纤维纸质基材经辊压、卷制得到中药材颗粒滤芯；S2. Prepare the scented plant particle filter element: wrap the scented plant particle with molding paper or sprinkle the scented plant particle on the tobacco fiber paper substrate, roll and roll to obtain a Chinese herbal medicine particle filter element;
S3.将烟草纤维纸质基材经辊压，卷制，切段，得烟草纤维纸质滤芯；将香味植物颗粒滤芯设置于两段烟草纤维纸质滤芯之间；在三段滤芯外包裹成型纸即得复合草本植物的三元烟草纤维纸质滤棒。S3. The tobacco fiber paper substrate is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the aroma plant particle filter element is arranged between two sections of tobacco fiber paper filter elements; wrapped and formed outside the three-section filter element The paper is a ternary tobacco fiber paper filter rod of composite herbal plants.
优选地，S3是将烟草纤维纸质基材经辊压，卷制，切段，得烟草纤维纸质滤芯，应用于卷烟的烟丝端；将烟草纤维纸质基材经辊压，卷制，压制沟槽，切段，得带有沟槽的烟草纤维纸质滤芯，应用于卷烟的嘴唇接触端；将增香植物滤芯设置于烟丝端和嘴唇接触端的烟草纤维纸质滤芯之间；在三段滤芯外包裹成型纸即得。Preferably, in S3, the tobacco fiber paper substrate is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element, which is applied to the shredded tobacco end of the cigarette; the tobacco fiber paper substrate is rolled, rolled, Press the groove, cut into sections, and obtain a tobacco fiber paper filter element with grooves, which is applied to the lip contact end of the cigarette; the flavoring plant filter element is arranged between the shredded tobacco end and the tobacco fiber paper filter element at the lip contact end; Wrap the section filter element with molding paper.
优选地，S1包括以下步骤：Preferably, S1 includes the following steps:
S11.将烟草纤维原料和长纤维原料浸提处理，分别得到烟草纤维原料的提取液、烟草纤维原料固体渣、长纤维原料提取液和长纤维原料固体渣；S11. extracting the tobacco fiber raw material and the long fiber raw material to obtain respectively the extract of the tobacco fiber raw material, the solid slag of the tobacco fiber raw material, the extract of the long fiber raw material and the solid slag of the long fiber raw material;
S12.将烟草纤维原料固体渣和长纤维原料固体渣分别磨浆，得到烟草纤维浆和长纤维浆；S12. Refining the tobacco fiber raw material solid slag and the long fiber raw material solid slag respectively to obtain tobacco fiber pulp and long fiber pulp;
S13.将烟草纤维浆和长纤维原料浆按质量比1：0.5～3混合抄片，经压榨，干燥，制成烟草纤维纸基；S13. Mixing the tobacco fiber pulp and the long fiber raw material pulp according to the mass ratio of 1:0.5-3 to make a sheet, pressing and drying to make a tobacco fiber paper base;
S14.将步骤S1得到的烟草纤维原料提取液涂到S3所得的烟草纤维纸基上，干燥，得到烟草纤维纸质基材。S14. Apply the tobacco fiber raw material extract obtained in step S1 to the tobacco fiber paper base obtained in S3, and dry to obtain a tobacco fiber paper base.
优选地，所述烟草纤维浆和长纤维浆进行配浆的质量比例为1:0.5～3。更优选为1：1～2。Preferably, the mass ratio of the tobacco fiber pulp and the long fiber pulp is 1:0.5-3. More preferably, it is 1:1-2.
S2所述将中药材粉碎过8目～50目筛；或者将中药材切成厚度≦0.1mm的薄片。As described in S2, crush the Chinese herbal medicine through a sieve of 8 mesh to 50 mesh; or cut the Chinese herbal medicine into thin slices with a thickness ≤ 0.1 mm.
S11所述浸提处理的温度为60～90℃，持续60～100分钟，反复1～3次。The temperature of the leaching treatment in S11 is 60-90°C, lasts for 60-100 minutes, and repeats 1-3 times.
