CN102697169A - Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereof - Google Patents
Moisturizing and flavor-enhancing additive for cigarettes as well as preparation method and application thereofDownload PDFInfo
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Abstract
Translated fromChineseDescription
Translated fromChinese技术领域technical field
本发明涉及烟用添加剂及其制备与应用领域，尤其是涉及一种包含中药提取物组合或中药复方提取物的，具有保润增香作用的卷烟添加剂及其制备方法与应用。The invention relates to the field of tobacco additives and their preparation and application, in particular to a cigarette additive containing a combination of traditional Chinese medicine extracts or compound Chinese medicine extracts, which has the effect of moisturizing and enhancing flavor, and its preparation method and application.
背景技术Background technique
保润剂是指在烟草制品加工过程中施加于烟草中能够增强烟草，烟草制品保湿性能、增加柔软性、降低碎损的物质。保润剂能够改善叶片与烟丝的物理性质，增加卷烟产品韧性，弹性和保水性能，减少加工过程中工艺损耗。目前我国卷烟工业中主要采用甘油、丙二醇、山梨醇、木糖醇等多羟基物质为保润剂，靠这些物质吸收空气中的水分以保持烟丝的润湿，但使用此类保润剂的目的仅在于维持加工过程中烟丝的含水率，提高烟丝的耐加工性，而对于成品卷烟吸食舒适度的改善则效果不太理想。此外这类保润剂受环境温湿度影响大，甘油与丙二醇成本较高，山梨醇和木糖醇成本尽管可控，但保润效果不如甘油和丙二醇。Humectants refer to substances that are added to tobacco during the processing of tobacco products to enhance the moisturizing properties of tobacco and tobacco products, increase softness, and reduce damage. The humectant can improve the physical properties of leaves and shredded tobacco, increase the toughness, elasticity and water retention performance of cigarette products, and reduce the process loss during processing. At present, polyhydroxy substances such as glycerin, propylene glycol, sorbitol, and xylitol are mainly used as humectants in the cigarette industry in my country. These substances absorb moisture in the air to keep tobacco shreds moist, but the purpose of using such humectants It is only to maintain the moisture content of shredded tobacco during processing and improve the processing resistance of shredded tobacco, but the effect of improving the smoking comfort of finished cigarettes is not ideal. In addition, this kind of humectant is greatly affected by the temperature and humidity of the environment, and the cost of glycerin and propylene glycol is relatively high. Although the cost of sorbitol and xylitol is controllable, the moisturizing effect is not as good as that of glycerin and propylene glycol.
我国从上世纪中叶开始就开始进行中药类天然植物添加剂卷烟的研究开发。在数十年间，行业内的科研工作者在中草药添加剂减少卷烟对人体危害领域做了大量工作，如《一种含有植物提取物的低危害烟草及其制备方法》(申请号：201110181597.0，公开号：CN102349697A)，《一种卷烟减害添加剂及其制备方式》(申请号：201110241463.3，公开号：CN102318896A)等。近年来，随着行业产业化发展加速，南方湿润地区生产卷烟在北方干燥地区销售增加，保润剂研发引起更高重视，采用中药类天然产物提高卷烟保润性能的研究应当成为研究热点。Since the middle of last century, my country has started to research and develop traditional Chinese medicine natural plant additive cigarettes. For decades, scientific researchers in the industry have done a lot of work in the field of Chinese herbal medicine additives to reduce the harm of cigarettes to the human body, such as "A Low-Hazard Tobacco Containing Plant Extracts and Its Preparation Method" (Application No.: 201110181597.0, Publication No. : CN102349697A), "A Cigarette Hazard Reduction Additive and Its Preparation Method" (Application No.: 201110241463.3, Publication No.: CN102318896A), etc. In recent years, with the accelerated industrialization of the industry, cigarettes produced in humid areas in the south are sold in dry areas in the north, and more attention has been paid to the research and development of humectants. The use of natural products of traditional Chinese medicine to improve the moisture retention performance of cigarettes should become a research hotspot.
发明内容Contents of the invention
本发明目的之一在于提供一种卷烟保润增香添加剂及其制备方法。One of the objectives of the present invention is to provide a cigarette moisturizing and flavoring additive and a preparation method thereof.
本发明的另一目的，在于提供这种卷烟保润增香添加剂的应用。Another object of the present invention is to provide the application of this cigarette moisturizing and flavoring additive.
