Movatterモバイル変換


[0]ホーム

URL:


CN103181613A - Preparation method of electric dry distillation type tobacco sheet - Google Patents

Preparation method of electric dry distillation type tobacco sheet
Download PDF

Info

Publication number
CN103181613A
CN103181613ACN2013101230504ACN201310123050ACN103181613ACN 103181613 ACN103181613 ACN 103181613ACN 2013101230504 ACN2013101230504 ACN 2013101230504ACN 201310123050 ACN201310123050 ACN 201310123050ACN 103181613 ACN103181613 ACN 103181613A
Authority
CN
China
Prior art keywords
tobacco
reconstituted tobacoo
extract
sheet base
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN2013101230504A
Other languages
Chinese (zh)
Other versions
CN103181613B (en
Inventor
刘华臣
潘曦
罗诚浩
刘祥浩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hunan Industrial Co Ltd, Wuhan Huanghelou Science and Technology Park Co LtdfiledCriticalChina Tobacco Hunan Industrial Co Ltd
Priority to CN201310123050.4ApriorityCriticalpatent/CN103181613B/en
Publication of CN103181613ApublicationCriticalpatent/CN103181613A/en
Application grantedgrantedCritical
Publication of CN103181613BpublicationCriticalpatent/CN103181613B/en
Activelegal-statusCriticalCurrent
Anticipated expirationlegal-statusCritical

Links

Landscapes

Abstract

Translated fromChinese

本发明提供了一种电干馏型烟草薄片的制备方法,其步骤包括:(1)将烟草提取物和天然植物提取物中的一种或多种混合得到片基喷涂物;(2)再将片基喷涂物均匀涂布在重量为片基喷涂物1-10倍的烟草薄片片基上然后在40-90℃下干燥;(3)然后将烟草薄片片基重量的2-50%的雾化剂香料喷洒在烟草薄片片基上;(4)最后将烟草薄片片基干燥后得到所述电干馏型烟草薄片。本发明制备出的烟草薄片,能够在电干馏装置中燃烧而产生烟雾。电干馏的方式能够干馏出烟草提取物包含的烟草本香。该种薄片制备工艺制备的薄片具有烟草本香与烟用香精香料浑然一体。满足消费的需求,降低卷烟燃烧对消费者的危害,避免二手烟的产生,具有很强的实用性。The invention provides a method for preparing electric dry distillation tobacco sheet, the steps of which include: (1) mixing one or more of tobacco extracts and natural plant extracts to obtain a base spray; (2) adding The base spray is evenly coated on the tobacco sheet base whose weight is 1-10 times that of the base spray and then dried at 40-90°C; (4) finally drying the tobacco sheet base to obtain the electric dry distillation tobacco sheet. The tobacco sheet prepared by the invention can be burned in an electric dry distillation device to generate smoke. The method of electric dry distillation can dry distill the tobacco aroma contained in the tobacco extract. The sheet prepared by the thin sheet preparation process has the natural tobacco flavor and tobacco essence and fragrance in one. It is very practical to meet the needs of consumption, reduce the harm of cigarette burning to consumers, and avoid the generation of second-hand smoke.

Description

Translated fromChinese
一种电干馏型烟草薄片的制备方法A preparation method of electric dry distillation tobacco sheet

技术领域technical field

本发明涉及一种烟草薄片的制备方法,具体地说是一种电干馏型烟草薄片的制备方法。The invention relates to a preparation method of tobacco sheet, in particular to a preparation method of electric dry distillation type tobacco sheet.

背景技术Background technique

烟草薄片是指烟厂将包括打叶工序在内的卷烟制造过程中的烟草废弃料如烟末、烟梗、烟叶碎片、低次烟叶等烟草废弃料作为原料,经过重新组合加工而成的再生烟叶。传统再生烟草薄片是将再生烟叶经过加工与烟草掺配加工方式,卷制成卷烟,可以提高烟叶原料的利用率。由于干馏型卷烟所需要的烟草薄片材质要有一定的厚度,能够浸润一定浓度的香精香料和甘油等易挥发性的物质。而一般工艺生产的烟草薄片,再生烟草薄片的片基厚度以及添加的浓缩物都不能够满足电干馏型卷烟的需求,Tobacco sheet refers to the tobacco waste materials such as tobacco dust, tobacco stems, tobacco leaf fragments, low-grade tobacco leaves and other tobacco waste materials in the cigarette manufacturing process including the leaf threshing process as raw materials, which are recombined and processed. tobacco leaf. The traditional reconstituted tobacco sheet is processed by blending reconstituted tobacco leaves with tobacco, and rolled into cigarettes, which can improve the utilization rate of tobacco leaf raw materials. Because the tobacco sheet material required by dry distillation type cigarettes has a certain thickness, it can infiltrate volatile substances such as flavors and fragrances and glycerin of a certain concentration. However, the tobacco sheet produced by the general process, the base thickness of the regenerated tobacco sheet, and the added concentrate cannot meet the needs of electric dry distillation cigarettes.

发明内容Contents of the invention

本发明的目的是根据现有技术的不足提供一种电干馏型烟草薄片的制备方法,用该制备方法的制备得到的电干馏型烟草薄片具有一定的厚度,可以在较低的温度下,通过较低的电干馏的温度干馏出烟草薄片中添加的香精香料和一些易挥发的香味物质,满足电干馏型卷烟的需要。The object of the present invention is to provide a method for preparing electric dry distillation tobacco sheet according to the deficiencies of the prior art. The electric dry distillation tobacco sheet prepared by the preparation method has a certain thickness and can be passed through The lower electric distillation temperature dry-distills the flavors and fragrances and some volatile flavor substances added in the tobacco sheet to meet the needs of electric dry distillation cigarettes.

