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Selenite fluoride

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From Wikipedia, the free encyclopedia

Class of chemical compounds

Aselenite fluoride is a chemical compound or salt that containsfluoride andselenite anions (F⁻
andSeO²⁻
₃). These aremixed anion compounds. Some have third anions, includingnitrate (NO⁻
₃),molybdate (MoO²⁻
₄),oxalate (C
₂O²⁻
₄),selenate (SeO²⁻
₄),silicate (SiO²⁻
₄) andtellurate (TeO²⁻
₄).

Naming

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A selenite fluoride compound may also be called a fluoride oxoselenate(IV) using IUPAC naming for inorganic compounds.

Production

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Rare earth selenite fluorides can be produced by dissolving the rare earthselenate into moltenlithium fluoride at over 800°C, whereupon the selenate loses oxygen to become selenite, and crystals of the selenite fluoride can form.^[1] Another similar method involves heating the rare earth oxide, with a rare earth fluoride and selenium dioxide with acaesium bromide flux. If glass or silica containers are used, they are eaten away by the molten flux and silicates are formed some of which may be fluoride selenite silicate compounds.^[2]

[edit]

Related to these are theselenite chlorides andselenite bromides by varying the halogenide. Similar compounds by varying thechalcogen also include thesulfite fluorides andtellurite fluorides.

List

[edit]