本发明有益效果如下：The beneficial effects of the present invention are as follows:
1、本发明提供了一种新的三元复合烟草纤维纸质滤棒，本发明设计三段滤芯结构的滤棒，为依次相连接的烟草纤维纸质滤芯、香味植物颗粒滤芯、烟草纤维纸质滤芯，基于烟草纤维纸质滤棒，本发明彻底改变了现有的滤棒材料设计思想，真正将天然烟草纤维材料的质感和优良的滤棒功能完美结合，本发明纸质滤棒具有较高的吸附性及相对吸收性，相比现有的醋酸纤维或聚丙烯纤维纤维材料，纸质的滤棒比醋酸纤维有更强的去除焦油和尼古丁的能力，可以吸附更多的卷烟主流烟气气溶胶，从而提高滤棒的过滤效率，保证了优良的降焦和减害功能，香味植物颗粒的有效成分被烟气带出，补充降焦给烟气香韵和吃味带来的损失，实验证明，本发明滤棒中香味植物成分与烟气中的致香成分相辅相成，改善卷烟烟气润湿性，赋予卷烟更加丰富的香韵，提升烟气香气丰富度。1. The present invention provides a new ternary composite tobacco fiber paper filter rod. The present invention designs a three-stage filter element structure filter rod, which is a tobacco fiber paper filter element, a fragrance plant particle filter element, and a tobacco fiber paper filter element connected in sequence. Based on the tobacco fiber paper filter rod, the present invention has completely changed the design idea of the existing filter rod material, and truly perfectly combines the texture of the natural tobacco fiber material with the excellent filter rod function. The paper filter rod of the present invention has a relatively high High adsorption and relative absorption. Compared with the existing acetate fiber or polypropylene fiber material, the paper filter stick has a stronger ability to remove tar and nicotine than acetate fiber, and can absorb more cigarette mainstream smoke Aerosol, thereby improving the filtration efficiency of the filter rod, ensuring excellent coke reduction and harm reduction functions, the active ingredients of the scented plant particles are carried out by the smoke, supplementing the loss of coke reduction to the aroma and taste of the smoke , Experiments have proved that the aroma plant components in the filter stick of the present invention and the aroma components in the smoke complement each other, improve the wettability of the cigarette smoke, endow the cigarette with a richer aroma, and increase the aroma richness of the smoke.
2、本发明滤棒使用的原料全部来源于天然植物，纸质的滤嘴摈除了消费者不喜欢的“纸张的味道”和“化纤的味道”，滤棒颜色外观与卷烟烟丝相近，具有强烈的烟草天然材料质感，配以香味植物的香味成分，带给消费者全新的天然、增香的感官冲击。实现滤棒技术可视化、可触摸化，产品具有丰富的香味，引发消费者兴趣，易于口碑相传，对卷烟产品的销售具有较强的市场触动性，为卷烟技术领域指引了新的研究方向。2. The raw materials used in the filter stick of the present invention are all derived from natural plants. The paper filter tip eliminates the "taste of paper" and "taste of chemical fiber" that consumers do not like. The texture of natural tobacco materials, together with the aroma components of aromatic plants, brings consumers a new natural and aroma-enhancing sensory impact. Realize the visualization and touchability of the filter stick technology, the product has a rich fragrance, arouses consumers' interest, is easy to spread by word of mouth, has a strong market impact on the sales of cigarette products, and guides a new research direction for the field of cigarette technology.
3、本发明滤棒材料具有优良的承载能力，其更适合承载各种烟用添加剂。3. The filter rod material of the present invention has excellent load-carrying capacity, and is more suitable for carrying various cigarette additives.
4、采用合适的短纤维浆和长纤维浆的比例，采用造纸法制备得到纸质烟草纤维纸质滤芯，不但有效提高了滤棒的过滤效率，降低卷烟的焦油及有害物质，而且大大的提高了吸烟者对滤棒纸质和天然烟草感官体验的需求，在吸食香烟时得到更好的接触感受。4. Using a suitable ratio of short fiber pulp and long fiber pulp, the paper tobacco fiber paper filter element is prepared by papermaking method, which not only effectively improves the filtration efficiency of the filter rod, reduces the tar and harmful substances of cigarettes, but also greatly improves the It meets the needs of smokers for the sensory experience of filter rod paper and natural tobacco, and obtains a better contact feeling when smoking cigarettes.
5、本发明滤棒的制备方法简单，易于推广。5. The preparation method of the filter rod of the present invention is simple and easy to popularize.
附图说明Description of drawings
图1烟草纤维纸质滤棒材料实物图。Fig. 1 The actual picture of the tobacco fiber paper filter rod material.
图2烟草纤维纸质滤棒电子显微镜图。Fig. 2 Electron microscope image of tobacco fiber paper filter rod.
