CN102070983A - Antibacterial ultraviolet-curable coating - Google Patents
Antibacterial ultraviolet-curable coatingDownload PDFInfo
- Publication number
- CN102070983A CN102070983ACN2010106189057ACN201010618905ACN102070983ACN 102070983 ACN102070983 ACN 102070983ACN 2010106189057 ACN2010106189057 ACN 2010106189057ACN 201010618905 ACN201010618905 ACN 201010618905ACN 102070983 ACN102070983 ACN 102070983A
- Authority
- CN
- China
- Prior art keywords
- coating material
- material solidified
- antibacterial ultraviolet
- ultraviolet according
- antibacterial
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011248coating agentSubstances0.000titleclaimsabstractdescription29
- 238000000576coating methodMethods0.000titleclaimsabstractdescription29
- 230000000844anti-bacterial effectEffects0.000titleclaimsabstractdescription20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-NSilicium dioxideChemical compoundO=[Si]=OVYPSYNLAJGMNEJ-UHFFFAOYSA-N0.000claimsabstractdescription24
- 125000003118aryl groupChemical group0.000claimsabstractdescription6
- 239000000463materialSubstances0.000claimsdescription15
- 239000000377silicon dioxideSubstances0.000claimsdescription8
- -12-hydroxy-2-methyl-1-phenyl-1-propyl group ketoneChemical class0.000claimsdescription6
- CSCPPACGZOOCGX-UHFFFAOYSA-NAcetoneChemical compoundCC(C)=OCSCPPACGZOOCGX-UHFFFAOYSA-N0.000claimsdescription6
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- 239000003795chemical substances by applicationSubstances0.000claimsdescription6
- 229920005989resinPolymers0.000claimsdescription5
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- 239000002904solventSubstances0.000claimsdescription5
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N2-ButanoneChemical compoundCCC(C)=OZWEHNKRNPOVVGH-UHFFFAOYSA-N0.000claimsdescription4
- LCGLNKUTAGEVQW-UHFFFAOYSA-NDimethyl etherChemical compoundCOCLCGLNKUTAGEVQW-UHFFFAOYSA-N0.000claimsdescription4
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- DKPFZGUDAPQIHT-UHFFFAOYSA-Nbutyl acetateChemical compoundCCCCOC(C)=ODKPFZGUDAPQIHT-UHFFFAOYSA-N0.000claimsdescription4
- UHESRSKEBRADOO-UHFFFAOYSA-Nethyl carbamate;prop-2-enoic acidChemical compoundOC(=O)C=C.CCOC(N)=OUHESRSKEBRADOO-UHFFFAOYSA-N0.000claimsdescription4
- KRIOVPPHQSLHCZ-UHFFFAOYSA-NpropiophenoneChemical compoundCCC(=O)C1=CC=CC=C1KRIOVPPHQSLHCZ-UHFFFAOYSA-N0.000claimsdescription4
- 229910000108silver(I,III) oxideInorganic materials0.000claimsdescription4
- NIXOWILDQLNWCW-UHFFFAOYSA-MAcrylateChemical compound[O-]C(=O)C=CNIXOWILDQLNWCW-UHFFFAOYSA-M0.000claimsdescription3
- APZPSKFMSWZPKL-UHFFFAOYSA-N[3-hydroxy-2,2-bis(hydroxymethyl)propyl] 2-methylprop-2-enoateChemical compoundCC(=C)C(=O)OCC(CO)(CO)COAPZPSKFMSWZPKL-UHFFFAOYSA-N0.000claimsdescription3
- RWCCWEUUXYIKHB-UHFFFAOYSA-NbenzophenoneChemical compoundC=1C=CC=CC=1C(=O)C1=CC=CC=C1RWCCWEUUXYIKHB-UHFFFAOYSA-N0.000claimsdescription3
- 239000012965benzophenoneSubstances0.000claimsdescription3
- 239000000178monomerSubstances0.000claimsdescription3
- GZBSIABKXVPBFY-UHFFFAOYSA-N2,2-bis(hydroxymethyl)propane-1,3-diol;prop-2-enoic acidChemical compoundOC(=O)C=C.OC(=O)C=C.OC(=O)C=C.OC(=O)C=C.OCC(CO)(CO)COGZBSIABKXVPBFY-UHFFFAOYSA-N0.000claimsdescription2
- 239000004721Polyphenylene oxideSubstances0.000claimsdescription2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-NSiliconChemical compound[Si]XUIMIQQOPSSXEZ-UHFFFAOYSA-N0.000claimsdescription2