name	formula	ratio SeO₃:F	mw	system	space group	unit cell Å	volume	density	optical	references
scandium selenite fluoride	ScSeO₃F	1:1		triclinic	P1 <13	−173°C a=6.2769 b=6.5578 c=4.0627 α=95.478 β=95.332 γ=92.363 Z=2		3.830		^[3]
scandium selenite fluoride	ScSeO₃F	1:1		monoclinic	P2₁/m >13	a=4.0643b =6.6109c=6.32.35β=93.298° Z=2				^[2]
	Na₃Ti₃O₃(SeO₃)₄F	4:1		hexagonal	P6₃	a =12.8439c =5.2339			SHG 6 × KDP	^[4]
dimanganese difluoride selenite	Mn₂SeO₃F₂	1:2	274.83	orthorhombic	Pnma	a = 7.50848b = 10.350 andc = 5.47697 Z=4			pink	^[5]
ferric difluoride selenite	FeSeO₃F	1:1	201.81	monoclinic	P2₁/n	a=4.9559 b=5.2023 c=12.040β=97.87 Z=4	307.50	4.359	yellow	^[6]
ammonium diferric trifluoride diselenite	NH₄Fe₂F₃(SeO₃)₂	2:3								^[7]
piperizinium	[C₄N₂H₁₂]Fe₄F₆(SeO₃)₄	2:3	933.40	monoclinic	C2/c	a=15.168 b=7.3973 c=16.127β=90.044 Z=5	1928.9	3.14	brown	^[7]
diethylenetriamine	[C₄N₃H₁₄]Fe₄F₆(SeO₃)₄	2:3								^[7]
dicobalt difluoride selenite	Co₂SeO₃F₂	1:2	282.82	orthorhombic	Pnma	a = 7.2655b = 10.001c = 5.3564 Z=4	389.22	4.826	pink	^[8]
	Ni₂(SeO₃)F₂	1:2	282.3	orthorhombic	Pnma	a=7.1727 b=9.9377 c=5.2364	373.25		yellow	^[9]
dicopper difluoride selenite	Cu₂(SeO₃)F₂	1:2	292.05	orthorhombic	Pnma	a = 7.066b = 9.590c = 5.563 Z=4	377.0	5.146	light green	^[10]
dizinc difluoride selenite	Zn₂(SeO₃)F₂	1:2	295.70	orthorhombic	Pnma	a=7.276 b=10.042 c=5.256 Z=4	384.0	5.114	colourless	^[11]
triethylenediamin-di-ium digallium hexafluoride selenite	C₆H₁₄N₂Ga₂F₆SeO₃	1:6	494.59	Monoclinic	P2₁/c	a=12.616 b=7.2700 c=13.605β=104.746 Z=4	1206.8	2.722	colourless	^[12]
ethelenediamin-di-ium gallium trifluoride selenite	C₂H₁₀N₂GaF₃SeO₃	1:3	315.80	monoclinic	P2₁/c	a=9.1107 b=8.0382 c=10.8302β=90.045 Z=4	793.1	2.2355	colourless	^[12]
piperizin-di-ium gallium fluoride oxalate selenite hydrate	H₂pipGaFSeO₃[C₂O₄]H₂O	1:1	409.87	triclinic	P1	a=6.377 b=9.2820 c=11.4112 α=66.53 β=77.44 γ=71.89	585.47	2.325	colourless	^[12]
	(C₄H₁₅N₃)₂Ga₄F₂(SeO₃)₆(C₂O₄).4H₂O	6:2	1467.11	triclinic	P1	a=8.9941 b=9.4963 c=11.2959 α=77.13 β=68.073 γ=83.776 Z=1	872.17	2.793	colourless	^[12]
	Sr(VO₂F)(SeO₃)		316.52	orthorhombic	Pbca	a=9.7816 b=8.0278 c=12.927 Z=8	1015.07	4.142	yellow	^[13]
yttrium selenite fluoride	YSeO₃F	1:1		monoclinic	P2₁/c <319	a=6.5765 b=6.8971 c=7.1728β=99.036 Z=4				^[14]^[3]^[15]
yttrium selenite fluoride	YSeO₃F	1:1		monoclinc	P 2₁/m >319	600° a=6.5840 b=6.9809 c=4.3434 β =95.032 Z=2		3.922		^[3]
	Ag₃Ti₃O₃(SeO₃)₄F		1042.15	hexagonal	P6₃	a=12.8975 c=5.2180 Z=2	751.70	4.604	colourless SHG 2×KDP	^[16]
	Ag₂ZrF₂(SeO₃)₂		598.88	orthorhombic	Cmca	a=7.3640 b=31.451 c=6.2719	1452.6	5.477	colopurless	^[16]
dicadmium difluoride selenite	Cd₂(SeO₃)F₂	1:2	389.76	orthorhombic	Pnma	a=7.803 b=10.566 c=5.729 Z=4	472.4	5.480	colourless	^[11]
ethelenediamin-di-ium indium trifluoride selenite	C₂H₁₀N₂InF₃SeO₃		360.90	monoclinic	P2₁/c	a=9.3066 b=8.3012 c=11.2923 Z=4	871.68	2.750	colourless	^[12]
caesium triscandium hexafluoride diselenite	CsSc₃F₆[SeO₃]₂	2:6		trigonal	P3m1	a = 5.6534c = 10.6987Z = 1				^[17]
	Cs(TiOF)₃(SeO₃)₂	2:3	635.53	hexagonal	P6₃mc	a=7.2420 c=11.8152 Z=2	536.65	3.933	Colourless SHG 5xKDP	^[18]
caesium triiron hexafluoride diselenite	CsFe₃(SeO₃)₂F₆	2:6		trigonal	P3m1	a=5.459 c=10.537 Z=1	271.9		cyan	^[19]
	Ba(VO₂F)(SeO₃)		366.24	orthorhombic	Pbca	a=10.0539 b=8.3967 c=13.174	1112.18	4.375	yellow	^[13]
lanthanum selenite fluoride	LaSeO₃F	1:1		monoclinic	P2₁/c	a = 18.198 b = 7.1575 c = 8.464 β = 96.89 Z = 12				^[1]^[20]