本发明是通过如下技术方案实现的:一种电干馏型烟草薄片的制备方法,其步骤包括:(1)将烟草提取物和天然植物提取物中的一种或多种混合得到片基喷涂物;(2)再将片基喷涂物均匀涂布在重量为片基喷涂物1-10倍的烟草薄片片基上然后在40-90℃下干燥;(3)然后按照重量百分数为20-75%的丙二醇、10-45%的甘油、1-10%的去离子水、1-10%的酒精、1-10%的烟用香精和1-10%的烟草提取物混合得到雾化剂香料,将烟草薄片片基重量的2-50%的雾化剂香料喷洒在干燥好的烟草薄片片基上;这是由于电干馏卷烟的温度较低,达不到卷烟燃烧的600℃以上,在抽吸的时候,烟草薄片不能燃烧,需要通过加热将烟草制品中的香味物质干馏出来,为了模拟烟草燃烧过程的的烟雾效果,需要辅助的添加一些雾化剂香料,便于产生可见的烟雾;(4)最后将烟草薄片片基干燥后得到所述电干馏型烟草薄片。The present invention is achieved through the following technical scheme: a preparation method of electric dry distillation tobacco sheet, the steps of which include: (1) mixing one or more of tobacco extract and natural plant extract to obtain a base spray (2) Evenly coat the base spray on the tobacco sheet base with a weight of 1-10 times that of the base spray and then dry it at 40-90°C; % propylene glycol, 10-45% glycerin, 1-10% deionized water, 1-10% alcohol, 1-10% tobacco essence and 1-10% tobacco extract are mixed to obtain aerosol flavor , spray 2-50% of the tobacco sheet base weight of the atomizer flavor on the dried tobacco sheet base; When smoking, the tobacco flakes cannot be burned, and the aroma substances in the tobacco products need to be dry-distilled by heating. In order to simulate the smoke effect of the tobacco burning process, it is necessary to add some atomizer spices to facilitate the generation of visible smoke; ( 4) Finally, the tobacco sheet base is dried to obtain the electric dry distillation tobacco sheet.

优选的,所述烟草薄片片基厚度为0.1-0.5mm。Preferably, the base thickness of the tobacco sheet is 0.1-0.5 mm.

更优选的,所述烟草薄片片基厚度为0.2-0.4mm。More preferably, the base thickness of the tobacco sheet is 0.2-0.4mm.

所述烟草提取物为晾晒烟提取物、香料烟提取物、烤烟提取物、白肋烟提取物、雪茄烟提取物以及烟草废弃料提取物中的一种或多种提取物。所述的烟草提取物可以进行单独提取,主要是为了协调加工好的烟草薄片的口味,具体的实际需求根据实际进行调配。The tobacco extract is one or more extracts of air-cured tobacco extract, oriental tobacco extract, flue-cured tobacco extract, Burley tobacco extract, cigar tobacco extract and tobacco waste extract. The tobacco extract can be extracted separately, mainly for the purpose of coordinating the taste of the processed tobacco flakes, and it can be formulated according to the specific actual needs.

所述烟草提取物通过如下方式中的一种提取:(1)将烟草和质量百分数为95%的乙醇按照质量比烟草:乙醇=1:2-5混合,优选为1:3,浸泡在室温干燥处1周,再过滤在50℃以下浓缩得到烟草提取物,该方法该方法浸泡出的成分主要为一些轻组分,保持烟草轻组分的吸味;(2)将烟草和质量百分数为75%的乙醇按照质量比烟草:乙醇=1:2-5混合,优选为1:3,浸泡在室温干燥处1周,再过滤在50℃以下浓缩得到烟草提取物,该方法浸泡出的成分主要为一些轻组分,保持烟草轻组分中较大极性物质的吸味;(3)将烟草和质量百分数为95%的乙醇按照质量比烟草:乙醇=1:1-4混合,优选为1:2,加热回流1-4小时,优选2小时,再过滤在50℃以下浓缩得到烟草提取物,该方法能够较大程度的提取烟草中的醇溶性物质,较高的温度提取对烟草轻组分中易挥发的物质造成损失;(4)将烟草和质量百分数为75%的乙醇按照质量比烟草:乙醇=1:1-4混合,优选为1:2,加热回流1-4小时,优选2小时,再过滤在50℃以下浓缩得到烟草提取物,该方法能够较大程度的提取烟草中的较大极性物质,较高的温度提取对烟草轻组分中易挥发的物质造成损失。The tobacco extract is extracted by one of the following methods: (1) mix tobacco and ethanol with a mass percentage of 95% according to the mass ratio of tobacco: ethanol = 1:2-5, preferably 1:3, soak at room temperature Dry for 1 week, then filter and concentrate below 50°C to obtain tobacco extract. The components soaked by this method are mainly some light components to keep the smoking flavor of tobacco light components; (2) the tobacco and the mass percentage are 75% ethanol is mixed according to the mass ratio of tobacco: ethanol = 1:2-5, preferably 1:3, soaked in a dry place at room temperature for 1 week, then filtered and concentrated below 50°C to obtain tobacco extract, the ingredients soaked by this method Mainly some light components, to keep the taste of relatively large polar substances in the light components of tobacco; (3) Mix tobacco and ethanol with a mass percentage of 95% according to the mass ratio of tobacco: ethanol = 1:1-4, preferably 1:2, heat and reflux for 1-4 hours, preferably 2 hours, then filter and concentrate below 50°C to obtain tobacco extract. The volatile substances in the light component cause loss; (4) Mix tobacco and ethanol with a mass percentage of 75% according to the mass ratio of tobacco: ethanol = 1:1-4, preferably 1:2, and heat and reflux for 1-4 hours , preferably 2 hours, and then filter and concentrate below 50°C to obtain tobacco extract. This method can extract relatively large polar substances in tobacco to a greater extent, and extraction at a higher temperature will cause damage to volatile substances in tobacco light components. loss.

