技术领域technical field
本发明涉及一种电子烟烟液及其制备方法，具体地指一种淡雅香型电子烟雾化烟液及其制备方法。The invention relates to an electronic cigarette liquid and a preparation method thereof, in particular to an elegant and fragrant electronic smoke liquid and a preparation method thereof.
背景技术Background technique
降焦减害一直是烟草行业的重点课题，近年来，随着社会各界对吸烟与健康关系的日益重视，控烟行动已经在很多地方兴起，公共场合全面禁烟法规的出台，给香烟的市场的冲击和对香烟品质的提高都提出了新的要求。Reducing tar and reducing harm has always been a key issue in the tobacco industry. In recent years, with the increasing emphasis on the relationship between smoking and health from all walks of life in the society, tobacco control actions have emerged in many places. The introduction of comprehensive smoking bans in public places has had an impact on the cigarette market. New requirements have been put forward for the improvement of cigarette quality.
香烟的消费方式主要是香烟燃烧产生的烟气进行的，烟气容易引起吸烟者患上各种呼吸系统疾病，例如气管炎、支气管炎、咽炎、咳嗽痰多等症状。为了降低吸烟的危害，电子烟于2005年在中国发明，它尼古丁替代疗法，得到广大吸烟者的认可。电子烟是将含有烟碱和香精的溶液雾化成微粒，通过肺部吸收，同时吐出模拟烟雾，而不含香烟中的焦油和其他有害成分，也不会产生二手烟亦不会弥漫或缭绕在密闭空间中；而传统香烟是以烟叶或烟草点火燃烧，同时危害了吸烟者与非吸烟者的健康。Cigarette consumption is mainly carried out by the smoke generated by burning cigarettes, which can easily cause smokers to suffer from various respiratory diseases, such as bronchitis, bronchitis, pharyngitis, cough and phlegm and other symptoms. In order to reduce the harm of smoking, electronic cigarette was invented in China in 2005. Its nicotine replacement therapy has been recognized by the majority of smokers. E-cigarettes atomize a solution containing nicotine and essence into particles, absorb it through the lungs, and at the same time spit out simulated smoke without tar and other harmful components in cigarettes, and will not produce second-hand smoke and will not permeate or linger in the air. In a confined space; while traditional cigarettes are ignited and burned with tobacco leaves or tobacco, which endangers the health of smokers and non-smokers.
但是电子烟虽然能降低吸烟的危害，却无法改善吸烟者咽喉及肺部的不适。However, although e-cigarettes can reduce the harm of smoking, they cannot improve the discomfort of smokers' throats and lungs.
发明内容Contents of the invention
本发明的目的在于克服现有电子烟的不足，提供一种能满足烟民的吸烟需求，同时又能起到止咳提神功效，增加喉部舒适感的淡雅香型电子烟雾化烟液及其制备方法。The purpose of the present invention is to overcome the deficiencies of the existing electronic cigarettes, and provide a light-flavored electronic cigarette liquid that can meet the smoking needs of smokers, and at the same time have the effect of relieving cough and refreshing, increasing the comfort of the throat and its preparation method.
为实现上述目的，本发明所提供的淡雅香型电子烟雾化烟液，其组分及重量百分比含量为：丙二醇30~45%，甘油20~35%，去离子水5~15%，酒精5~15%，中药药液15~45%，烟用香精2~5%，烟草提取物2~6%，成型剂0.1~2%，其中，所述中药药液是用水蒸馏提取或乙醇萃取中药混合物所获得的提取液，所述中药混合物中各组分的重量百分比为：川贝母0.1%~50%、薄荷叶0.1%~50%、枇杷叶0.1%~50%、神农香菊0.1%~50%、紫罗兰0.1%~50%、桂花0.1%~50%、绿茶0.1%~50%。In order to achieve the above-mentioned purpose, the components and weight percentages of the light-flavored e-cigarette liquid provided by the present invention are as follows: 30-45% propylene glycol, 20-35% glycerin, 5-15% deionized water, 5% alcohol ~15%, Chinese medicine liquid 15~45%, tobacco essence 2~5%, tobacco extract 2~6%, molding agent 0.1~2%, wherein, the Chinese medicine liquid is distilled with water or extracted with ethanol For the extract obtained from the mixture, the percentages by weight of the components in the traditional Chinese medicine mixture are: Fritillaria 0.1%-50%, mint leaves 0.1%-50%, loquat leaves 0.1%-50%, Shennong Xiangju 0.1% ~50%, Violet 0.1%~50%, Osmanthus 0.1%~50%, Green Tea 0.1%~50%.