根据本发明的目的之一，本发明的技术方案如下：According to one of purpose of the present invention, technical scheme of the present invention is as follows:
一种卷烟保润增香添加剂，包含中药提取物组合物或复方中药提取物，其特征在于：所述中药提取物组合物或复方中药提取物包含淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红。A cigarette moisturizing and flavoring additive, comprising a Chinese medicine extract composition or a compound Chinese medicine extract, characterized in that: the Chinese medicine extract composition or compound Chinese medicine extract contains Epimedium, Eclipta, sweet almond, motherwort , Dandelion And Oranges.
所述中药提取物组合物中淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的提取物重量比例为1-8∶0.8-6∶0.5-4∶0.3-4∶0.3-5∶1。The weight ratio of the extracts of Epimedium, Eclipta, Sweet Almond, Motherwort, Dandelion and Citrus Red in the Chinese medicine extract composition is 1-8: 0.8-6: 0.5-4: 0.3-4: 0.3-5 : 1.
所述复方中药提取物中原料药淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的重量比例为0.5～8∶0.5-6∶0.2-4∶0.3-4∶0.3-5∶1。The weight ratio of raw materials Epimedium, Eclipta, sweet almond, motherwort, dandelion and Huajuhong in the compound Chinese medicine extract is 0.5～8: 0.5-6: 0.2-4: 0.3-4: 0.3-5: 1.
所述制备方法优选方案一，按照以下步骤进行：The preferred option one of the preparation method is carried out according to the following steps:
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入6-15倍量纯净水，浸泡2-48h，65-100℃热回流提取1-3h，共提取3次，合并3次提取液，60-80℃，压力0.02-0.08Mpa条件下浓缩至密度为1.12±0.01流浸膏；Take epimedium, eclipta, sweet almond, motherwort, dandelion, and citrus red, grind them and extract them separately, add 6-15 times the amount of purified water respectively, soak for 2-48 hours, heat reflux at 65-100°C for 1-3 hours, Extracted 3 times in total, combined 3 extracts, concentrated at 60-80°C, pressure 0.02-0.08Mpa to a fluid extract with a density of 1.12±0.01;
随后，加入2倍体积乙醇，静置24-96h，过滤沉淀，60-80℃，压力0.02-0.08Mpa条件下浓缩至密度为1.12±0.01流浸膏；Then, add 2 times the volume of ethanol, let it stand for 24-96h, filter the precipitate, concentrate at 60-80°C and a pressure of 0.02-0.08Mpa to a fluid extract with a density of 1.12±0.01;
将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按1-8∶0.8-6∶0.5-4∶0.3-4∶0.3-5∶1混合均匀，过滤即得保润增香添加剂。Mix the liquid extracts of Epimedium, Eclipta, sweet almond, motherwort, dandelion and orange red according to the ratio of 1-8:0.8-6:0.5-4:0.3-4:0.3-5:1, and filter to obtain Moisturizing and flavoring additive.
作为优选方案之二，所述制备方法按照以下步骤进行：As the second preferred option, the preparation method is carried out according to the following steps:
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按0.5-8∶0.5-6∶0.2-4∶0.3-4∶0.3-5∶1比例均匀混合，加入6-15倍量纯净水，浸泡2-48h后，65-100℃热回流提取1-3h，共提取3次，合并3次提取液，60-80℃，压力0.02-0.08Mpa条件下浓缩至密度为1.12±0.01流浸膏；Take Epimedium, Eclipta, Sweet Almond, Motherwort, Dandelion, and Juhong respectively, grind them and mix evenly according to the ratio of 0.5-8:0.5-6:0.2-4:0.3-4:0.3-5:1, add 6 -15 times the amount of pure water, after soaking for 2-48 hours, heat reflux extraction at 65-100°C for 1-3 hours, extract 3 times in total, combine the extracts from 3 times, concentrate to density at 60-80°C, pressure 0.02-0.08Mpa It is 1.12±0.01 liquid extract;
加入2倍体积乙醇，静置24-96h，过滤沉淀，60-80℃，压力0.02-0.08Mpa条件下浓缩至密度为1.12±0.01流浸膏，过滤，即得保润增香添加剂。Add 2 times the volume of ethanol, let it stand for 24-96 hours, filter the precipitate, concentrate at 60-80°C and pressure 0.02-0.08Mpa to a liquid extract with a density of 1.12±0.01, and filter to obtain the moisturizing and flavoring additive.