所述步骤(4)中最后将烟草薄片片基干燥是指在25℃下阴凉干燥处放置2小时。The final drying of the tobacco sheet base in the step (4) refers to placing it in a cool and dry place at 25°C for 2 hours.

所述步骤(1)中干燥好的烟草薄片片基上片基喷涂物含量为150-250g/m2,厚度为0.3-0.4mm,水分的含量为10-12%。In the step (1), the dried tobacco sheet base has a content of 150-250 g/m2 of spray coating on the base, a thickness of 0.3-0.4 mm, and a moisture content of 10-12%.

优选的,所述步骤(1)中将片基喷涂物均匀涂布在重量为片基喷涂物2-8倍的烟草薄片片基上。Preferably, in the step (1), the base spray is evenly coated on the tobacco sheet base whose weight is 2-8 times that of the base spray.

优选的,所述步骤(3)中是将烟草薄片片基重量的5-45%的雾化剂香料喷洒在烟草薄片片基上。Preferably, in the step (3), 5-45% of the weight of the tobacco sheet base is sprayed on the tobacco sheet base with an aerosol spice.

所述步骤(3)中的烟用香精包括天然香料或人工合成香料。如:烃类、醇类、醚类、酚类、含硫化合物、挥发性胺类、醛类、酮类、羧酸类、内酯类或杂环化合物类。The tobacco flavor in the step (3) includes natural flavors or artificial flavors. Such as: hydrocarbons, alcohols, ethers, phenols, sulfur compounds, volatile amines, aldehydes, ketones, carboxylic acids, lactones or heterocyclic compounds.

一种电干馏型烟草薄片的制备方法优选技术方案为:其步骤包括:(1)将烟草提取物和天然植物提取物中的一种或多种混合得到片基喷涂物;(2)再将片基喷涂物均匀涂布在重量为片基喷涂物2-8倍的烟草薄片片基上然后在50-70℃下干燥,得到的烟草薄片片基上片基喷涂物含量为150-250g/m2,厚度为0.3-0.4mm,水分的含量为10-12%;(3)然后按照重量百分数为20-75%的丙二醇、10-45%的甘油、1-10%的去离子水、1-10%的酒精、1-10%的烟用香精和1-10%的烟草提取物混合得到雾化剂香料,将烟草薄片片基重量的5-45%的雾化剂香料喷洒在干燥好的烟草薄片片基上;(4)最后将烟草薄片片基在25℃下阴凉干燥处放置2小时,干燥后得到所述电干馏型烟草薄片。A preferred technical solution for the preparation method of electric dry distillation tobacco sheet is as follows: the steps include: (1) mixing one or more of tobacco extracts and natural plant extracts to obtain a base spray; (2) adding The substrate sprayed material is uniformly coated on the tobacco sheet base whose weight is 2-8 times that of the base sprayed material, and then dried at 50-70°C, and the content of the obtained tobacco sheet base sprayed material is 150-250g/ m2 , the thickness is 0.3-0.4mm, and the water content is 10-12%; (3) Then, according to the weight percentage, it is 20-75% propylene glycol, 10-45% glycerin, 1-10% deionized water, 1-10% alcohol, 1-10% tobacco essence and 1-10% tobacco extract are mixed to obtain an aerosol flavor, and 5-45% of the tobacco sheet basis weight is sprayed on a dry (4) Finally, place the tobacco sheet base in a cool and dry place at 25° C. for 2 hours, and obtain the electric dry distillation tobacco sheet after drying.

本发明提供的电干馏型烟草薄片的制备方法制备出的烟草薄片,能够在电干馏装置中燃烧而产生烟雾。电干馏的方式能够干馏出烟草提取物包含的烟草本香。该种薄片制备工艺制备的薄片具有烟草本香与烟用香精香料浑然一体。满足消费的需求,降低卷烟燃烧对消费者的危害,避免二手烟的产生,具有很强的实用性。The tobacco sheet prepared by the method for preparing electric dry distillation tobacco sheet provided by the present invention can be burned in an electric dry distillation device to generate smoke. The method of electric dry distillation can dry distill the tobacco aroma contained in the tobacco extract. The sheet prepared by the thin sheet preparation process has the natural tobacco flavor and tobacco essence and fragrance in one. It is very practical to meet the needs of consumption, reduce the harm of cigarette burning to consumers, and avoid the generation of second-hand smoke.

具体实施方式Detailed ways

以下通过具体实施例来进一步说明本发明:The present invention is further illustrated below by specific examples:

实施例1Example 1

(1)称取烤烟烟叶100g,加入95%乙醇300g,放在室温下浸泡1周。然后过滤掉烟叶,50℃以下浓缩,得到烟草提取物。(1) Weigh 100g of flue-cured tobacco leaves, add 300g of 95% ethanol, and soak at room temperature for 1 week. Then filter out the tobacco leaves and concentrate below 50°C to obtain tobacco extract.

(2)将提取后的烟草提取物涂布在厚度为0.2mm的烟草薄片片基上,每100g烟草提取物涂布烟草薄片片基400g,在40℃下干燥,得到烟草薄片片基喷涂物含量为200g/m2,厚度为0.35mm,水分含量为11%。(2) Coat the extracted tobacco extract on the tobacco sheet base with a thickness of 0.2mm, coat 400g of the tobacco sheet base per 100g of tobacco extract, and dry at 40°C to obtain the tobacco sheet base spray The content is 200g/m2 , the thickness is 0.35mm, and the moisture content is 11%.

(3)按重量百分数为:丙二醇65%,甘油15%,去离子水3%,酒精5%,天然香料6%,烟草提取物6%混合得到雾化剂香料。然后将雾化剂香料喷洒在已经涂布烟草提取物的烟草薄片片基上,涂布量为100g烟草薄片片基喷洒雾化剂香料的量为15g,即15%的雾化剂香料的量。(3) Percentage by weight: 65% propylene glycol, 15% glycerin, 3% deionized water, 5% alcohol, 6% natural flavor, and 6% tobacco extract are mixed to obtain an atomizer flavor. Then the atomizing agent spice is sprayed on the tobacco sheet base that has been coated with tobacco extract, and the coating amount is 100g tobacco sheet base spraying the amount of atomizer spice being 15g, i.e. the amount of 15% atomizer spice .