图3含增香植物的三元纸质滤棒结构示意图。Fig. 3 Schematic diagram of the structure of a ternary paper filter stick containing aromatizing plants.
其中，1为烟草纤维纸质滤芯，2为天然香味植物滤芯，3为成型纸。Wherein, 1 is a tobacco fiber paper filter element, 2 is a natural fragrance plant filter element, and 3 is a molding paper.
图4带有沟槽设计复合增香植物的三元纸质滤棒结构示意图Figure 4 Schematic diagram of the structure of the ternary paper filter rod with a groove design compound aroma-enhancing plant
其中，1为烟草纤维纸质滤芯，2为保润植物滤芯，3为成型纸，4为带有沟槽的烟草纤维纸质滤芯，5为沟槽。Among them, 1 is a tobacco fiber paper filter element, 2 is a moisturizing plant filter element, 3 is a molding paper, 4 is a tobacco fiber paper filter element with grooves, and 5 is a groove.
具体实施方式Detailed ways
下面结合附图和具体实施例进一步详细说明本发明。天然香味植物均为市购。The present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments. All natural fragrance plants were purchased from the market.
实施例1Example 1
S1用烟叶、烟梗和甘草制备烟草纤维滤芯S1 prepares tobacco fiber filter element with tobacco leaves, tobacco stems and licorice
（1）提取烟叶和烟梗(1) Extracting tobacco leaves and stems
S11.将烟草原料浸提处理，得到烟草原料的提取液、烟草原料的固体渣；S11. extracting the tobacco raw material to obtain an extract of the tobacco raw material and a solid slag of the tobacco raw material;
本实施例按料液质量比为1：7分别将烟梗和水，提取温度为60℃，提取时间为100分钟，反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1：10分别将烟叶和水，提取温度为80℃，提取时间为60分钟，反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
S12.将烟草原料的固体渣磨浆，得到烟草纤维浆；市购木质纤维浆本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。S12. Refining the solid slag of tobacco raw materials to obtain tobacco fiber pulp; commercially available lignocellulosic pulp. The refining process in this embodiment refers to the refining process in the existing tobacco sheet.
将甘草用适量水浸泡（浸泡时间不做严格限定，通常为60分钟左右）后磨浆得甘草长纤维浆；Soak the licorice with an appropriate amount of water (soaking time is not strictly limited, usually about 60 minutes), and then refine to obtain licorice long-fiber pulp;
S13.将烟草纤维浆和甘草长纤维浆按质量比为1：0.5的比例配抄，抄片获得烟草纤维纸基，在压力为0.4MPa压力下压榨5分钟，然后置于温度为105℃下干燥1小时。S13. Blend tobacco fiber pulp and licorice long fiber pulp at a mass ratio of 1:0.5, and sheet to obtain tobacco fiber paper base, press at a pressure of 0.4MPa for 5 minutes, and then place at a temperature of 105°C Let dry for 1 hour.
S14.将S11所得的烟梗提取液和烟叶提取液重新涂布到烟草纤维纸基上，自然干燥，得到烟草纤维纸质基材。S14. Recoat the tobacco stem extract and tobacco leaf extract obtained in S11 on a tobacco fiber paper base, and dry naturally to obtain a tobacco fiber paper base.
S2.制备茶叶滤芯：将茶叶切成与卷烟烟丝粗细近似的茶叶丝，包裹成型纸即得；茶叶可以采用市购的铁观音、乌龙茶等品种茶叶，不做严格限定。S2. Preparation of tea filter element: cut the tea leaves into shreds of tea leaves which are similar in thickness to cigarette shreds, and wrap them in molding paper; the tea leaves can be Tieguanyin tea, oolong tea and other varieties available in the market, and are not strictly limited.
S3.将烟草纤维纸质基材经辊压，卷制，切段，得烟草纤维纸质滤芯；将茶叶滤芯设置于两段烟草纤维纸质滤芯之间；在三段滤芯外包裹水松纸即得含草本植物的三元纸质滤棒。三段滤芯的长度比例为1:1:1。S3. The tobacco fiber paper substrate is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the tea filter element is placed between the two sections of tobacco fiber paper filter elements; and tipping paper is wrapped around the three sections of the filter element A ternary paper filter stick containing herbs is obtained. The length ratio of the three-section filter element is 1:1:1.