为大工业的推广应用，本发明还提供一种卷烟保润增香添加剂的应用：取适量保润增香添加剂，溶于一定体积蒸馏水，均匀喷洒于卷烟烟丝、梗丝、薄片。保润增香添加剂的用量为烟丝，梗丝，薄片重量的0.002-1％wt。For popularization and application in large industries, the present invention also provides an application of the moisturizing and flavoring additive for cigarettes: take an appropriate amount of the moisturizing and flavoring additive, dissolve it in a certain volume of distilled water, and evenly spray it on shredded tobacco, shredded stems and thin slices of cigarettes. The dosage of the moisturizing and flavoring additive is 0.002-1%wt of the weight of shredded tobacco, shredded stems and flakes.
本发明的有益效果之一在于：该添加剂添加于卷烟烟丝，梗丝，薄片后，在常温干燥环境下具有良好的持水能力，可提高烟丝样品的含水率，可以减缓水分的散失，降低烟丝的失水率，起到维持烟丝水分的作用，具有良好的物理保润作用。One of the beneficial effects of the present invention is that: after the additive is added to shredded tobacco, shredded stems, and thin slices of cigarettes, it has good water-holding capacity in a dry environment at room temperature, can increase the moisture content of shredded tobacco samples, can slow down the loss of water, and reduce the moisture content of shredded tobacco. The water loss rate is high, which plays the role of maintaining the moisture of cut tobacco, and has a good physical moisturizing effect.
本技术与现有技术相比还具有以下优点：该添加剂不仅具有良好的物理保润作用，还可以有效增加卷烟的香气量，改善香气质和协调性，减少杂气与刺激性，增加甜润感，使余味更干净、舒适，整体提升了卷烟的内在品质。并且设备简单，提取工艺简单易行，成本可控，原料易得。Compared with the existing technology, this technology also has the following advantages: the additive not only has a good physical moisturizing effect, but also can effectively increase the aroma of cigarettes, improve aroma quality and coordination, reduce miscellaneous gas and irritation, and increase sweetness , making the aftertaste cleaner and more comfortable, and improving the inner quality of cigarettes as a whole. Moreover, the equipment is simple, the extraction process is simple and easy, the cost is controllable, and the raw materials are easy to obtain.
附图说明Description of drawings
结合附图对实施例的描述中将使本发明变得明显和容易理解，其中：The present invention will be apparent and easily understood in the description of the embodiments in conjunction with the accompanying drawings, in which:
图1为常温干燥条件下，含保润增香剂的烟丝与空白烟丝(空白)、含丙二醇烟丝(对照)含水率随时间变化趋势图；Fig. 1 is under normal temperature drying condition, the cut tobacco that contains moistening and flavoring agent and blank cut tobacco (blank), contains propylene glycol shredded tobacco (contrast) moisture content trend graph with time;
图2为常温干燥条件下，含保润增香剂的烟丝与空白烟丝(空白)、含丙二醇烟丝(对照)失水率随时间变化趋势图。Fig. 2 is a graph showing the change in water loss rate over time of shredded tobacco containing moisturizing and flavoring agent, blank shredded tobacco (blank), and shredded tobacco containing propylene glycol (control) under normal temperature drying conditions.
具体实施方式Detailed ways
下面详细描述本发明的实施例。下面通过参考附图描述的实施例是示例性的，仅用于解释本发明，而不能解释为对本发明的限制。Embodiments of the present invention are described in detail below. The embodiments described below by referring to the figures are exemplary only for explaining the present invention and should not be construed as limiting the present invention.
实验例：Experimental example:
一.保润效果评价1. Evaluation of moisturizing effect
1.测试目的1. Test purpose
对比在同等条件下，含保润增香剂的烟丝与空白烟丝(空白)、含丙二醇烟丝(对照)的物理保润效果。Under the same conditions, the physical moisturizing effect of cut tobacco containing moisturizing and flavoring agent was compared with blank cut tobacco (blank) and cut tobacco containing propylene glycol (control).
2.测试样品2. Test samples
保润增香剂：1％保润增香剂+中档空白烟丝Moisturizing and flavoring agent: 1% moisturizing and flavoring agent + mid-range blank tobacco
对照：1％丙二醇+中档空白烟丝Control: 1% propylene glycol + mid-range blank tobacco
空白：中档空白烟丝Blank: mid-range blank tobacco
3.测试方法3. Test method
3.1平衡过程：将测试实验的三组样品置于温度：(22±1)℃，湿度：(60±3)％的恒温恒湿箱中平衡48小时，用烘箱法测出三组测试样品的初始水份含量，即为0h的含水率。3.1 Balance process: put the three groups of samples in the test experiment in a temperature: (22±1)°C, humidity: (60±3)% in a constant temperature and humidity chamber for 48 hours, and use the oven method to measure the temperature of the three groups of test samples The initial moisture content is the moisture content of 0h.