- 244000028419Styrax benzoinSpecies0.000claimsdescription2
- 235000000126Styrax benzoinNutrition0.000claimsdescription2
- 235000008411Sumatra benzointreeNutrition0.000claimsdescription2
- HVVWZTWDBSEWIH-UHFFFAOYSA-N[2-(hydroxymethyl)-3-prop-2-enoyloxy-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoateChemical groupC=CC(=O)OCC(CO)(COC(=O)C=C)COC(=O)C=CHVVWZTWDBSEWIH-UHFFFAOYSA-N0.000claimsdescription2
- 239000002253acidSubstances0.000claimsdescription2
- 229960002130benzoinDrugs0.000claimsdescription2
- 239000004205dimethyl polysiloxaneSubstances0.000claimsdescription2
- 150000002148estersChemical class0.000claimsdescription2
- 235000019382gum benzoicNutrition0.000claimsdescription2
- YDKNBNOOCSNPNS-UHFFFAOYSA-Nmethyl 1,3-benzoxazole-2-carboxylateChemical compoundC1=CC=C2OC(C(=O)OC)=NC2=C1YDKNBNOOCSNPNS-UHFFFAOYSA-N0.000claimsdescription2
- 230000004048modificationEffects0.000claimsdescription2
- 238000012986modificationMethods0.000claimsdescription2
- 229940059574pentaerithritylDrugs0.000claimsdescription2
- WXZMFSXDPGVJKK-UHFFFAOYSA-NpentaerythritolChemical compoundOCC(CO)(CO)COWXZMFSXDPGVJKK-UHFFFAOYSA-N0.000claimsdescription2
- 229920000435poly(dimethylsiloxane)Polymers0.000claimsdescription2
- 229920000728polyesterPolymers0.000claimsdescription2
- 229920000570polyetherPolymers0.000claimsdescription2
- QQONPFPTGQHPMA-UHFFFAOYSA-NpropyleneNatural productsCC=CQQONPFPTGQHPMA-UHFFFAOYSA-N0.000claimsdescription2
- 229910052710siliconInorganic materials0.000claimsdescription2
- 239000010703siliconSubstances0.000claimsdescription2
- 125000000391vinyl groupChemical group[H]C([*])=C([H])[H]0.000claimsdescription2
- 229920002554vinyl polymerPolymers0.000claimsdescription2
- 238000004132cross linkingMethods0.000abstractdescription2
- 239000005543nano-size silicon particleSubstances0.000abstract4
- 235000012239silicon dioxideNutrition0.000abstract4
- NDVLTYZPCACLMA-UHFFFAOYSA-Nsilver oxideChemical compound[O-2].[Ag+].[Ag+]NDVLTYZPCACLMA-UHFFFAOYSA-N0.000abstract4
- 229910001923silver oxideInorganic materials0.000abstract2
- MPIAGWXWVAHQBB-UHFFFAOYSA-N[3-prop-2-enoyloxy-2-[[3-prop-2-enoyloxy-2,2-bis(prop-2-enoyloxymethyl)propoxy]methyl]-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoateChemical compoundC=CC(=O)OCC(COC(=O)C=C)(COC(=O)C=C)COCC(COC(=O)C=C)(COC(=O)C=C)COC(=O)C=CMPIAGWXWVAHQBB-UHFFFAOYSA-N0.000abstract1
- 238000005054agglomerationMethods0.000abstract1
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- 238000007711solidificationMethods0.000description4
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- 150000003254radicalsChemical class0.000description3
- 238000000034methodMethods0.000description2
- 239000003504photosensitizing agentSubstances0.000description2
- 239000000126substanceSubstances0.000description2
- 241000305071EnterobacteralesSpecies0.000description1
- 241000191940StaphylococcusSpecies0.000description1
- PPBRXRYQALVLMV-UHFFFAOYSA-NStyreneChemical compoundC=CC1=CC=CC=C1PPBRXRYQALVLMV-UHFFFAOYSA-N0.000description1
- NIXOWILDQLNWCW-UHFFFAOYSA-Nacrylic acid groupChemical groupC(C=C)(=O)ONIXOWILDQLNWCW-UHFFFAOYSA-N0.000description1
- 239000000654additiveSubstances0.000description1
- 150000005215alkyl ethersChemical class0.000description1
- QVGXLLKOCUKJST-UHFFFAOYSA-Natomic oxygenChemical compound[O]QVGXLLKOCUKJST-UHFFFAOYSA-N0.000description1