优选地，所述中药混合物各组分的重量百分比为：川贝母1%~20%、薄荷叶1%~20%、枇杷叶1%~20%、神农香菊1%~20%、紫罗兰1%~20%、桂花1%~20%、绿茶1%~20%。Preferably, the weight percentages of the components of the traditional Chinese medicine mixture are: Fritillaria 1%-20%, mint leaves 1%-20%, loquat leaves 1%-20%, Shennong chrysanthemum 1%-20%, violet 1%~20%, osmanthus 1%~20%, green tea 1%~20%.
优选地，所述成型剂为海藻酸钠、琼脂、黄原胶和酪蛋白酸钠中的一种或几种的混合物。Preferably, the forming agent is one or a mixture of sodium alginate, agar, xanthan gum and sodium caseinate.
结合上述优选范围，所述淡雅香型电子烟雾化烟液更好的组分及重量百分比含量为：丙二醇30%，甘油25%，去离子水10%，酒精10%，中药药液17%，烟用香精3%，烟草提取物5%，成型剂0.1%，其中，所述中药药液是用水蒸馏提取或乙醇萃取中药混合物所获得的提取液，所述中药混合物中各组分的重量百分比为：川贝母13.3%、薄荷叶10%、枇杷叶16.7%、神农香菊13.3%、紫罗兰13.3%、桂花16.7%、绿茶16.7%。Combining the above preferred ranges, the more preferable components and weight percentages of the elegant and fragrant electronic cigarette liquid are: 30% propylene glycol, 25% glycerin, 10% deionized water, 10% alcohol, 17% traditional Chinese medicine liquid, Tobacco essence 3%, tobacco extract 5%, forming agent 0.1%, wherein, the traditional Chinese medicine liquid is the extract obtained by water distillation extraction or ethanol extraction of the Chinese medicine mixture, and the weight percentage of each component in the Chinese medicine mixture Contains: Chuan Fritillaria 13.3%, Mint Leaf 10%, Loquat Leaf 16.7%, Shennong Fragrant Chrysanthemum 13.3%, Violet 13.3%, Osmanthus 16.7%, Green Tea 16.7%.
本发明还提供了一种淡雅香型电子烟雾化烟液的制备方法，其原料的重量百分比组成为：丙二醇30~45%，甘油20~35%，去离子水5~15%，酒精5~15%，中药药液15~45%，烟用香精2~5%，烟草提取物2~6%，成型剂0.1~2%，其中，所述中药药液是用水蒸馏提取或乙醇萃取中药混合物所获得的提取液，所述中药混合物中各组分的重量百分比为：川贝母0.1%~50%、薄荷叶0.1%~50%、枇杷叶0.1%~50%、神农香菊0.1%~50%、紫罗兰0.1%~50%、桂花0.1%~50%、绿茶0.1%~50%；The present invention also provides a method for preparing an elegant-flavored e-cigarette liquid. The raw materials are composed of 30-45% propylene glycol, 20-35% glycerin, 5-15% deionized water, and 5-5% alcohol. 15%, Chinese medicinal liquid 15-45%, tobacco essence 2-5%, tobacco extract 2-6%, forming agent 0.1-2%, wherein, the traditional Chinese medicinal liquid is distilled with water or extracted with ethanol. For the obtained extract, the percentage by weight of each component in the traditional Chinese medicine mixture is: Fritillaria 0.1%~50%, mint leaves 0.1%~50%, loquat leaves 0.1%~50%, Shennong Xiangju 0.1%~ 50%, violet 0.1%~50%, osmanthus 0.1%~50%, green tea 0.1%~50%;
制备步骤如下：The preparation steps are as follows:
1）去离子水加热到60℃，加入成型剂，搅拌并继续加热至85~95℃，使成型剂完全溶解得到成型剂水溶液；1) Heat the deionized water to 60°C, add the molding agent, stir and continue heating to 85~95°C to completely dissolve the molding agent to obtain an aqueous solution of the molding agent;
2）取丙二醇和甘油搅拌混合均匀，然后将成型剂水溶液加入后，保持在80℃搅拌均匀得到成型剂溶剂混合液，保温备用；2) Stir and mix propylene glycol and glycerin evenly, then add the forming agent aqueous solution, keep stirring at 80°C to obtain a forming agent solvent mixture, keep warm for later use;
3）将中药药液，烟用香精和烟草提取物一并溶于酒精中，搅拌均匀得到中药烟草混合液，备用；3) Dissolve the Chinese medicinal liquid, tobacco essence and tobacco extract in alcohol, and stir evenly to obtain a Chinese medicinal tobacco mixture, which is set aside;
4）将中药烟草混合液倒入成型剂溶剂混合液中，不断搅拌，使其温度降至室温，制得淡雅香型保健电子烟雾化烟液。4) Pour the mixture of traditional Chinese medicine and tobacco into the mixture of forming agent and solvent, and keep stirring to make the temperature drop to room temperature, so as to prepare the light and fragrant health-care electronic cigarette liquid.