滤棒的结构如附图3所示，其中，1为烟草纤维纸质滤芯，2为茶叶滤芯，3为成型纸。下述实施例结构同本实施例。The structure of the filter rod is as shown in accompanying drawing 3, wherein, 1 is the tobacco fiber paper filter core, 2 is the tea filter core, 3 is the molding paper. The structure of the following embodiments is the same as this embodiment.
实施例2Example 2
S1.用烟末、烟碎片和烟秸秆制备带沟槽烟草纤维滤棒S1. Preparation of grooved tobacco fiber filter rods from tobacco powder, tobacco fragments and tobacco stalks
S11.将原料浸提处理，得到原料的提取液、原料的固体渣；S11. extracting the raw material to obtain the extract of the raw material and the solid slag of the raw material;
本实施例按料液质量比为1：7分别将烟梗和水，提取温度为60℃，提取时间为100分钟，反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1：10分别将烟叶和水，提取温度为80℃，提取时间为60分钟，反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
按料液质量比为1：10分别将烟碎片和水，提取温度为75℃，提取时间为60分钟。处理后得到的烟碎片提取液和烟碎片固体渣。According to the mass ratio of solid to liquid of 1:10, the smoke fragments and water were separated, the extraction temperature was 75°C, and the extraction time was 60 minutes. The smoke chip extract and the smoke chip solid slag obtained after treatment.
S12.将烟叶固体渣和烟碎片固体渣按照1:1的质量比例混合后磨浆，得到烟草纤维浆；S12. mixing the solid slag of tobacco leaves and the solid slag of tobacco chips according to the mass ratio of 1:1, and refining to obtain tobacco fiber pulp;
另取干燥的烟秸秆用适量水浸泡（浸泡时间不做严格限定，通常为60分钟左右）后磨浆得烟秸秆长纤维浆；本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。Separately take dry tobacco stalks and soak them in an appropriate amount of water (soaking time is not strictly limited, usually about 60 minutes) and refine them to obtain tobacco stalk long-fiber pulp; the refining process in this example refers to the refining process in the existing tobacco sheet .
S13.将烟草纤维浆和烟秸秆长纤维浆按质量比为1：3的比例配抄，抄片获得烟草纤维纸基，在压力为0.4MPa压力下压榨5分钟，然后置于温度为105℃下干燥1小时。S13. Blend tobacco fiber pulp and tobacco stalk long-fiber pulp at a mass ratio of 1:3, and sheet to obtain tobacco fiber paper base, press at a pressure of 0.4MPa for 5 minutes, and then place at a temperature of 105°C Dry for 1 hour.
S14.将步骤S11得到的烟草纤维原料的提取液涂步到S13干燥后的烟草纤维纸基上，然后干燥，得到烟草纤维纸质基材；见附图1，烟草纤维纸质基材的颜色和质感与烟丝十分相近。S14. apply the extract of the tobacco fiber raw material obtained in step S11 to the tobacco fiber paper base after drying in S13, and then dry to obtain the tobacco fiber paper base; see accompanying drawing 1, the color of the tobacco fiber paper base The texture is very similar to shredded tobacco.
S2.制备薄荷滤芯：将薄荷切成与卷烟烟丝粗细近似的薄荷丝，包裹成型纸即得；S2. Prepare the mint filter element: cut the mint into mint shreds that are similar in thickness to cigarette shreds, and wrap them in molding paper to obtain;
S3.将烟草纤维纸质基材经辊压，卷制，切段，得烟草纤维纸质滤芯，应用于卷烟的烟丝端；将烟草纤维纸质基材经辊压，卷制，压制沟槽，切段，得带有沟槽的烟草纤维纸质滤芯，应用于卷烟的嘴唇接触端；将增香植物滤芯设置于烟丝端和嘴唇接触端烟草纤维纸质滤芯之间；在三段滤芯外包裹成型纸即得。滤棒结构见附图4所示。S3. Rolling, rolling, and cutting the tobacco fiber paper base material to obtain a tobacco fiber paper filter element, which is applied to the shredded tobacco end of the cigarette; rolling, rolling, and pressing the tobacco fiber paper base material into grooves , cut into sections to obtain a tobacco fiber paper filter element with grooves, which is applied to the lip contact end of the cigarette; the flavoring plant filter element is arranged between the shredded tobacco end and the tobacco fiber paper filter element at the lip contact end; outside the three-section filter element Wrap in wrapping paper and serve. The filter rod structure is shown in accompanying drawing 4.