- 238000006243chemical reactionMethods0.000description1
- 150000001875compoundsChemical class0.000description1
- 230000000694effectsEffects0.000description1
- 239000000945fillerSubstances0.000description1
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- 239000010985leatherSubstances0.000description1
- 239000001301oxygenSubstances0.000description1
- 229910052760oxygenInorganic materials0.000description1
- 239000000123paperSubstances0.000description1
- 239000000049pigmentSubstances0.000description1
- 239000004033plasticSubstances0.000description1
- 229920003023plasticPolymers0.000description1
- 229920000642polymerPolymers0.000description1
- 238000006116polymerization reactionMethods0.000description1
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Landscapes
- Paints Or Removers (AREA)
Abstract
Description
Technical field
The present invention relates to a kind of UV-light to visible light solidifying material, it is coating material solidified to relate in particular to a kind of antibacterial ultraviolet.
Background technology
Photo-cured coating claims photoactive coating again, is the ultraviolet-curing paint that is called of the paint solidification energy with the UV-light.UV-light (UV) is coating material solidified need not to be heated, can be on inflammable grounds such as paper, plastics, leather and timber film-forming rapidly.Ultraviolet-curing paint mainly is made up of photosensitive resin, photosensitizers (light trigger) and thinner, adds some additives simultaneously, as thermo-stabilizer, adds pigment and filler during the preparation colored paint.
Photosensitive resin generally is the low-molecular-weight resin that has unsaturated link(age), as unsaturated polyester, acrylic oligomers; Photosensitizers is easily to absorb the compound that UV-light produces living radical, as benzophenone, st-yrax alkyl ether; The main effect of thinner is to reduce dope viscosity, also participates in film-forming simultaneously, is reactive thinner, as vinylbenzene, acrylate etc.
The photo-cured coating advantage is set time short (part second to several minutes), solidification value is low, volatile matter is low, is to economize the energy, resource-saving, nuisanceless, high efficiency coating new variety; Its shortcoming is that free radical type photo-cured coating solidification process is prevented by oxygen, and surface cure is bad.
Traditional paint solidification is that the method for physical dryness is removed the solvent in the macromolecular solution by heating normally, obtains the hardened paint film.It then is to utilize the energy of UV-light to cause low molecule performed polymer in the coating or oligomer and as polymerization between the monomer molecule of reactive thinner and crosslinking reaction, obtain the paint film that hardens that UV solidifies, and comes down to realize chemical seasoning by forming chemical bond.
UV coating is widely used in the various electronic products at present, especially on toy, mobile phone, computor-keyboard, therefore this electronic product requires it to possess certain antibacterial effect owing to contact frequently with human body, and therefore providing a kind of antibacterial ultraviolet coating material solidified is the technology that industry is thirsted for always.