cerium selenite fluoride	CeSeO₃F	1:1								^[14]
tetrapraseodymium selenate diselenite hexafluoride	Pr₄(SeO₃)₂(SeO₄)F₆	2:6		monoclinic	C2/c	a = 22.305 b = 7.1054 c = 8.356 β = 98.05° Z = 4				^[21]
tripraseodymium fluoride tetraselenite	Pr₃F[SeO₃]₄								pale green	^[22]
	Pr₅F[SiO₄]₂[SeO₃]₃	3:1		triclinic	P1	a = 7.0114b = 9.8268c = 12.8679α = 70.552β = 76.904γ = 69.417°Z = 2		5.511	pale green	^[22]
trineodymium fluoride tetraselenite	Nd₃(SeO₃)₄F			hexagonal	P6₃mc	a=10.515 c=7.1211				^[23]
trisamarium fluoride tetraselenite	Sm₃(SeO₃)₄F			hexagonal	P6₃mc	a=10.474 c=7.0224				^[23]
trigadolinium tetraselenite fluoride	Gd₃(SeO₃)₄F	4:1		hexagonal	P6₃mc	a = 10.443 b = 6.9432 Z=2				^[24]^[1]
tridysprosium tetraselenite fluoride	Dy₃(SeO₃)₄F	4:1	1014.34	hexagonal	P6₃mc	a=10.360c=6.8647 Z=2				^[1]
holmium selenite fluoride	HoSeO₃F	1:1		monoclinic	P2₁/c	a=6.5784 b=6.8873 c=7.1825 β =99.213 Z=4		6.43		^[15]
	Ho₃F[SeO₃]₄	4:1		hexagonal	P6₃mc	a = 10.3024c = 6.8037Z = 2				^[25]
erbium selenite fluoride	ErSeO₃F	1:1		monoclinic	P2₁/c	a=6.5553 b=6.8741 c=7.1516 β =99.020 Z=4		6.54		^[15]
	Er₃F[SiO₄][SeO₃]₂	2:1		orthorhombic	Pnna	a = 5.8692b = 15.2931c = 10.2967Z = 4			pink	^[22]^[26]
thulium selenite fluoride	TmSeO₃F	1:1		monoclinic	P2₁/c	a=6.5342 b=68607 c=7.1213 β =98,828 Z=4		6.63		^[15]
ytterbium selenite fluoride	YbSeO₃F	1:1		monoclinic	P2₁/c	a=6.5146 b=6.8475 c=7.0924 β =98.637 Z=4		6.77		^[15]
Lutetium selenite fluoride	LuF[SeO₃]	1:1		monoclinic	P2₁/c	−173°C: a=6.4839 b=6.8128 c=7.0581 β=98.657 Z=4	308.23	6.916		^[14]
				triclinic	P1	a=6.4486 b=6.8441 c=4.2798 α=94.063 β=98.657 γ=91.895 Z=2	187.04	5.698		^[14]
				monoclinic	P2₁/m	173°C: a=6.4734 b=6.8702 c=4.2843 β=95.602 Z=2	189.63	5.621		^[14]
trilutetium fluoride tetraselenite	Lu₃F(SeO₃)₄	4:1	1051.75	trigonal	P6₃	a=9.883 c=7.066 Z=2	597.7	5.844	colourless SHG 2.5×KDP	^[27]
	PbVO₂(SeO₃)F	1:1	436.09	orthorhombic	Pbca	a=9.812 b=8.147 c=13.026 Z=8	1041.3	5.563	yellow	^[28]
cadmium lead fluoride nitrate selenite	PbCdF(SeO₃)(NO₃)	1:1		orthorhombic	Pca2₁	a=11.121 b=10.366 c=5.3950 Z=4	621.9	5.634	SHG 2.6×KDP band gap 4.42 eV	^[29]
bismuth selenite fluoride	BiFSeO₃	1:1	354.94	orthorhombic	Pca2₁	a=6.6774 b=6.8872 c=7.4702 Z=4	343.54	6.862	colourless SHG 13.5×KDP	^[30]
tribismuth triselenite pyroselenite fluoride	Bi₃(SeO₃)₃(Se₂O₅)F	3:1		monoclinic	F21				SHG 3×KDP	^[31]
dibismuth potassium pentafluoride selenite	KBi₂SeO₃F₅	1:5	679.02	orthorhombic	Pbcm	a=4.553 b=17.80 c=8.80 Z=4	712.9	6.326	white band gap 4.08 eV	^[32]
dibismuth rubidium pentafluoride selenite	RbBi₂SeO₃F₅	1:5	725.39	Triclinic	P1	a=8.842 b=8.917 c=9.63 α=88.28 β=89.82 γ=89.76 Z=4	758.9	6.349	white band gap 4.18 eV	^[32]
	RbBi(SeO₃)F₂	1:2	459.41	orthorhombic	Pnma	a=13.251 b=6.073 c=6.780 Z=4	545.6			^[33]
	Bi₄TiO₂F₄(SeO₃)₄	4:4	1499.66	monoclinic	P2₁/c	a=7.0237 b=6.6824 c=17.3240 β=106.637 Z=2	779.07	6.393	colourless	^[34]
	Bi₄NbO₃F₃(SeO₃)₄	4:3	1541.67	monoclinic	P2₁/c	a=7.0448 b=6.6814 c=17.4051 β=106.931 Z=2	783.73	6.533	colourless	^[34]
	Bi₄TeO₄F₂(TeO₃)₂(SeO₃)₂	2:2	1670.64	monoclinic	P2₁/c	a=7.0304 b=6.6782 c=17.355 β=106.155 Z=2	782.66	7.089	colourless	^[34]
	Bi₂F₂(MoO₄)(SeO₃)	1:2	742.86	monoclinic	P2₁/c	a=7.1005 b=9.660 c=12.972 β=12.091 Z=4	753.82	6.546	colourless	^[34]
	Bi₂ZrO₂F₂(SeO₃)₂	2:2	833.10	triclinic	P1	a=5.8047 b=6.3469 c=6.7419 α=77.665 β=71.365 γ=72.795 Z=1	222.87	6.207	colourless	^[34]
	PbBi(SeO₃)₂F	2:1		orthorhombic	Pca2₁	a=12.9672b=4.5022c=11.8221			SHG 10.5×KDP; band gap 3.75 eV	^[35]