实施例3Example 3
S1.用烟末、烟碎片和烟茎制备带沟槽烟草纤维滤棒S1. Preparation of grooved tobacco fiber filter rods from tobacco dust, tobacco fragments and tobacco stems
S11.将原料浸提处理，得到原料的提取液、原料的固体渣；S11. extracting the raw material to obtain the extract of the raw material and the solid slag of the raw material;
本实施例按料液质量比为1：7分别将烟梗和水，提取温度为60℃，提取时间为100分钟，反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1：10分别将烟叶和水，提取温度为80℃，提取时间为60分钟，反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
按料液质量比为1：10分别将烟碎片和水，提取温度为75℃，提取时间为60分钟。处理后得到的烟碎片提取液和烟碎片固体渣。According to the mass ratio of solid to liquid of 1:10, the smoke fragments and water were separated, the extraction temperature was 75°C, and the extraction time was 60 minutes. The smoke chip extract and the smoke chip solid slag obtained after treatment.
S12.将烟叶固体渣和烟碎片固体渣按照1:1的质量比例混合后磨浆，得到烟草纤维浆；S12. mixing the solid slag of tobacco leaves and the solid slag of tobacco chips according to the mass ratio of 1:1, and refining to obtain tobacco fiber pulp;
另取干燥的烟茎用适量水浸泡（浸泡时间不做严格限定，通常为60分钟左右）后磨浆得烟茎长纤维浆；本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。Another dried tobacco stem is soaked in an appropriate amount of water (soaking time is not strictly limited, usually about 60 minutes) and then refined to obtain tobacco stem long-fiber pulp; the refining process in this example refers to the refining process in the existing tobacco sheet .
S13.将烟草纤维浆和烟茎长纤维浆按质量比为1：1的比例配抄，抄片获得烟草纤维纸基，在压力为0.4MPa压力下压榨5分钟，然后置于温度为105℃下干燥1小时。S13. Blend tobacco fiber pulp and tobacco stem long fiber pulp in a ratio of 1:1 by mass, and make sheet to obtain tobacco fiber paper base, press at a pressure of 0.4MPa for 5 minutes, and then place at a temperature of 105°C Dry for 1 hour.
S14.将步骤S11得到的烟草纤维原料的提取液涂步到S13干燥后的烟草纤维纸基上，然后干燥，得到烟草纤维纸质基材；见附图1，烟草纤维纸质基材的颜色和质感与烟丝十分相近。S14. apply the extract of the tobacco fiber raw material obtained in step S11 to the tobacco fiber paper base after drying in S13, and then dry to obtain the tobacco fiber paper base; see accompanying drawing 1, the color of the tobacco fiber paper base The texture and texture are very similar to shredded tobacco.
S2.制备菊花滤芯：将菊花切成与卷烟烟丝粗细近似的菊花丝，包裹成型纸即得；S2. Prepare the chrysanthemum filter element: cut the chrysanthemum into chrysanthemum shreds that are similar in thickness to cigarette shredded tobacco, and wrap them in molding paper to obtain the product;
S3.将烟草纤维纸质基材经辊压，卷制，切段，得烟草纤维纸质滤芯；将菊花滤芯设置于两段烟草纤维纸质滤芯之间；在三段滤芯外包裹水松纸即得含草本植物的三元纸质滤棒。S3. The tobacco fiber paper base material is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the chrysanthemum filter element is placed between two sections of tobacco fiber paper filter elements; tipping paper is wrapped outside the three sections of filter element A ternary paper filter stick containing herbs is obtained.
实施例4Example 4
S1.用烟末和木纤维浆制备烟草纤维滤棒S1. Preparation of tobacco fiber filter rods from tobacco dust and wood fiber pulp
S11.将烟草原料浸提处理，得到烟草原料的提取液、烟草原料的固体渣；S11. extracting the tobacco raw material to obtain an extract of the tobacco raw material and a solid slag of the tobacco raw material;
本实施例按料液质量比为1：7分别将烟梗和水，提取温度为60℃，提取时间为100分钟，反复提取三次。处理后得到的烟梗提取液和烟梗固体渣。In this example, tobacco stems and water were extracted at a mass ratio of 1:7 at a temperature of 60°C and an extraction time of 100 minutes, and the extraction was repeated three times. Tobacco stem extract and tobacco stem solid slag obtained after treatment.
按料液质量比为1：10分别将烟叶和水，提取温度为80℃，提取时间为60分钟，反复提取三次。处理后得到的烟叶提取液和烟叶固体渣。Tobacco leaves and water were extracted at a mass ratio of 1:10, the extraction temperature was 80°C, and the extraction time was 60 minutes, and the extraction was repeated three times. Tobacco leaf extract and tobacco leaf solid slag obtained after treatment.