3.2测试过程：将恒温恒湿箱环境调整为温度：(22±1)℃，湿度：(40±3)％，将三组测试样品置于其中，间隔一定时间称量一次样品重量，并依据此时的样品重量计算它的即时含水率。3.2 Test process: Adjust the environment of the constant temperature and humidity chamber to temperature: (22±1)℃, humidity: (40±3)%, put three groups of test samples in it, weigh the sample weight once at a certain interval, and according to The weight of the sample at this point is used to calculate its instant moisture content.
4.测试结果4. Test results
含水率和失水率随时间边哈趋势图分析：参见附图1和2。图1含保润增香剂的烟丝与空白烟丝(空白)、含丙二醇烟丝(对照)含水率随时间变化趋势图样。Analysis of water content and water loss rate with Bianha trend graph over time: see attached drawings 1 and 2. Fig. 1 The trend pattern of the moisture content of cut tobacco containing moisturizing and flavoring agent, blank cut tobacco (blank), and cut tobacco containing propylene glycol (control) over time.
图1所示为测试条件下即常温干燥条件的水分-时间测试曲线，曲线显示，在0-20h时，保润增香剂、空白、对照剧烈失水，水分呈直线下降趋势。24h后，两者的水份曲线趋于平缓，这意味着，在24h后，两者在该环境下达到水分的吸收平衡，从这时的含水率比较，保润增香剂＞空白。可见，在常温干燥的环境中，保润增香剂具有一定的持水能力，可提高烟丝样品的含水率。Figure 1 shows the moisture-time test curve under the test conditions, that is, the normal temperature drying condition. The curve shows that at 0-20 hours, the moisturizing and flavoring agent, the blank, and the control lose water violently, and the moisture shows a linear downward trend. After 24 hours, the moisture curves of the two tended to be flat, which means that after 24 hours, the two reached the moisture absorption equilibrium in this environment. From the comparison of the moisture content at this time, the moisturizing and flavoring agent>blank. It can be seen that in a dry environment at room temperature, the moisturizing and flavoring agent has a certain water holding capacity and can increase the moisture content of cut tobacco samples.
图2含保润增香剂的烟丝与空白烟丝(空白)、含丙二醇烟丝(对照)失水率随时间变化趋势图。Fig. 2 is a trend diagram of the water loss rate of shredded tobacco containing moisturizing and flavoring agent, blank shredded tobacco (blank), and shredded tobacco containing propylene glycol (control) over time.
如图2所示，失水率是指在某段时间内，样品的失水量与初始水分的比值。n小时失水率＝n小时的失水量/初始水分。24小时内，3组样品的失水率变化剧烈。由于样品放置于干燥的环境中，首先失去的是烟丝表面的游离态水分，因此水分散失的速率较快。48小时之后在随着平衡时间的延长，失水率趋于恒定。从48小时后失水率变化的情况可以看出，空白＞对照＞保润增香剂。从48h以后的对比失水率数据总体看来，在常温干燥环境下，保润增香剂可以延缓样品水分散失，延缓水分散失速率，作用强于丙二醇。As shown in Figure 2, the water loss rate refers to the ratio of the water loss of the sample to the initial moisture within a certain period of time. Water loss rate in n hours = water loss in n hours/initial moisture. Within 24 hours, the water loss rate of the three groups of samples changed drastically. Since the sample is placed in a dry environment, the first thing to lose is the free moisture on the surface of the shredded tobacco, so the rate of moisture loss is relatively fast. After 48 hours, the water loss rate tends to be constant with the prolongation of the equilibrium time. From the change of water loss rate after 48 hours, it can be seen that blank>control>moisturizing and flavoring agent. From the comparison of water loss rate data after 48 hours, it can be seen that in a normal temperature and dry environment, the moisturizing and flavoring agent can delay the water loss of the sample and the rate of water loss, and the effect is stronger than that of propylene glycol.
综上所述，保润增香剂能够在常温干燥环境中都能起到减缓水分的散失，降低烟丝的失水率，起到维持烟丝水分的作用。To sum up, the moisturizing and flavoring agent can slow down the loss of water in a dry environment at room temperature, reduce the water loss rate of shredded tobacco, and maintain the moisture of shredded tobacco.