SHG=second harmonic generator

References

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^Ma, Yun-Xiang; Hu, Chun-Li; Li, Bing-Xuan; Kong, Fang; Mao, Jiang-Gao (2018-09-17). "PbCdF(SeO 3 )(NO 3 ): A Nonlinear Optical Material Produced by Synergistic Effect of Four Functional Units".Inorganic Chemistry.57 (18):11839–11846.doi:10.1021/acs.inorgchem.8b02044.ISSN 0020-1669.PMID 30160946.S2CID 52136440.
^Liang, Ming-Li; Hu, Chun-Li; Kong, Fang; Mao, Jiang-Gao (2016-08-03). "BiFSeO 3 : An Excellent SHG Material Designed by Aliovalent Substitution".Journal of the American Chemical Society.138 (30):9433–9436.Bibcode:2016JAChS.138.9433L.doi:10.1021/jacs.6b06680.ISSN 0002-7863.PMID 27428359.
^Chung, Jee Yoon; Jo, Hongil; Yeon, Seongbeom; Byun, Hye Ryung; You, Tae-Soo; Jang, Joon I.; Ok, Kang Min (2020-07-01)."Bi3(SeO3)3(Se2O5)F: A Polar Bismuth Selenite Fluoride with Polyhedra of Highly Distortive Lone Pair Cations and Strong Second-Harmonic Generation Response".Chemistry of Materials.32 (17):7318–7326.doi:10.1021/acs.chemmater.0c02167.ISSN 0897-4756.S2CID 225568240.
^^a ^bShi, Shuangshuang; Luo, Min; Lin, Chensheng; Ye, Ning (2018)."A cation size effect on the framework structures in ABi 2 SeO 3 F 5 (A = K and Rb): first examples of alkali metal bismuth selenite fluorides".Dalton Transactions.47 (18):6598–6604.doi:10.1039/C8DT00450A.ISSN 1477-9226.PMID 29700544.
^Shang, Meng; Halasyamani, P. Shiv (February 2020). "Mixed lone-pair and mixed anion compounds: Pb3(SeO3)(HSeO3)Br3, Pb3(SeO3)(OH)Br3, CdPb8(SeO3)4Cl4Br6 and RbBi(SeO3)F2".Journal of Solid State Chemistry.282: 121121.Bibcode:2020JSSCh.28221121S.doi:10.1016/j.jssc.2019.121121.S2CID 214467836.
^^a ^b ^c ^d ^eGong, Ya-Ping; Hu, Chun-Li; Kong, Fang; Mao, Jiang-Gao (2019-03-07). "Exploration of New Birefringent Crystals in Bismuth d 0 Transition Metal Selenites".Chemistry – A European Journal.25 (14):3685–3694.doi:10.1002/chem.201806328.ISSN 0947-6539.PMID 30637825.S2CID 58575389.
^Jia, Ying-Jie; Zhang, Xingyu; Chen, Yi-Gang; Jiang, Xingxing; Song, Jia-Neng; Lin, Zheshuai; Zhang, Xian-Ming (2022-10-03)."PbBi(SeO 3 ) 2 F and Pb 2 Bi(SeO 3 ) 2 Cl 3 : Coexistence of Three Kinds of Stereochemically Active Lone-Pair Cations Exhibiting Excellent Nonlinear Optical Properties".Inorganic Chemistry.61 (39):15368–15376.doi:10.1021/acs.inorgchem.2c01802.ISSN 0020-1669.PMID 36121404.S2CID 252366831.

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