Summary of the invention
It is coating material solidified to the invention provides a kind of antibacterial ultraviolet, adopts silver suboxide to combine with the aromatic urethane acrylate, can play good antibacterial effect.
The present invention is achieved by the following technical solutions: a kind of antibacterial ultraviolet is coating material solidified, and the component and the mass percent of described photo-cured coating are as follows
Aromatic urethane acrylate 40～60%
Crosslinked thinner 25～45%
Light trigger 2～12%
Nanometer grade silica 5～15%
Silver suboxide 0.5～1%.
Further preferably, also comprise in the described photo-cured coating:
Solvent 5～20%.
Further preferably, also comprise in the described photo-cured coating:
Flow agent 0.2～1%.
More preferably, described crosslinked thinner is selected from pentaerythritol triacrylate, tetramethylol methane tetraacrylate, tetramethylolmethane six acrylate, the neopentylglycol diacrylate one or more.
More preferably, described light trigger is selected from 2-hydroxy-2-methyl-1-phenyl-1-propyl group ketone, 2,4, in 6-trimethylbenzoyl diphenyl phosphine oxide, 1-hydroxyl-ring ethyl-phenyl ketone, benzoin dimethylether, the benzophenone one or more.
Described nanometer grade silica is meant grafted nanometer grade silica on double pentaerythritol methacrylate.
More preferably, described flow agent is selected from organic silicon modified by polyether, polyester modification organosilicon, polyacrylic ester, propylene soda acid and holds resin, polydimethylsiloxane, PSI, in the organic radical modified polyorganosiloxane one or more.
More preferably, described solvent is selected from vinyl acetic monomer, N-BUTYL ACETATE, toluene, dimethylbenzene, acetone, the butanone one or more.
Because nanometer grade silica is reunited in system easily, disperse inhomogeneously, can influence the transparency and the wear resistance of system, the grafted nanometer grade silica can well solve the transparency and the wear resistance of system on double pentaerythritol methacrylate.Adopt silver suboxide to combine, can play good antibacterial effect with the aromatic urethane acrylate.
Embodiment
Below by embodiment the present invention is further elaborated.
The light curing agent that the various embodiments described above are made is applied on the mobile phone products, test in the laboratory then, measure this patent light curing agent Chinese People's Anti-Japanese Military and Political College enterobacteria rate and reach 99.5%, the staphylococcus rate reaches 99.8%, and this patent product has very strong antibacterial effect as can be seen.Those skilled in the art will recognize that; above-mentioned embodiment is exemplary; be in order to make those skilled in the art can better understand this patent content; should not be construed as is restriction to this patent protection domain; change or modify so long as disclose spiritual any being equal to of being done, all fall into this patent protection domain according to this patent.
Claims (8)
1. an antibacterial ultraviolet is coating material solidified, it is characterized in that, the component and the mass percent of described photo-cured coating are as follows
Aromatic urethane acrylate 40～60%
Crosslinked thinner 25～45%
Light trigger 2～12%
Nanometer grade silica 5～15%
Silver suboxide 0.5～1%.
2. antibacterial ultraviolet according to claim 1 is coating material solidified, it is characterized in that,
Also comprise in the described photo-cured coating:
Solvent 5～20%.
3. antibacterial ultraviolet according to claim 1 and 2 is coating material solidified, it is characterized in that,
Also comprise in the described photo-cured coating:
Flow agent 0.2～1%.
4. antibacterial ultraviolet according to claim 3 is coating material solidified, it is characterized in that,
Described crosslinked thinner is selected from pentaerythritol triacrylate, tetramethylol methane tetraacrylate, tetramethylolmethane six acrylate, the neopentylglycol diacrylate one or more.