二.评吸效果评价2. Evaluation of suction effect
取成品保润增香剂，分别按照0.005％，0.01％，0.02％添加于高、中、低烤烟型卷烟叶组烟丝上，于密封袋中室温放置2h后，用CMBl20卷烟机上卷成烟支，于22℃±1℃和RH60％±2％的湿箱内平衡48h，组织本评吸委员会专家评吸，专家共7名，均为省级评委。Take the finished moisturizing and flavoring agent, add it on the shredded tobacco of high, medium and low flue-cured tobacco leaf groups according to 0.005%, 0.01%, and 0.02% respectively, place it in a sealed bag at room temperature for 2 hours, and roll it into a cigarette with a CMB120 cigarette rolling machine , Balanced in a humid box at 22°C±1°C and RH60%±2% for 48 hours, and organized experts in this evaluation committee to evaluate smoking. There are a total of 7 experts, all of whom are provincial judges.
结果显示，保润增香剂添加于卷烟叶组后，可以有效增加卷烟的香气量，改善香气质和协调性，减少杂气与刺激性，增加甜润感，使余味更干净、舒适，整体提升了卷烟的内在品质，尤其在中低档卷烟中效果更加明显。评吸结果见表2。The results show that the moisturizing and flavoring agent added to the cigarette leaf group can effectively increase the aroma of cigarettes, improve aroma quality and coordination, reduce miscellaneous gas and irritation, increase sweetness, make the aftertaste cleaner and more comfortable, and improve the overall quality of cigarettes. It improves the inherent quality of cigarettes, especially in middle and low-grade cigarettes. The evaluation results are shown in Table 2.
表2.保润增香剂添加于卷烟后的评吸结果Table 2. Smoking results after moisturizing and flavoring agents were added to cigarettes
实施例一Embodiment one
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按0.5∶0.5∶0.2∶0.3∶0.3∶1比例均匀混合，加入8倍量纯净水，浸泡2h后，75℃热回流提取1h，共提取3次，合并3次提取液，80℃，压力0.02Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置24h，过滤沉淀，80℃，压力0.02Mpa条件下浓缩至密度为1.12流浸膏，过滤，即得保润增香添加剂。取添加剂10g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take Epimedium, Eclipta, sweet almond, motherwort, dandelion and Huajuhong respectively, grind them and mix them uniformly according to the ratio of 0.5:0.5:0.2:0.3:0.3:1, add 8 times the amount of pure water, soak for 2 hours, 75 Heat reflux at ℃ for 1 hour, extract 3 times in total, combine the extracts from the 3 times, concentrate at 80 ℃ and pressure 0.02Mpa to a fluid extract with a density of 1.12. Add 2 times the volume of ethanol, let it stand for 24 hours, filter the precipitate, concentrate at 80°C and a pressure of 0.02Mpa to a liquid extract with a density of 1.12, and filter to obtain a moisturizing and flavoring additive. Take 10g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例二Embodiment two
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按1∶0.75∶0.5∶0.5∶0.5∶1比例均匀混合，加入6倍量纯净水，浸泡6h后，70℃热回流提取1.5h，共提取3次，合并3次提取液，75℃，压力0.06Mpa条件下浓缩至密度为1.11流浸膏。加入2倍体积乙醇，静置36h，过滤沉淀，75℃，压力0.06Mpa条件下浓缩至密度为1.11流浸膏，过滤，即得保润增香添加剂。取添加剂50g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take Epimedium, Eclipta, sweet almond, motherwort, dandelion and Huajuhong respectively, grind them and mix them uniformly according to the ratio of 1:0.75:0.5:0.5:0.5:1, add 6 times the amount of pure water, soak for 6 hours, 70 ℃ heat reflux extraction for 1.5h, a total of 3 extractions, combined 3 extracts, 75 ℃, concentrated under the conditions of pressure 0.06Mpa to a density of 1.11 liquid extract. Add 2 times the volume of ethanol, let it stand for 36 hours, filter the precipitate, concentrate at 75°C and a pressure of 0.06Mpa to a liquid extract with a density of 1.11, and filter to obtain a moisturizing and flavoring additive. Take 50g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例三Embodiment Three