(4)将喷洒雾化剂的烟草薄片片基在25℃下阴凉干燥处放置2小时,可以保证雾化剂较好的浸润到烟草薄片中,得到电干馏型烟草薄片1。(4) The tobacco sheet base sprayed with the atomizing agent is placed in a cool and dry place at 25°C for 2 hours to ensure that the atomizing agent is well infiltrated into the tobacco sheet, and the electric dry distillation type tobacco sheet 1 is obtained.

实施例2Example 2

(1)称取晾晒烟烟叶100g,加入75%乙醇200g,放在室温下浸泡1周。然后过滤掉烟叶,50℃以下浓缩,得到烟草提取物。(1) Weigh 100g of air-cured tobacco leaves, add 200g of 75% ethanol, and soak at room temperature for 1 week. Then filter out the tobacco leaves and concentrate below 50°C to obtain tobacco extract.

(2)将提取后的烟草提取物涂布在厚度为0.1mm的烟草薄片片基上,每100g烟草提取物涂布烟草薄片片基100g,在50℃下干燥,得到烟草薄片片基喷涂物含量为250g/m2,厚度为0.3mm,水分含量为10%。(2) Coat the extracted tobacco extract on the tobacco sheet base with a thickness of 0.1mm, coat 100g of the tobacco sheet base per 100g of tobacco extract, and dry at 50°C to obtain the tobacco sheet base spray The content is 250g/m2 , the thickness is 0.3mm, and the moisture content is 10%.

(3)按重量百分数为:丙二醇75%,甘油10%,去离子水1%,酒精10%,人工合成香料1%,烟草提取物5%混合得到雾化剂香料。然后将雾化剂香料喷洒在已经涂布烟草提取物的烟草薄片片基上,涂布量为100g烟草薄片片基喷洒雾化剂香料的量为50g,即50%的雾化剂香料的量。(3) Percentage by weight: 75% propylene glycol, 10% glycerin, 1% deionized water, 10% alcohol, 1% artificial flavor, and 5% tobacco extract are mixed to obtain an atomizer flavor. Then the atomizing agent spice is sprayed on the tobacco sheet base that has been coated with tobacco extract, and the coating amount is 100g tobacco sheet base spraying the amount of atomizer spice being 50g, i.e. the amount of 50% atomizer spice .

(4)将喷洒雾化剂的烟草薄片片基在25℃下阴凉干燥处放置2小时,可以保证雾化剂较好的浸润到烟草薄片中,得到电干馏型烟草薄片2。(4) The tobacco sheet base sprayed with the atomizing agent is placed in a cool and dry place at 25°C for 2 hours to ensure that the atomizing agent is well infiltrated into the tobacco sheet, and the electric carbonization type tobacco sheet 2 is obtained.

实施例3Example 3

(1)称取白肋烟烟叶100g,加入95%乙醇200g,加热冷凝回流条件下萃取1-4小时。然后过滤掉烟叶,50℃以下浓缩,得到烟草提取物。(1) Weigh 100g of Burley tobacco leaves, add 200g of 95% ethanol, and extract for 1-4 hours under the condition of heating, condensing and reflux. Then filter out the tobacco leaves and concentrate below 50°C to obtain tobacco extract.

(2)将提取后的烟草提取物涂布在厚度为0.4mm的烟草薄片片基上,每100g烟草提取物涂布烟草薄片片基1000g,在70℃下干燥,得到烟草薄片片基喷涂物含量为150g/m2,厚度为0.4mm,水分含量为12%。(2) Coat the extracted tobacco extract on the tobacco sheet base with a thickness of 0.4mm, coat 1000g of the tobacco sheet base per 100g of tobacco extract, and dry at 70°C to obtain the tobacco sheet base spray The content is 150g/m2 , the thickness is 0.4mm, and the moisture content is 12%.

(3)按重量百分数为:丙二醇20%,甘油45%,去离子水10%,酒精5%,天然香料10%,烟草提取物10%混合得到雾化剂香料。然后将雾化剂香料喷洒在已经涂布烟草提取物的烟草薄片片基上,涂布量为100g烟草薄片片基喷洒雾化剂香料的量为2g,即2%的雾化剂香料的量。(3) Percentage by weight: 20% propylene glycol, 45% glycerin, 10% deionized water, 5% alcohol, 10% natural flavor, and 10% tobacco extract are mixed to obtain an atomizer flavor. Then the atomizing agent flavoring is sprayed on the tobacco sheet base that has been coated with tobacco extract, and the coating amount is that the amount of spraying the atomizing agent flavoring on the 100g tobacco sheet base is 2g, i.e. the amount of 2% atomizing agent flavoring .

(4)将喷洒雾化剂的烟草薄片片基在25℃下阴凉干燥处放置2小时,可以保证雾化剂较好的浸润到烟草薄片中,得到电干馏型烟草薄片3。(4) The tobacco sheet base sprayed with the atomizing agent is placed in a cool and dry place at 25°C for 2 hours to ensure that the atomizing agent is well infiltrated into the tobacco sheet, and the electric dry distillation type tobacco sheet 3 is obtained.

实施例4Example 4

(1)称取白肋烟烟叶和香料烟烟叶共100g,加入75%乙醇200g,加热冷凝回流条件下萃取1-4小时。然后过滤掉烟叶,50℃以下浓缩,得到烟草提取物。(1) Weigh 100 g of Burley tobacco leaves and oriental tobacco leaves in total, add 200 g of 75% ethanol, and extract under heating, condensing and reflux conditions for 1-4 hours. Then filter out the tobacco leaves and concentrate below 50°C to obtain tobacco extract.