优选地，所述中药混合物各组分的重量百分比为：川贝母1%~20%、薄荷叶1%~20%、枇杷叶1%~20%、神农香菊1%~20%、紫罗兰1%~20%、桂花1%~20%、绿茶1%~20%。Preferably, the weight percentages of the components of the traditional Chinese medicine mixture are: Fritillaria 1%-20%, mint leaves 1%-20%, loquat leaves 1%-20%, Shennong chrysanthemum 1%-20%, violet 1%~20%, osmanthus 1%~20%, green tea 1%~20%.
优选地，所述成型剂为海藻酸钠、琼脂、黄原胶和酪蛋白酸钠中的一种或几种的混合物。Preferably, the forming agent is one or a mixture of sodium alginate, agar, xanthan gum and sodium caseinate.
优选地，所述中药药液的制备方法为：利用50%~95%乙醇提取中药混合物，提取时间为2~6小时，提取所得溶液用0.2~0.8个微米的膜过滤，然后减压浓缩，制得中药药液。Preferably, the preparation method of the traditional Chinese medicine liquid is: using 50%~95% ethanol to extract the Chinese medicine mixture, the extraction time is 2~6 hours, the extracted solution is filtered with a membrane of 0.2~0.8 microns, and then concentrated under reduced pressure, Prepare the traditional Chinese medicine liquid.
更优选地，所述中药药液的制备方法为：利用70%~95%乙醇提取中药混合物，提取时间为3~4小时，提取所得溶液用0.2~0.8个微米的膜过滤，然后减压浓缩，制得中药药液。More preferably, the preparation method of the traditional Chinese medicinal liquid is as follows: using 70%~95% ethanol to extract the Chinese medicinal mixture, the extraction time is 3~4 hours, the extracted solution is filtered with a membrane of 0.2~0.8 microns, and then concentrated under reduced pressure , to prepare traditional Chinese medicine liquid.
结合上述优选范围，所述淡雅香型电子烟雾化烟液更好的组分及重量百分比含量为：丙二醇30%，甘油25%，去离子水10%，酒精10%，中药药液17%，烟用香精3%，烟草提取物5%，成型剂0.1%，其中，所述中药药液是用水蒸馏提取或乙醇萃取中药混合物所获得的提取液，所述中药混合物中各组分的重量百分比为：川贝母13.3%、薄荷叶10%、枇杷叶16.7%、神农香菊13.3%、紫罗兰13.3%、桂花16.7%、绿茶16.7%。Combining the above preferred ranges, the more preferable components and weight percentages of the elegant and fragrant electronic cigarette liquid are: 30% propylene glycol, 25% glycerin, 10% deionized water, 10% alcohol, 17% traditional Chinese medicine liquid, Tobacco essence 3%, tobacco extract 5%, forming agent 0.1%, wherein, the traditional Chinese medicine liquid is the extract obtained by water distillation extraction or ethanol extraction of the Chinese medicine mixture, and the weight percentage of each component in the Chinese medicine mixture Contains: Chuan Fritillaria 13.3%, Mint Leaf 10%, Loquat Leaf 16.7%, Shennong Fragrant Chrysanthemum 13.3%, Violet 13.3%, Osmanthus 16.7%, Green Tea 16.7%.