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按1.5∶1∶1∶1.5∶1.5∶1比例均匀混合，加入10倍量纯净水，浸泡12h后，65℃热回流提取1.5h，共提取3次，合并3次提取液，70℃，压力0.03Mpa条件下浓缩至密度为1.13流浸膏。加入2倍体积乙醇，静置48h，过滤沉淀，70℃，压力0.03Mpa条件下浓缩至密度为1.13流浸膏，过滤，即得保润增香添加剂。取添加剂100g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take Epimedium, Eclipta, Sweet Almond, Leonurus, Dandelion and Huajuhong respectively, grind them and mix them uniformly according to the ratio of 1.5:1:1:1.5:1.5:1, add 10 times the amount of pure water, soak for 12 hours, and 65 ℃ heat reflux extraction for 1.5h, a total of 3 extractions, combined 3 extracts, 70 ℃, concentrated under the conditions of pressure 0.03Mpa to a density of 1.13 liquid extract. Add 2 times the volume of ethanol, let it stand for 48 hours, filter the precipitate, concentrate at 70°C and a pressure of 0.03Mpa to a liquid extract with a density of 1.13, and filter to obtain a moisturizing and flavoring additive. Take 100g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例四Embodiment four
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按2∶1.5∶1∶1∶1∶1比例均匀混合，加入12倍量纯净水，浸泡24h后，90℃热回流提取2h，共提取3次，合并3次提取液，65℃，压力0.05Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置72h，过滤沉淀，65℃，压力0.05Mpa条件下浓缩至密度为1.12流浸膏，过滤，即得保润增香添加剂。取添加剂500g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take Epimedium, Eclipta, Sweet Almond, Leonurus, Dandelion and Huajuhong respectively, grind them and mix them uniformly according to the ratio of 2:1.5:1:1:1:1, add 12 times the amount of pure water, soak for 24 hours, and then 90 ℃ heat reflux extraction for 2 hours, a total of 3 extractions, combined 3 extracts, 65 ℃, concentrated under the conditions of pressure 0.05Mpa to a density of 1.12 liquid extract. Add 2 times the volume of ethanol, let it stand for 72 hours, filter the precipitate, concentrate at 65°C and a pressure of 0.05Mpa to a liquid extract with a density of 1.12, and filter to obtain a moisturizing and flavoring additive. Take 500g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例五Embodiment five
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按4∶3∶2∶2∶2∶1比例均匀混合，加入13倍量纯净水，浸泡36h后，80℃热回流提取2.5h，共提取3次，合并3次提取液，75℃，压力0.04Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置72h，过滤沉淀，75℃，压力0.04Mpa条件下浓缩至密度为1.12流浸膏，过滤，即得保润增香添加剂。取添加剂1kg，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take Epimedium, Eclipta, sweet almond, motherwort, dandelion and Huajuhong respectively, grind them and mix them uniformly according to the ratio of 4:3:2:2:2:1, add 13 times the amount of pure water, soak for 36 hours, and 80 ℃ heat reflux extraction for 2.5h, a total of 3 extractions, combined 3 extracts, 75 ℃, concentrated under the conditions of pressure 0.04Mpa to a density of 1.12 liquid extract. Add 2 times the volume of ethanol, let it stand for 72 hours, filter the precipitate, concentrate at 75°C and a pressure of 0.04Mpa to a liquid extract with a density of 1.12, and filter to obtain a moisturizing and flavoring additive. Take 1kg of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例六Embodiment six
分别取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后按8∶6∶4∶4∶5∶1比例均匀混合，加入15倍量纯净水，浸泡48h后，100℃热回流提取3h，共提取3次，合并3次提取液，60℃，压力0.06Mpa条件下浓缩至密度为1.13流浸膏。加入2倍体积乙醇，静置96h，过滤沉淀，60℃，压力0.06Mpa条件下浓缩至密度为1.13流浸膏，过滤，即得保润增香添加剂。取添加剂5kg，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take Epimedium, Eclipta, Sweet Almond, Leonurus, Dandelion and Huajuhong respectively, grind them and mix them evenly according to the ratio of 8:6:4:4:5:1, add 15 times the amount of pure water, soak for 48 hours, and then 100 ℃ heat reflux extraction for 3 hours, a total of 3 extractions, combined 3 extracts, concentrated at 60 ℃, pressure 0.06Mpa to a fluid extract with a density of 1.13. Add 2 times the volume of ethanol, let it stand for 96 hours, filter the precipitate, concentrate at 60°C and a pressure of 0.06Mpa to a liquid extract with a density of 1.13, and filter to obtain a moisturizing and flavoring additive. Take 5kg of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例七Embodiment seven