(2)将提取后的烟草提取物涂布在厚度为0.5mm的烟草薄片片基上,每100g烟草提取物涂布烟草薄片片基200g,在90℃下干燥,得到烟草薄片片基喷涂物含量为200g/m2,厚度为0.4mm,水分含量为12%。(2) Coat the extracted tobacco extract on the tobacco sheet base with a thickness of 0.5mm, coat 200g of the tobacco sheet base per 100g of tobacco extract, and dry at 90°C to obtain the sprayed tobacco sheet base The content is 200g/m2 , the thickness is 0.4mm, and the moisture content is 12%.

(3)按重量百分数为:丙二醇58%,甘油30%,去离子水5%,酒精1%,人工合成香料5%,烟草提取物1%混合得到雾化剂香料。然后将雾化剂香料喷洒在已经涂布烟草提取物的烟草薄片片基上,涂布量为100g烟草薄片片基喷洒雾化剂香料的量为45g,即45%的雾化剂香料的量。(3) Percentage by weight: 58% propylene glycol, 30% glycerin, 5% deionized water, 1% alcohol, 5% artificial flavor, and 1% tobacco extract are mixed to obtain an atomizer flavor. Then the atomizing agent spice is sprayed on the tobacco sheet base that has been coated with tobacco extract, and the coating amount is that the amount of spraying atomizer spice on the 100g tobacco sheet base is 45g, i.e. the amount of 45% atomizer spice .

(4)将喷洒雾化剂的烟草薄片片基在25℃下阴凉干燥处放置2小时,可以保证雾化剂较好的浸润到烟草薄片中,得到电干馏型烟草薄片4。(4) The tobacco sheet base sprayed with the atomizing agent is placed in a cool and dry place at 25°C for 2 hours to ensure that the atomizing agent is well infiltrated into the tobacco sheet, and the electric dry distillation type tobacco sheet 4 is obtained.

实施例5Example 5

(1)称取雪茄烟烟叶和烟草废弃料共100g,加入75%乙醇200g,加热冷凝回流条件下萃取1-4小时。然后过滤掉烟叶,50℃以下浓缩,得到烟草提取物。(1) Weigh 100g of cigar tobacco leaves and tobacco waste in total, add 200g of 75% ethanol, and extract under heating, condensing and reflux conditions for 1-4 hours. Then filter out the tobacco leaves and concentrate below 50°C to obtain tobacco extract.

(2)将提取后的烟草提取物涂布在厚度为0.5mm的烟草薄片片基上,每100g烟草提取物涂布烟草薄片片基200g,在90℃下干燥,得到烟草薄片片基喷涂物含量为200g/m2,厚度为0.4mm,水分含量为12%。(2) Coat the extracted tobacco extract on the tobacco sheet base with a thickness of 0.5mm, coat 200g of the tobacco sheet base per 100g of tobacco extract, and dry at 90°C to obtain the sprayed tobacco sheet base The content is 200g/m2 , the thickness is 0.4mm, and the moisture content is 12%.

(3)按重量百分数为:丙二醇58%,甘油30%,去离子水5%,酒精1%,烟用香精5%,烟草提取物1%混合得到雾化剂香料。然后将雾化剂香料喷洒在已经涂布烟草提取物的烟草薄片片基上,涂布量为100g烟草薄片片基喷洒雾化剂香料的量为45g,即45%的雾化剂香料的量。(3) Percentage by weight: 58% propylene glycol, 30% glycerin, 5% deionized water, 1% alcohol, 5% tobacco essence, and 1% tobacco extract are mixed to obtain an atomizer fragrance. Then the atomizing agent spice is sprayed on the tobacco sheet base that has been coated with tobacco extract, and the coating amount is that the amount of spraying atomizer spice on the 100g tobacco sheet base is 45g, i.e. the amount of 45% atomizer spice .

(4)将喷洒雾化剂的烟草薄片片基在25℃下阴凉干燥处放置2小时,可以保证雾化剂较好的浸润到烟草薄片中,得到电干馏型烟草薄片5。(4) The tobacco sheet base sprayed with the atomizing agent is placed in a cool and dry place at 25°C for 2 hours to ensure that the atomizing agent is well infiltrated into the tobacco sheet, and the electric carbonization type tobacco sheet 5 is obtained.

实施例6Example 6

(1)称取烤烟烟叶100g,加入95%乙醇300g,放在室温下浸泡1周。然后过滤掉烟叶,在50℃以下浓缩,得到烟草提取物(1) Weigh 100g of flue-cured tobacco leaves, add 300g of 95% ethanol, and soak at room temperature for 1 week. The tobacco leaves are then filtered and concentrated below 50°C to obtain tobacco extract

称取雪茄烟烟叶100g,加入95%乙醇200g,加热冷凝回流条件下萃取2小时,冷却、过滤掉烟叶,在50℃以下浓缩,得到一定浓度的浸泡烤烟烟草提取物,备用。Weigh 100g of cigar tobacco leaves, add 200g of 95% ethanol, extract under heating and condensing reflux for 2 hours, cool, filter out the tobacco leaves, concentrate below 50°C to obtain a certain concentration of soaked flue-cured tobacco extract, and set aside.

(2)将两种提取方法的烟草提取物按照1:1的比例调配后,涂布在烟草薄片片基上,每100g烟草提取物涂布烟草薄片400g,在70℃下干燥,得到烟草薄片片基喷涂物含量为200g/m2,厚度为0.4mm,水分含量为11%。(2) After blending the tobacco extracts of the two extraction methods according to the ratio of 1:1, they are coated on the base of the tobacco sheet, and 400g of the tobacco sheet is coated with each 100g of tobacco extract, and dried at 70°C to obtain the tobacco sheet The content of sprayed matter on the film base is 200g/m2 , the thickness is 0.4mm, and the moisture content is 11%.