S12.将烟草原料的固体渣别磨浆，得到烟草纤维浆；市购木纤维浆，本实施例磨浆工艺参照现有烟草薄片中的磨浆工艺。S12. Separately refine the solid slag of the tobacco raw material to obtain tobacco fiber pulp; commercially available wood fiber pulp, the refining process in this embodiment refers to the refining process in the existing tobacco sheet.
S13.将烟草纤维浆和竹纤维浆（市购）按质量比为1：2的比例配抄，抄片获得烟草纤维纸基，在压力为0.4MPa压力下压榨5分钟，然后置于温度为105℃下干燥1小时。S13. Blending tobacco fiber pulp and bamboo fiber pulp (commercially available) at a mass ratio of 1:2, sheeting to obtain a tobacco fiber paper base, pressing for 5 minutes under a pressure of 0.4 MPa, and then placing it at a temperature of Dry at 105°C for 1 hour.
S14.将步骤S11得到的烟草纤维原料的提取液涂步到S13干燥后的烟草纤维纸基上，然后干燥，得到烟草纤维纸质基材；S14. Apply the extract of the tobacco fiber raw material obtained in step S11 to the tobacco fiber paper base dried in S13, and then dry to obtain the tobacco fiber paper base material;
S2.制备丁香滤芯：将丁香切成与卷烟烟丝粗细近似的丁香丝，包裹成型纸即得；S2. Prepare the clove filter element: cut the clove into clove shreds that are similar in thickness to cigarette shredded tobacco, and wrap the clove in molding paper to obtain the product;
S3.将烟草纤维纸质基材经辊压，卷制，切段，得烟草纤维纸质滤芯；将丁香滤芯设置于两段烟草纤维纸质滤芯之间；在三段滤芯外包裹水松纸即得含草本植物的三元纸质滤棒。S3. The tobacco fiber paper substrate is rolled, rolled, and cut into sections to obtain a tobacco fiber paper filter element; the clove filter element is placed between two sections of tobacco fiber paper filter elements; and tipping paper is wrapped outside the three sections of filter element A ternary paper filter stick containing herbs is obtained.
实施例5应用检测Example 5 Application detection
1、物理性能根据Y/CT152-2001进行测定实施例1、2、3、4所得滤棒的物理性能，结果如表1所述。1. Physical properties The physical properties of the filter rods obtained in Examples 1, 2, 3, and 4 were measured according to Y/CT152-2001, and the results are as described in Table 1.
表1纤维材料物理性能Table 1 Physical properties of fiber materials
2、卷烟感官评价结果2. Results of sensory evaluation of cigarettes
以采用醋酸纤维滤棒的卷烟为对照样，与采用本发明所得烟草纤维纸质滤棒的卷烟样品为试验样，进行卷烟感官评吸，结果见表2所示，感官评吸的分数由7名专业评吸员各自打分后，取平均分后所得（每个项目满分为10分，小数点后保留一位小数，趋势越好，分数越高）。Taking the cigarette that adopts the cellulose acetate filter rod as the control sample, and the cigarette sample that adopts the tobacco fiber paper filter rod obtained by the present invention as the test sample, carry out the cigarette sensory evaluation and smoking, the results are shown in Table 2, and the scores of the sensory evaluation and smoking are divided by 7 The average score is obtained after each professional reviewer scores each item (the full score for each item is 10 points, and one decimal place is reserved after the decimal point. The better the trend, the higher the score).
表2感官评价结果Table 2 Sensory evaluation results
3、卷烟烟气七种有害成分化学分析3. Chemical analysis of seven harmful components in cigarette smoke
以采用醋酸纤维滤棒的卷烟为对照样，与采用本发明实施例3所得烟草纤维纸质滤棒的卷烟样品为试验样，根据卷烟危害性评价指数，对样品燃吸产生的烟气成分进行化学检测，以7种主要的有害物质作为检测指标，卷烟危害性指数见表3所示，结果显示，实施例3的危害性指数与正常样相比，降低了16.17%。Taking the cigarette that adopts the cellulose acetate filter rod as the control sample, and the cigarette sample that adopts the tobacco fiber paper filter rod obtained in Example 3 of the present invention as the test sample, according to the cigarette hazard evaluation index, the smoke components generated by the burning of the sample are analyzed. For chemical detection, 7 main harmful substances were used as detection indicators. The hazard index of cigarettes is shown in Table 3. The results showed that the hazard index of Example 3 was reduced by 16.17% compared with the normal sample.