上述雾化烟液中的成型剂的主要更能是提高电子烟烟液的粘度，防止烟液在实用过程中，会过多的流入到电子烟雾化器当中，引起雾化效果低等问题的存在。同时，提高电子烟烟液的粘度也能够方便运输和保存。The main function of the forming agent in the above-mentioned atomized liquid is to increase the viscosity of the e-liquid and prevent the liquid from flowing too much into the e-cigarette atomizer during the practical process, causing problems such as low atomization effect exist. At the same time, increasing the viscosity of e-cigarette liquid can also facilitate transportation and storage.
本发明的有益效果：所提供的淡雅香型保健电子烟雾化烟液，不仅能够满足烟民的吸烟需求，还可有效的降低烟气对身体气管、支气管、喉、肺的刺激，具有清热润肺、止咳祛痰、提神醒脑、理气开郁等功效。其中薄荷的加入能够起到提神醒脑的作用。绿茶和神农香菊不仅具有明显的止咳、抗炎、祛痰、平喘的功效，添加到烟液中，使烟气细腻柔和，抽吸后可显著降低副作用，缓解喉部不适反应。对吸烟者的喉部、呼吸道能起到保护作用，可显著降低吸烟所引起的咳嗽、多痰等不良症状，而且香气飘逸优雅，烟草本香与淡雅的天然植物香气浑然一体。Beneficial effects of the present invention: the provided light and fragrant health-care electronic cigarette liquid can not only meet the smoking needs of smokers, but also effectively reduce the stimulation of smoke on the body's trachea, bronchi, larynx, and lungs, and has the functions of clearing away heat and moistening Lung, cough and expectorant, refreshing, qi and depression and other effects. Among them, the addition of peppermint can play a refreshing effect. Green tea and Shennong chrysanthemum not only have obvious effects of relieving cough, anti-inflammation, eliminating phlegm, and relieving asthma, they are added to the liquid smoke to make the smoke delicate and soft, and can significantly reduce side effects and relieve throat discomfort after smoking. It can protect the throat and respiratory tract of smokers, and can significantly reduce adverse symptoms such as cough and phlegm caused by smoking. It has an elegant and elegant aroma, and the natural aroma of tobacco is integrated with the elegant natural plant aroma.
具体实施方式Detailed ways
以下结合具体实施例对本发明作进一步的详细描述。The present invention will be described in further detail below in conjunction with specific examples.
实施例1Example 1
（1）中药药液的制备：(1) Preparation of traditional Chinese medicine liquid:
首先称取川贝母20g、薄荷叶15g、枇杷叶25g、神农香菊20g、紫罗兰20g、桂花25g、绿茶25g，用75%的乙醇300ml加热提取，提取过程中进行冷却回流，回流3h后冷却取出提取液，然后加入等量的75%乙醇进行第二次提取，加热回流3h。冷却后取出第二次提取液，将两次提取液混匀，过滤，减压浓缩，得到相对密度为1.05的50ml的中药药液1，备用。First weigh 20g of Chuan Fritillaria, 15g of mint leaves, 25g of loquat leaves, 20g of Shennong chrysanthemum, 20g of violet, 25g of sweet-scented osmanthus, and 25g of green tea, heat and extract with 75% ethanol 300ml, cool and reflux during the extraction process, and cool after reflux for 3 hours Take out the extract, then add an equal amount of 75% ethanol for the second extraction, and heat to reflux for 3h. After cooling, take out the second extract, mix the two extracts evenly, filter, and concentrate under reduced pressure to obtain 50ml of traditional Chinese medicine liquid 1 with a relative density of 1.05, which is set aside.
（2）淡雅香型电子烟雾化烟液制备：(2) Preparation of Elegant and Elegant E-cigarette E-liquid:
1．取10g去离子水，将去离子水加热到60℃，加入0.05g海藻酸钠和0.05g黄原胶，继续加热搅拌，加热到90℃，直到海藻酸钠和黄原胶完全溶解，得到成型剂水溶液1。1. Take 10g of deionized water, heat the deionized water to 60°C, add 0.05g of sodium alginate and 0.05g of xanthan gum, continue to heat and stir, and heat to 90°C until the sodium alginate and xanthan gum are completely dissolved to obtain a molded Agent aqueous solution 1.
2．称取30g丙二醇和25g甘油混合后，充分搅拌，然后将成型剂水溶液1加入后，保持在80℃搅拌均匀得到成型剂溶剂混合液1，保温备用。2. Weigh 30g of propylene glycol and 25g of glycerin and mix them thoroughly, then add the forming agent aqueous solution 1, keep stirring at 80°C to obtain the forming agent-solvent mixture 1, and keep it warm for later use.