(3)按重量百分数为:丙二醇58%,甘油30%,去离子水5%,酒精1%,烟用香精5%,烟草提取物1%混合得到雾化剂香料。然后将雾化剂香料喷洒在已经涂布烟草提取物的烟草薄片片基上,涂布量为100g烟草薄片片基喷洒雾化剂香料的量为45g,即45%的雾化剂香料的量。(3) Percentage by weight: 58% propylene glycol, 30% glycerin, 5% deionized water, 1% alcohol, 5% tobacco essence, and 1% tobacco extract are mixed to obtain an atomizer fragrance. Then the atomizing agent spice is sprayed on the tobacco sheet base that has been coated with tobacco extract, and the coating amount is that the amount of spraying atomizer spice on the 100g tobacco sheet base is 45g, i.e. the amount of 45% atomizer spice .

(4)将喷洒雾化剂的烟草薄片片基在25℃下阴凉干燥处放置2小时,可以保证雾化剂较好的浸润到烟草薄片中,得到电干馏型烟草薄片6。(4) The tobacco sheet base sprayed with the atomizing agent is placed in a cool and dry place at 25°C for 2 hours to ensure that the atomizing agent is well infiltrated into the tobacco sheet, and the electric carbonization type tobacco sheet 6 is obtained.

将上述烟草薄片切丝后放置在电干馏装置中进行感官和雾化量评价,得到的结果如表1所示。The above-mentioned tobacco thin slices were shredded and placed in an electric dry distillation device for sensory evaluation and atomization evaluation. The results are shown in Table 1.

Figure BDA0000303318071
Figure BDA0000303318071

表1 烟草薄片在电干馏装置中的感官和雾化量评价Table 1 Sensory and atomization evaluation of tobacco sheet in electric dry distillation device

从上述评价可以看出,本发明方法制备得到的电干馏型烟草薄片感官效果好。It can be seen from the above evaluation that the electric dry distillation tobacco sheet prepared by the method of the present invention has a good sensory effect.

Claims (10)

1. the preparation method of an electric destructive distillation type reconstituted tobacoo, its step comprises: (1) obtains sheet base spray with one or more mixing in tobacco extract and the natural plant extracts; (2) it is dry down at 40-90 ℃ then on the sheet base spray 1-10 reconstituted tobacoo sheet base doubly sheet base spray being uniformly coated on weight again; (3) be that the glycerine of propane diols, the 10-45% of 20-75%, the deionized water of 1-10%, the alcohol of 1-10%, the flavouring essence for tobacco of 1-10% and the tobacco extract of 1-10% mix atomized dose of spices according to percetage by weight then, the Alevaire spices of the 2-50% of reconstituted tobacoo sheet basic weight amount is sprayed on the dry good reconstituted tobacoo sheet base; (4) obtain described electric destructive distillation type reconstituted tobacoo after at last reconstituted tobacoo sheet backbone is dry.
2. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: described reconstituted tobacoo sheet base thickness is 0.1-0.5mm.
3. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 2, it is characterized in that: described reconstituted tobacoo sheet base thickness is 0.2-0.4mm.
4. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: described tobacco extract is one or more extracts in airing tobacco extract, Turkish tobaccos extract, flue-cured tobacco extract, burley tobaccos extract, cigar extract and the tobacco dead meal extract.
5. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: a kind of extraction of described tobacco extract in the following way: (1) is 95% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:2-5 mixes, be immersed in 1 week of drying at room temperature place, refilter at the concentrated tobacco extract that obtains below 50 ℃; (2) be 75% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:2-5 mixes, and is immersed in 1 week of drying at room temperature place, refilters concentrating below 50 ℃ and obtains tobacco extract; (3) be 95% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:1-4 mixes, and adds hot reflux 1-4 hour, refilters concentrating below 50 ℃ and obtains tobacco extract; (4) be 75% ethanol with tobacco and mass percent according to quality than tobacco: ethanol=1:1-4 mixes, and adds hot reflux 1-4 hour, refilters concentrating below 50 ℃ and obtains tobacco extract.
6. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: in the described step (4) at last with reconstituted tobacoo sheet backbone dry refer to 25 ℃ down shady and cool dry place placed 2 hours.
7. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: the dry good basic spray content of reconstituted tobacoo sheet base last slice is 150-250g/m in the described step (1)2, thickness is 0.3-0.4mm, the content of moisture is 10-12%.
8. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: in the described step (1) sheet base spray being uniformly coated on weight is on the sheet base spray 2-8 reconstituted tobacoo sheet base doubly.
9. according to the preparation method of the described electric destructive distillation type reconstituted tobacoo of claim 1, it is characterized in that: be that Alevaire spices with the 5-45% of reconstituted tobacoo sheet basic weight amount is sprayed on the reconstituted tobacoo sheet base in the described step (3).
10. the preparation method of the described electric destructive distillation type reconstituted tobacoo of described claim 1 is characterized in that: the flavouring essence for tobacco in the described step (3) comprises natural perfume material or artificial synthetic perfume.
CN201310123050.4A2013-04-102013-04-10A kind of preparation method of electric destructive distillation type reconstituted tobacooActiveCN103181613B (en)

Priority Applications (1)

Application NumberPriority DateFiling DateTitle
CN201310123050.4ACN103181613B (en)2013-04-102013-04-10A kind of preparation method of electric destructive distillation type reconstituted tobacoo

Applications Claiming Priority (1)

Application NumberPriority DateFiling DateTitle
CN201310123050.4ACN103181613B (en)2013-04-102013-04-10A kind of preparation method of electric destructive distillation type reconstituted tobacoo

Publications (2)

Publication NumberPublication Date
CN103181613Atrue CN103181613A (en)2013-07-03
CN103181613B CN103181613B (en)2015-10-21