5. antibacterial ultraviolet according to claim 3 is coating material solidified, it is characterized in that,
Described light trigger is selected from 2-hydroxy-2-methyl-1-phenyl-1-propyl group ketone, 2,4, in 6-trimethylbenzoyl diphenyl phosphine oxide, 1-hydroxyl-ring ethyl-phenyl ketone, benzoin dimethylether, the benzophenone one or more.
6. antibacterial ultraviolet according to claim 3 is coating material solidified, it is characterized in that,
Described nanometer grade silica is meant grafted nanometer grade silica on double pentaerythritol methacrylate.
7. antibacterial ultraviolet according to claim 3 is coating material solidified, it is characterized in that,
Described solvent is selected from vinyl acetic monomer, N-BUTYL ACETATE, toluene, dimethylbenzene, acetone, the butanone one or more.
8. antibacterial ultraviolet according to claim 3 is coating material solidified, it is characterized in that,
Described flow agent is selected from organic silicon modified by polyether, polyester modification organosilicon, polyacrylic ester, propylene soda acid and holds resin, polydimethylsiloxane, PSI, in the organic radical modified polyorganosiloxane one or more.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106189057ACN102070983A (en) | 2010-12-31 | 2010-12-31 | Antibacterial ultraviolet-curable coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010106189057ACN102070983A (en) | 2010-12-31 | 2010-12-31 | Antibacterial ultraviolet-curable coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102070983Atrue CN102070983A (en) | 2011-05-25 |
Family
ID=44029745
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010106189057APendingCN102070983A (en) | 2010-12-31 | 2010-12-31 | Antibacterial ultraviolet-curable coating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102070983A (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103264540A (en)* | 2013-05-20 | 2013-08-28 | 北京合众研创科技有限公司 | Antisepsis film |
| CN103396737A (en)* | 2013-07-10 | 2013-11-20 | 淮南联合大学 | High temperature resistant ultraviolet curing coating and preparation method of same |
| WO2014126862A1 (en)* | 2013-02-13 | 2014-08-21 | Becton, Dickinson And Company | Uv curable solventless antimicrobial compositions |
| CN104277675A (en)* | 2014-10-27 | 2015-01-14 | 芜湖县双宝建材有限公司 | Highly wear-resisting antibacterial water-based ultraviolet curing paint |
| US9352119B2 (en) | 2012-05-15 | 2016-05-31 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| US9579486B2 (en) | 2012-08-22 | 2017-02-28 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| US9675793B2 (en) | 2014-04-23 | 2017-06-13 | Becton, Dickinson And Company | Catheter tubing with extraluminal antimicrobial coating |
| US9750928B2 (en) | 2013-02-13 | 2017-09-05 | Becton, Dickinson And Company | Blood control IV catheter with stationary septum activator |
| US9789279B2 (en) | 2014-04-23 | 2017-10-17 | Becton, Dickinson And Company | Antimicrobial obturator for use with vascular access devices |
| CN109135603A (en)* | 2018-08-02 | 2019-01-04 | 江苏双星彩塑新材料股份有限公司 | A kind of antibacterial explosion-proof fenestrated membrane |
| US10232088B2 (en) | 2014-07-08 | 2019-03-19 | Becton, Dickinson And Company | Antimicrobial coating forming kink resistant feature on a vascular access device |
| US10376686B2 (en) | 2014-04-23 | 2019-08-13 | Becton, Dickinson And Company | Antimicrobial caps for medical connectors |
| US10493244B2 (en) | 2015-10-28 | 2019-12-03 | Becton, Dickinson And Company | Extension tubing strain relief |
| CN112795302A (en)* | 2021-01-14 | 2021-05-14 | 昆山三越油墨有限公司 | Water-based ultraviolet-curing antibacterial and anti-fouling material for touch surface and preparation method thereof |