3．称取酒精10g，将17g中药药液1，3g烟用香精和5g烟草提取物一起放入到酒精中，搅拌均匀得到中药烟草混合液1，备用。3. Weigh 10 g of alcohol, put 17 g of traditional Chinese medicine liquid 1, 3 g of tobacco essence and 5 g of tobacco extract into the alcohol, stir evenly to obtain Chinese medicine tobacco mixture 1, and set aside.
4．将中药烟草混合液1倒入成型剂溶剂混合液1中，不断搅拌，使其慢慢温度降至室温，制得淡雅香型电子烟雾化烟液1。4. Pour the traditional Chinese medicine tobacco mixed liquid 1 into the forming agent solvent mixed liquid 1, and keep stirring until the temperature is slowly lowered to room temperature to prepare the light and fragrant electronic cigarette liquid 1.
实施例2Example 2
（1）中药药液的制备：(1) Preparation of traditional Chinese medicine liquid:
首先称取川贝母20g、薄荷叶15g、枇杷叶25g、神农香菊20g、紫罗兰20g、桂花25g、绿茶25g，用75%的乙醇300 ml加热提取，提取过程中进行冷却回流，回流3h后冷却取出提取液，然后加入等量的75%乙醇进行第二次提取，加热回流3h。冷却后取出第二次提取液，将两次提取液混匀，过滤，减压浓缩，得到相对密度为1.10的50ml的中药药液2，备用。First weigh 20g of Fritillaria sichuanensis, 15g of mint leaves, 25g of loquat leaves, 20g of Shennong chrysanthemum, 20g of violets, 25g of sweet-scented osmanthus, and 25g of green tea, heat and extract with 300 ml of 75% ethanol, cool and reflux during the extraction process, and reflux for 3 hours Cool and take out the extract, then add an equal amount of 75% ethanol for the second extraction, and heat to reflux for 3h. After cooling, take out the second extract, mix the two extracts evenly, filter, and concentrate under reduced pressure to obtain 50ml of traditional Chinese medicine liquid 2 with a relative density of 1.10, which is set aside.
（2）淡雅香型电子烟雾化烟液制备：(2) Preparation of Elegant and Elegant E-cigarette E-liquid:
1．取10g去离子水，将去离子水加热到60℃，加入0.05g海藻酸钠和0.05g黄原胶，继续加热搅拌，加热到95℃，直到海藻酸钠和黄原胶完全溶解，得到成型剂水溶液2。1. Take 10g of deionized water, heat the deionized water to 60°C, add 0.05g of sodium alginate and 0.05g of xanthan gum, continue to heat and stir, and heat to 95°C until the sodium alginate and xanthan gum are completely dissolved to obtain a molded Agent aqueous solution 2.
2．称取30g丙二醇和23g甘油混合后，充分搅拌，然后将成型剂水溶液2加入后，保持在80℃搅拌均匀得到成型剂溶剂混合液2，保温备用。2. Weigh 30g of propylene glycol and 23g of glycerin and mix them thoroughly, then add the forming agent aqueous solution 2, keep stirring at 80°C to obtain the forming agent solvent mixture 2, and keep it warm for later use.
3．称取酒精12g，将18g中药药液2，4g烟用香精和4g烟草提取物一起放入到酒精中，搅拌均匀得到中药烟草混合液2，备用。3. Weigh 12g of alcohol, put 18g of Chinese medicinal liquid 2, 4g of tobacco essence and 4g of tobacco extract into the alcohol, stir evenly to obtain Chinese medicinal tobacco mixture 2, and set aside.
4．将中药烟草混合液2倒入成型剂溶剂混合液2中，不断搅拌，使其慢慢温度降至室温，制得淡雅香型电子烟雾化烟液2。4. Pour the traditional Chinese medicine tobacco mixed liquid 2 into the forming agent solvent mixed liquid 2, and keep stirring to make the temperature slowly drop to room temperature, and prepare the light and fragrant electronic cigarette liquid 2.