Family

ID=48673271

Family Applications (1)

Application NumberTitlePriority DateFiling Date
CN201310123050.4AActiveCN103181613B (en)2013-04-102013-04-10A kind of preparation method of electric destructive distillation type reconstituted tobacoo

Country Status (1)

CountryLink
CN (1)CN103181613B (en)

Cited By (14)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
CN103919268A (en)*2014-03-282014-07-16广东中烟工业有限责任公司Cigarette without generating secondhand smoke
CN103919270A (en)*2014-03-282014-07-16广东中烟工业有限责任公司Tobacco product
CN105219530A (en)*2015-10-082016-01-06中烟施伟策(云南)再造烟叶有限公司A kind of tobacco spice preparation method reinforced for reconstituted tobacco
CN105996111A (en)*2016-07-202016-10-12湖北中烟工业有限责任公司Fragrance-keeping method for increasing quality of tobacco leaves reprocessed through paper-making process
WO2017181685A1 (en)2016-04-202017-10-26贵州中烟工业有限责任公司Method for manufacturing heat-not-burn tobacco substrate containing activated carbon
CN107319641A (en)*2017-07-212017-11-07上海烟草集团有限责任公司A kind of tobacco fuming liquids for heating the tobacco product that do not burn and its production and use
CN109875096A (en)*2017-12-062019-06-14湖北中烟工业有限责任公司 Tobacco sheet feeding process for a new type of tobacco product
AU2018204476A1 (en)*2018-05-122019-11-28Shenzhen Dakavape Tech Co., Ltd.Dual-use cigarette and tobacco filler thereof
CN110679984A (en)*2019-11-152020-01-14湖北中烟工业有限责任公司 A kind of preparation method of special sheet for heating cigarette
CN111096472A (en)*2018-10-102020-05-05云南巴菰生物科技有限公司A synthetic tobacco shred containing Chinese herbal materials and its preparation method
JP2022510056A (en)*2019-11-202022-01-26ケーティー・アンド・ジー・コーポレーション Aerosol-producing articles comprising a method and an apparatus for manufacturing an aerosol-producing rod and an aerosol-producing rod produced by the method and the apparatus.
ES2898232R1 (en)*2019-01-282022-03-09Broadfar Shanghai Man Consulting Co Ltd HEATING CIGARETTE WITHOUT COMBUSTION AND METHOD OF MANUFACTURING THE SAME
CN114532573A (en)*2022-02-182022-05-27上海烟草集团有限责任公司Auxiliary material spraying system and coating method for improving utilization rate of auxiliary materials of reconstituted tobacco
JP2023171941A (en)*2020-08-252023-12-05ケーティー アンド ジー コーポレイション Flavor-containing sheet containing modified cellulose and smoking article containing the same

Citations (10)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
EP0056308B1 (en)*1981-01-071986-05-28Philip Morris IncorporatedReconstituted tobacco smoking material and method for its production
JPS6214772A (en)*1985-07-101987-01-23中島 三夫Innoxious tobacco
RU2289981C1 (en)*2005-07-082006-12-27Олег Иванович КвасенковMethod for producing of aromatized exploded tobacco vein
CN1907149A (en)*2006-07-312007-02-07福建省安溪县铁观音文化传播有限公司Method for manufacturing tealamina for cigarette
WO2008110932A2 (en)*2007-03-092008-09-18Philip Morris Products S.A.Methods of making reconstituted tobacco sheets
CN101912147A (en)*2010-07-302010-12-15华南理工大学 Functional tobacco sheet and preparation method thereof
CN101926506A (en)*2009-06-192010-12-29李文博Application of neophytadiene being taken as cigarette additive
CN102217782A (en)*2010-04-152011-10-19厦门中海钓台生物工程有限公司Tea leaf thin sheet for cigarette, preparation method thereof and cigarette
CN102217789A (en)*2010-04-152011-10-19厦门中海钓台生物工程有限公司Thin sheet for cigarette, preparation method thereof and cigarette
CN102934837A (en)*2012-11-092013-02-20红云红河烟草(集团)有限责任公司Preparation method of mixed reconstituted tobacco with burley tobacco style

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
EP0056308B1 (en)*1981-01-071986-05-28Philip Morris IncorporatedReconstituted tobacco smoking material and method for its production
JPS6214772A (en)*1985-07-101987-01-23中島 三夫Innoxious tobacco
RU2289981C1 (en)*2005-07-082006-12-27Олег Иванович КвасенковMethod for producing of aromatized exploded tobacco vein
CN1907149A (en)*2006-07-312007-02-07福建省安溪县铁观音文化传播有限公司Method for manufacturing tealamina for cigarette
WO2008110932A2 (en)*2007-03-092008-09-18Philip Morris Products S.A.Methods of making reconstituted tobacco sheets
CN101926506A (en)*2009-06-192010-12-29李文博Application of neophytadiene being taken as cigarette additive
CN102217782A (en)*2010-04-152011-10-19厦门中海钓台生物工程有限公司Tea leaf thin sheet for cigarette, preparation method thereof and cigarette
CN102217789A (en)*2010-04-152011-10-19厦门中海钓台生物工程有限公司Thin sheet for cigarette, preparation method thereof and cigarette
CN101912147A (en)*2010-07-302010-12-15华南理工大学 Functional tobacco sheet and preparation method thereof
CN102934837A (en)*2012-11-092013-02-20红云红河烟草(集团)有限责任公司Preparation method of mixed reconstituted tobacco with burley tobacco style

Cited By (19)