| CN116018364A (en)* | 2020-12-11 | 2023-04-25 | 东洋油墨Sc控股株式会社 | Antibacterial active energy ray-curable coating composition, coating, antibacterial member, and article |
- 2010
- 2010-12-31CNCN2010106189057Apatent/CN102070983A/enactivePending
Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9770580B2 (en) | 2012-05-15 | 2017-09-26 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| US9352119B2 (en) | 2012-05-15 | 2016-05-31 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| US9579486B2 (en) | 2012-08-22 | 2017-02-28 | Becton, Dickinson And Company | Blood control IV catheter with antimicrobial properties |
| WO2014126862A1 (en)* | 2013-02-13 | 2014-08-21 | Becton, Dickinson And Company | Uv curable solventless antimicrobial compositions |
| US11357962B2 (en) | 2013-02-13 | 2022-06-14 | Becton, Dickinson And Company | Blood control IV catheter with stationary septum activator |
| US9695323B2 (en) | 2013-02-13 | 2017-07-04 | Becton, Dickinson And Company | UV curable solventless antimicrobial compositions |
| US9750928B2 (en) | 2013-02-13 | 2017-09-05 | Becton, Dickinson And Company | Blood control IV catheter with stationary septum activator |
| CN103264540A (en)* | 2013-05-20 | 2013-08-28 | 北京合众研创科技有限公司 | Antisepsis film |
| CN103396737A (en)* | 2013-07-10 | 2013-11-20 | 淮南联合大学 | High temperature resistant ultraviolet curing coating and preparation method of same |
| US9789279B2 (en) | 2014-04-23 | 2017-10-17 | Becton, Dickinson And Company | Antimicrobial obturator for use with vascular access devices |
| US11357965B2 (en) | 2014-04-23 | 2022-06-14 | Becton, Dickinson And Company | Antimicrobial caps for medical connectors |
| US9956379B2 (en) | 2014-04-23 | 2018-05-01 | Becton, Dickinson And Company | Catheter tubing with extraluminal antimicrobial coating |
| US9675793B2 (en) | 2014-04-23 | 2017-06-13 | Becton, Dickinson And Company | Catheter tubing with extraluminal antimicrobial coating |
| US10589063B2 (en) | 2014-04-23 | 2020-03-17 | Becton, Dickinson And Company | Antimicrobial obturator for use with vascular access devices |
| US10376686B2 (en) | 2014-04-23 | 2019-08-13 | Becton, Dickinson And Company | Antimicrobial caps for medical connectors |
| US10232088B2 (en) | 2014-07-08 | 2019-03-19 | Becton, Dickinson And Company | Antimicrobial coating forming kink resistant feature on a vascular access device |
| US11219705B2 (en) | 2014-07-08 | 2022-01-11 | Becton, Dickinson And Company | Antimicrobial coating forming kink resistant feature on a vascular access device |
| CN104277675A (en)* | 2014-10-27 | 2015-01-14 | 芜湖县双宝建材有限公司 | Highly wear-resisting antibacterial water-based ultraviolet curing paint |
| US10493244B2 (en) | 2015-10-28 | 2019-12-03 | Becton, Dickinson And Company | Extension tubing strain relief |
| US11904114B2 (en) | 2015-10-28 | 2024-02-20 | Becton, Dickinson And Company | Extension tubing strain relief |
| CN109135603A (en)* | 2018-08-02 | 2019-01-04 | 江苏双星彩塑新材料股份有限公司 | A kind of antibacterial explosion-proof fenestrated membrane |
| CN116018364A (en)* | 2020-12-11 | 2023-04-25 | 东洋油墨Sc控股株式会社 | Antibacterial active energy ray-curable coating composition, coating, antibacterial member, and article |
| CN112795302A (en)* | 2021-01-14 | 2021-05-14 | 昆山三越油墨有限公司 | Water-based ultraviolet-curing antibacterial and anti-fouling material for touch surface and preparation method thereof |
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| WD01 | Invention patent application deemed withdrawn after publication | Application publication date:20110525 |