实施例3Example 3
（1）中药药液的制备：(1) Preparation of traditional Chinese medicine liquid:
首先称取川贝母15g、薄荷叶20g、枇杷叶20g、神农香菊25g、紫罗兰15g、桂花25g、绿茶30g，用75%的乙醇300 ml加热提取，提取过程中进行冷却回流，回流3h后冷却取出提取液，然后加入等量的75%乙醇进行第二次提取，加热回流3h。冷却后取出第二次提取液，将两次提取液混匀，过滤，减压浓缩，得到相对密度为1.17的50ml的中药药液3，备用。First weigh 15g of Fritillaria sichuanensis, 20g of mint leaves, 20g of loquat leaves, 25g of Shennong chrysanthemum, 15g of violets, 25g of sweet-scented osmanthus, and 30g of green tea, heat and extract with 300 ml of 75% ethanol, cool and reflux during the extraction process, and reflux for 3 hours Cool and take out the extract, then add an equal amount of 75% ethanol for the second extraction, and heat to reflux for 3h. After cooling, take out the second extract, mix the two extracts evenly, filter, and concentrate under reduced pressure to obtain 50ml of traditional Chinese medicine liquid 3 with a relative density of 1.17, which is set aside.
（2）淡雅香型电子烟雾化烟液制备：(2) Preparation of Elegant and Elegant E-cigarette E-liquid:
1．取10g去离子水，将去离子水加热到60℃，加入0.05g海藻酸钠和0.05g黄原胶，继续加热搅拌，加热到85℃，直到海藻酸钠和黄原胶完全溶解，得到成型剂水溶液3。1. Take 10g of deionized water, heat the deionized water to 60°C, add 0.05g of sodium alginate and 0.05g of xanthan gum, continue to heat and stir, and heat to 85°C until the sodium alginate and xanthan gum are completely dissolved to obtain a molded Agent aqueous solution 3.
2．称取30g丙二醇和25g甘油混合后，充分搅拌，然后将成型剂水溶液3加入后，保持在80℃搅拌均匀得到成型剂溶剂混合液3，保温备用。2. Weigh 30g of propylene glycol and 25g of glycerin and mix them thoroughly, then add the forming agent aqueous solution 3, keep stirring at 80°C to obtain the forming agent solvent mixture 3, and keep it warm for later use.
3．称取酒精10g，将17g中药药液3，3g烟用香精和5g烟草提取物一起放入到酒精中，搅拌均匀得到中药烟草混合液3，备用。3. Weigh 10 g of alcohol, put 17 g of traditional Chinese medicine liquid 3, 3 g of tobacco essence and 5 g of tobacco extract into the alcohol, stir evenly to obtain Chinese medicine tobacco mixture 3, and set aside.
4．将中药烟草混合液3倒入成型剂溶剂混合液3中，不断搅拌，使其慢慢温度降至室温，制得淡雅香型电子烟雾化烟液3。4. Pour the traditional Chinese medicine tobacco mixed liquid 3 into the forming agent solvent mixed liquid 3, and keep stirring to make the temperature slowly drop to room temperature, and prepare the light and fragrant electronic cigarette liquid 3.
将上述实施例分别进行效果评价，其结果如下表：Above-mentioned embodiment is carried out effect evaluation respectively, and its result is as following table:
实施例1效果评价表Example 1 Effect Evaluation Form
实施例2效果评级表Embodiment 2 Effect Rating Table
实施例3效果评价表Example 3 Effect Evaluation Form
上述效果评价显示，本发明提供的淡雅香型电子烟雾化烟液，气味芬芳、具有淡雅且层次感丰富的烤烟香气，杂气较轻，口感细腻、回甜，对咽喉刺激性小，具有较好的雾化性能，能实现较好的烟雾效果。The above-mentioned effect evaluation shows that the light-flavored e-cigarette liquid provided by the present invention has a fragrant smell, an elegant and rich layered flue-cured tobacco aroma, light miscellaneous gas, delicate taste, sweet aftertaste, less irritation to the throat, and has a relatively Good atomization performance can achieve better smoke effect.
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210457376.6ACN102960852B (en) | 2012-11-14 | 2012-11-14 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210457376.6ACN102960852B (en) | 2012-11-14 | 2012-11-14 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| Publication Number | Publication Date |
|---|---|
| CN102960852A CN102960852A (en) | 2013-03-13 |
| CN102960852Btrue CN102960852B (en) | 2015-04-22 |
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210457376.6AActiveCN102960852B (en) | 2012-11-14 | 2012-11-14 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| Country | Link |
|---|---|
| CN (1) | CN102960852B (en) |
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