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入8倍量纯净水，浸泡6h后，70℃热回流提取1h，共提取3次，合并3次提取液，70℃，压力0.05Mpa条件下浓缩至密度为1.13流浸膏。加入2倍体积乙醇，静置24h，过滤沉淀，70℃，压力0.05Mpa条件下浓缩至密度为1.13流浸膏，将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按1∶0.8∶0.5∶0.3∶0.3∶1混合均匀，过滤即得保润增香添加剂。取添加剂10g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take epimedium, eclipta, sweet almond, motherwort, dandelion, and citrus red, grind them and extract them separately, add 8 times the amount of pure water respectively, soak for 6 hours, extract under reflux at 70°C for 1 hour, extract 3 times in total, and combine 3 The secondary extract is concentrated to a fluid extract with a density of 1.13 at 70°C and a pressure of 0.05Mpa. Add 2 times the volume of ethanol, let it stand for 24 hours, filter the precipitate, concentrate the liquid extract to a density of 1.13 under the condition of 70 ° C and a pressure of 0.05 Mpa, and mix the liquid extract of Epimedium, Eclipta, sweet almond, motherwort, dandelion, and orange red. The extract is mixed uniformly at the ratio of 1:0.8:0.5:0.3:0.3:1, and filtered to obtain the moisturizing and flavoring additive. Take 10g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例八Embodiment eight
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入10倍量纯净水，浸泡12h后，80℃热回流提取1.5h，共提取3次，合并3次提取液，75℃，压力0.08Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置36h，过滤沉淀，75℃，压力0.08Mpa条件下浓缩至密度为1.12流浸膏，将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按2∶1.5∶1.5∶1∶1∶1混合均匀，过滤即得保润增香添加剂。取添加剂50g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take epimedium, eclipta, sweet almond, motherwort, dandelion and citrus red, grind them and extract them separately, add 10 times the amount of purified water respectively, soak for 12 hours, heat reflux at 80°C for 1.5 hours, extract 3 times in total, and combine Three extracts were concentrated to a fluid extract with a density of 1.12 at 75°C and a pressure of 0.08Mpa. Add 2 times the volume of ethanol, let it stand for 36 hours, filter the precipitate, concentrate the fluid extract to a density of 1.12 under the condition of 75°C and a pressure of 0.08Mpa, and mix the fluid extracts of Epimedium, Eclipta, sweet almond, motherwort, dandelion and orange red The extract is mixed uniformly according to the ratio of 2:1.5:1.5:1:1:1, and filtered to obtain the moisturizing and flavoring additive. Take 50g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例九Embodiment nine
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入12倍量纯净水，浸泡18h后，85℃热回流提取2h，共提取3次，合并3次提取液，80℃，压力0.02Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置48h，过滤沉淀，80℃，压力0.02Mpa条件下浓缩至密度为1.12流浸膏，将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按3∶2∶2∶2∶1.5∶1混合均匀，过滤即得保润增香添加剂。取添加剂100g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Epimedium, Eclipta, sweet almond, motherwort, dandelion, and citrus were extracted separately after crushing, and 12 times the amount of purified water was added respectively. After soaking for 18 hours, heat reflux at 85°C for 2 hours, extracted 3 times in total, and combined 3 The secondary extract is concentrated to a fluid extract with a density of 1.12 at 80°C and a pressure of 0.02Mpa. Add 2 times the volume of ethanol, let it stand for 48 hours, filter the precipitate, concentrate the fluid extract to a density of 1.12 under the condition of 80°C and a pressure of 0.02Mpa, and mix the fluid extracts of Epimedium, Eclipta, sweet almond, motherwort, dandelion and orange red The extract is mixed uniformly according to the ratio of 3:2:2:2:1.5:1, and filtered to obtain the moisturizing and flavoring additive. Take 100g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例十Embodiment ten