* Cited by examiner, † Cited by third party
Publication numberPriority datePublication dateAssigneeTitle
CN103919268A (en)*2014-03-282014-07-16广东中烟工业有限责任公司Cigarette without generating secondhand smoke
CN103919270A (en)*2014-03-282014-07-16广东中烟工业有限责任公司Tobacco product
CN103919268B (en)*2014-03-282016-03-30广东中烟工业有限责任公司A kind of cigarette not producing second-hand-cigarette
CN103919270B (en)*2014-03-282016-08-17广东中烟工业有限责任公司 a cigarette product
CN105219530A (en)*2015-10-082016-01-06中烟施伟策(云南)再造烟叶有限公司A kind of tobacco spice preparation method reinforced for reconstituted tobacco
EP3263276A4 (en)*2016-04-202018-12-05China Tobacco Guizhou Industrial Co., Ltd.Method for manufacturing heat-not-burn tobacco substrate containing activated carbon
WO2017181685A1 (en)2016-04-202017-10-26贵州中烟工业有限责任公司Method for manufacturing heat-not-burn tobacco substrate containing activated carbon
CN105996111A (en)*2016-07-202016-10-12湖北中烟工业有限责任公司Fragrance-keeping method for increasing quality of tobacco leaves reprocessed through paper-making process
CN107319641A (en)*2017-07-212017-11-07上海烟草集团有限责任公司A kind of tobacco fuming liquids for heating the tobacco product that do not burn and its production and use
CN109875096A (en)*2017-12-062019-06-14湖北中烟工业有限责任公司 Tobacco sheet feeding process for a new type of tobacco product
AU2018204476A1 (en)*2018-05-122019-11-28Shenzhen Dakavape Tech Co., Ltd.Dual-use cigarette and tobacco filler thereof
CN111096472A (en)*2018-10-102020-05-05云南巴菰生物科技有限公司A synthetic tobacco shred containing Chinese herbal materials and its preparation method
ES2898232R1 (en)*2019-01-282022-03-09Broadfar Shanghai Man Consulting Co Ltd HEATING CIGARETTE WITHOUT COMBUSTION AND METHOD OF MANUFACTURING THE SAME
CN110679984A (en)*2019-11-152020-01-14湖北中烟工业有限责任公司 A kind of preparation method of special sheet for heating cigarette
JP2022510056A (en)*2019-11-202022-01-26ケーティー・アンド・ジー・コーポレーション Aerosol-producing articles comprising a method and an apparatus for manufacturing an aerosol-producing rod and an aerosol-producing rod produced by the method and the apparatus.
JP7164269B2 (en)2019-11-202022-11-01ケーティー アンド ジー コーポレイション Aerosol-generating articles and methods of making aerosol-generating rods
JP2023171941A (en)*2020-08-252023-12-05ケーティー アンド ジー コーポレイション Flavor-containing sheet containing modified cellulose and smoking article containing the same
JP7664988B2 (en)2020-08-252025-04-18ケーティー アンド ジー コーポレイション Flavor-containing sheet containing modified cellulose and smoking article containing the same
CN114532573A (en)*2022-02-182022-05-27上海烟草集团有限责任公司Auxiliary material spraying system and coating method for improving utilization rate of auxiliary materials of reconstituted tobacco

Also Published As

Publication numberPublication date
CN103181613B (en)2015-10-21

Similar Documents

PublicationPublication DateTitle
CN103181613B (en)A kind of preparation method of electric destructive distillation type reconstituted tobacoo
CN109288137B (en)Preparation method and application of tobacco shreds added with atomizing agent
CN108451001B (en) A kind of dry-process reconstituted tobacco leaf for heat-not-burn cigarette and preparation method thereof
CN104041935B (en)A kind of extracting method of electronic cigarette Chinese style flue-cured tobacco odor type style tobacco juice
CN107846963A (en)Aerosol generates material and includes its device
CN103750535A (en)Preparation method of heating non-combustion type cigarette block
CN110839947B (en)Extraction process of plant spice for cigarette without burning under heating
CN105112161B (en)A kind of flavoring essence of cigar cigarette paper
CN104531356B (en)Sweet fragrant additive and the electronic cigarette liquid with sweet perfume
CN104041936A (en)Method for extracting Chinese style mixed-fragrance cigarette juice for electronic cigarette
CN108968139A (en)The reconstituted tobacoo and production technology of the high porosity with the fragrance of a flower applied to low temperature cigarette
CN104783323B (en)A kind of tobacco juice for electronic smoke containing Dry distillated flavor
CN107183779A (en)The low temperature cigarette reconstituted tobacco prepared based on inorganic salts
CN108618188B (en)Preparation method of microporous cut tobacco applicable to low-temperature cigarettes
CN110257172A (en)Coating medium is fragrant, coating fluid and heating are not burnt cigarette
CN104178344A (en)Tobacco hydrolat as well as preparation method and application thereof
CN113795156B (en)Liquid tobacco extract, method of making and aerosol-generating article comprising the liquid tobacco extract
CN110506970A (en) A method for preparing a core base material of a heat-not-burn cigarette
CN108576912A (en)The reconstituted tobacoo and its production technology of a kind of metal-containing powders applied to low temperature cigarette
CN108926030A (en)A kind of tobacco style leaf composition for multiple heating mode cigarette, multiple heating mode cigarette and preparation method thereof
CN106381225A (en)Nut-flavored cigarette midline adhesive essence, and preparation method and application thereof
JP2022535507A (en) METHOD OF PRODUCING IMPROVED LIQUID TOBACCO EXTRACT
CN110236232A (en) A kind of electronic cigarette oil prepared by using tobacco leaf extract Maillard reaction product
CN108887726A (en)A kind of electric heating cigarette flavoring essence and its preparation method and application increasing this perfume of tobacco
CN102907757A (en)Preparation method of mixed reconstituted tobacco with partial sun-cured tobacco style

Legal Events

DateCodeTitleDescription
C06Publication
PB01Publication
C10Entry into substantive examination
SE01Entry into force of request for substantive examination
C14Grant of patent or utility model
GR01Patent grant

[8]ページ先頭

©2009-2025 Movatter.jp