表3卷烟危害性评价结果Table 3 Results of cigarette hazard evaluation
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210588882.9ACN103445295B (en) | 2012-12-29 | 2012-12-29 | Ternary tobacco fiber paper filter rod made from composite aroma-enhancing plants and preparation method of filter rod |
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210588882.9ACN103445295B (en) | 2012-12-29 | 2012-12-29 | Ternary tobacco fiber paper filter rod made from composite aroma-enhancing plants and preparation method of filter rod |
| Publication Number | Publication Date |
|---|---|
| CN103445295A CN103445295A (en) | 2013-12-18 |
| CN103445295Btrue CN103445295B (en) | 2015-06-03 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210588882.9AActiveCN103445295B (en) | 2012-12-29 | 2012-12-29 | Ternary tobacco fiber paper filter rod made from composite aroma-enhancing plants and preparation method of filter rod |
| Country | Link |
|---|---|
| CN (1) | CN103445295B (en) |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104018401A (en)* | 2014-05-30 | 2014-09-03 | 滁州卷烟材料厂 | Tipping paper base paper with health care function and preparation method thereof |
| CN104005268B (en)* | 2014-05-30 | 2016-05-04 | 滁州卷烟材料厂 | A kind of antibacterial moistureproof high-quality cork paper body paper and preparation method thereof |
| CN104005296B (en)* | 2014-05-30 | 2016-05-04 | 滁州卷烟材料厂 | A kind of cork paper with preventing phlegm from forming and stopping coughing effect and preparation method thereof |
| CN104005251B (en)* | 2014-05-30 | 2016-05-04 | 滁州卷烟材料厂 | A kind of pharynx-clearing throat-benefiting functional form cork paper and preparation method thereof |
| CN104005287A (en)* | 2014-05-30 | 2014-08-27 | 滁州卷烟材料厂 | Tipping paper capable of clearing away heat and toxic materials and alleviating hot and dry feelings of throat and preparation method thereof |
| CN104005301A (en)* | 2014-05-30 | 2014-08-27 | 滁州卷烟材料厂 | Cool, refreshing and comfortable type raw tipping paper and preparation method thereof |
| CN104153253A (en)* | 2014-07-29 | 2014-11-19 | 安徽省三环纸业(集团)有限公司 | Antioxidant, heat-clearing and detoxifying tipping paper of lady cigarettes and preparation method thereof |
| CN104153255A (en)* | 2014-07-29 | 2014-11-19 | 安徽省三环纸业(集团)有限公司 | Unprocessed rehmannia root and tortoise shell health aroma type tipping paper with high tensile strength and preparation method thereof |
| US20160073686A1 (en)* | 2014-09-12 | 2016-03-17 | R.J. Reynolds Tobacco Company | Tobacco-derived filter element |
| US9950858B2 (en) | 2015-01-16 | 2018-04-24 | R.J. Reynolds Tobacco Company | Tobacco-derived cellulose material and products formed thereof |
| CN105132167A (en)* | 2015-08-18 | 2015-12-09 | 昆明理工大学 | Plant particle capable of moisturizing and carrying fragrance, and preparation method and applications thereof |
| CN105795517A (en)* | 2016-05-18 | 2016-07-27 | 云南中烟新材料科技有限公司 | Fen-flavor cigarette holder containing various natural plant materials |
| CN106617286A (en)* | 2017-01-16 | 2017-05-10 | 河北中烟工业有限责任公司 | Preparation method of lotus leaf-type composite filter rods of cigarettes |
| CN107212466A (en)* | 2017-03-07 | 2017-09-29 | 南通烟滤嘴有限责任公司 | Hot-fluid Cigarette |
| CN108991598A (en)* | 2018-05-25 | 2018-12-14 | 颐中（青岛）实业有限公司 | A kind of preparation method of fermentation of Chinese herbal medicine Three-element composite filter core |
| CN108991597A (en)* | 2018-05-25 | 2018-12-14 | 颐中（青岛）实业有限公司 | A kind of preparation method of fermentation of Chinese herbal medicine binary compound filter candle |
| CN109602073A (en)* | 2018-11-16 | 2019-04-12 | 深圳市凯神科技股份有限公司 | Tobacco filler, cigarette feed liquid additive and cigarette |
| CN113455695A (en)* | 2021-06-30 | 2021-10-01 | 河南中烟工业有限责任公司 | Processing method of clove raw material and application of clove raw material in clove type cigarettes |
| CN116268564A (en)* | 2022-12-05 | 2023-06-23 | 内蒙古昆明卷烟有限责任公司 | A slow-release filter stick with aroma-enhancing function and its preparation process |