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入6倍量纯净水，浸泡24h后，90℃热回流提取2.5h，共提取3次，合并3次提取液，65℃，压力0.04Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置60h，过滤沉淀，65℃，压力0.04Mpa条件下浓缩至密度为1.12流浸膏，将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按4∶3∶2∶2∶1.5∶1混合均匀，过滤即得保润增香添加剂。取添加剂500g，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take epimedium, eclipta, sweet almond, motherwort, dandelion, and citrus red, grind them and extract them separately, add 6 times the amount of pure water respectively, soak for 24 hours, heat reflux at 90°C for 2.5 hours, extract 3 times in total, and combine Three extracts were concentrated to a fluid extract with a density of 1.12 at 65°C and a pressure of 0.04Mpa. Add 2 times the volume of ethanol, let it stand for 60 hours, filter the precipitate, concentrate the fluid extract to a density of 1.12 under the condition of 65°C and a pressure of 0.04Mpa, and mix the fluid extracts of Epimedium, Eclipta, sweet almond, motherwort, dandelion, and orange red The extract is mixed uniformly according to the ratio of 4:3:2:2:1.5:1, and filtered to obtain the moisturizing and flavoring additive. Take 500g of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例十一Embodiment Eleven
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入10倍量纯净水，浸泡36h后，65℃热回流提取3h，共提取3次，合并3次提取液，60℃，压力0.06Mpa条件下浓缩至密度为1.12流浸膏。加入2倍体积乙醇，静置72h，过滤沉淀，60℃，压力0.06Mpa条件下浓缩至密度为1.12流浸膏，将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按6∶5∶4∶3∶2∶1混合均匀，过滤即得保润增香添加剂。取添加剂1kg，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take epimedium, eclipta, sweet almond, motherwort, dandelion, and citrus red, grind them and extract them separately, add 10 times the amount of purified water respectively, soak for 36 hours, heat reflux at 65°C for 3 hours, extract 3 times in total, and combine 3 The secondary extract is concentrated to a fluid extract with a density of 1.12 at 60°C and a pressure of 0.06Mpa. Add 2 times the volume of ethanol, let it stand for 72 hours, filter the precipitate, concentrate the liquid extract to a density of 1.12 under the condition of 60°C and a pressure of 0.06Mpa, and mix the liquid extract of Epimedium, Eclipta, sweet almond, motherwort, dandelion, and orange red. The extract is mixed uniformly according to the ratio of 6:5:4:3:2:1, and filtered to obtain the moisturizing and flavoring additive. Take 1kg of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
实施例十二
取淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红，粉碎后单独提取，分别加入15倍量纯净水，浸泡48h后，100℃热回流提取3h，共提取3次，合并3次提取液，80℃，压力0.03Mpa条件下浓缩至密度为1.13流浸膏。加入2倍体积乙醇，静置96h，过滤沉淀，80℃，压力0.03Mpa条件下浓缩至密度为1.13流浸膏，将淫羊藿、墨旱莲、甜杏仁、益母草、蒲公英和化橘红的流浸膏按8∶6∶4∶4∶5∶1混合均匀，过滤即得保润增香添加剂。取添加剂5kg，溶于20kg蒸馏水，喷洒于500kg烟丝后，卷制成卷烟。Take epimedium, eclipta, sweet almond, motherwort, dandelion and citrus red, extract them separately after crushing, add 15 times the amount of purified water respectively, soak for 48 hours, heat reflux at 100°C for 3 hours, extract 3 times in total, and combine 3 The secondary extract is concentrated to a fluid extract with a density of 1.13 at 80°C and a pressure of 0.03Mpa. Add 2 times the volume of ethanol, let it stand for 96 hours, filter the precipitate, concentrate the fluid extract to a density of 1.13 under the condition of 80°C and a pressure of 0.03Mpa, and mix the fluid extract of Epimedium, Eclipta, sweet almond, motherwort, dandelion, and orange red The extract is mixed uniformly according to the ratio of 8:6:4:4:5:1, and filtered to obtain the moisturizing and flavoring additive. Take 5kg of the additive, dissolve it in 20kg of distilled water, spray it on 500kg of shredded tobacco, and roll it into cigarettes.
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| CN103497834B (en)* | 2013-10-22 | 2015-07-08 | 中国烟草总公司郑州烟草研究院 | Method for preparing dandelion absolute oil and application of dandelion absolute oil in cigarettes |
| CN103710149A (en)* | 2013-12-30 | 2014-04-09 | 湖南先伟实业有限公司 | Wild chrysanthemum extract and taraxacum extract matched tobacco flavor, preparation method and application thereof |
| CN105011370A (en)* | 2015-07-29 | 2015-11-04 | 将军烟草集团有限公司 | Cigarette moisture-preserving and harm-reducing device |
| CN109330016A (en)* | 2018-11-14 | 2019-02-15 | 河南中烟工业有限责任公司 | A kind of Huajuhong extract, its preparation method and application in cigarette |
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|---|---|
| CN102697169B (en) | 2014-08-20 |
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