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102273732B (en)* | 2011-06-03 | 2013-04-10 | 湖南中烟工业有限责任公司 | Weakly polar cigarette paper filter material and preparation and application methods thereof |
| CN102247013A (en)* | 2011-07-02 | 2011-11-23 | 云南瑞升烟草技术（集团）有限公司 | Method for preparing low-acetification natural fiber filter stick |
| CN102326863A (en)* | 2011-07-02 | 2012-01-25 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of cigarette paper filter material containing nicotiana tabacum extract |
| CN102277780B (en)* | 2011-07-19 | 2013-05-22 | 湖北中烟工业有限责任公司 | A kind of production method of tobacco sheet cigarette paper |
| CN102423135A (en)* | 2011-08-28 | 2012-04-25 | 云南烟草科学研究院 | Application of mint leaves and Pu'er tea in ternary composite filter tips |
| CN102599636B (en)* | 2012-03-10 | 2014-09-10 | 广东中烟工业有限责任公司 | Preparation method of reconstituted tobacco from tobacco stem and tobacco powder |
| CN102747647B (en)* | 2012-06-06 | 2014-06-25 | 云南瑞升烟草技术（集团）有限公司 | Paper cigarette filter rod filter media and processing method thereof |
| Publication number | Publication date |
|---|---|
| CN103445295A (en) | 2013-12-18 |
| Publication | Publication Date | Title |
|---|---|---|
| CN103445295B (en) | Ternary tobacco fiber paper filter rod made from composite aroma-enhancing plants and preparation method of filter rod | |
| CN103054189B (en) | Ternary tobacco fiber paper filter stick of composite moistening plants and preparation method thereof | |
| CN103829374A (en) | Tobacco fiber paper filter stick and preparation method thereof | |
| CN103284327B (en) | Tobacco paper filter stick combining bamboo fiber and preparation method of tobacco paper filter stick | |
| CN108783572A (en) | The reconstituted tobacoo and production technology of the high porosity with herbal applied to low temperature cigarette | |
| CN102860586B (en) | Non-woven fabric filter tip material with materia medica incense smoke and preparation method thereof | |
| CN108968139A (en) | The reconstituted tobacoo and production technology of the high porosity with the fragrance of a flower applied to low temperature cigarette | |
| CN112586795A (en) | Plant scented chip for cigarette leaf group and preparation method thereof | |
| CN112853811A (en) | Powder forming coating papermaking process | |
| CN206354420U (en) | A kind of dry process reproduction tobacco leaf filter stick | |
| CN118716667A (en) | Roll-pressed sheet, preparation method thereof and cigarette | |
| CN104256900A (en) | Novel electronic cigarette cotton | |
| CN103622157B (en) | Ternary tobacco fiber paper filter stick containing herbaceous plants and manufacturing method thereof | |
| CN101912161A (en) | A filter stick for menthol cigarettes and its preparation method | |
| CN103271439A (en) | Filter rod for composite cigarette and cigarette products thereof | |
| CN103110186B (en) | Dibasic compound hollow tobacco fiber paper filtering stick and preparation method thereof | |
| CN108523197A (en) | The preparation method of low temperature cigarette with green tea style | |
| CN108523242A (en) | The low temperature cigarette and preparation method thereof of loose integrated tobacco segment with herbal | |
| CN109619674A (en) | A kind of preparation method of cigarette lotus fiber and moisturizing filter rod containing the lotus fiber | |
| CN111418888B (en) | Heating non-combustion smoke body and low-temperature cigarette | |
| CN103110185B (en) | A kind of ternary tobacco fiber paper filter rod of composite shredded tobacco and its preparation method | |
| CN107319632A (en) | A kind of preparation method of paper filter stick | |
| CN108338399A (en) | A kind of health care tobacco preparation of sections method | |
| CN108420124A (en) | A kind of low temperature cigarette and preparation method thereof with pungent fragrant loose integrated tobacco segment | |
| CN101897478A (en) | A filter stick for cigarettes and its preparation method |
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |